O-(trimethylsilyl) thiobenzoate

Base Information

• Chemical Name: O-(trimethylsilyl) thiobenzoate
• CAS No.: 7528-43-0
• Molecular Formula: C₁₀H₁₄OSSi
• Molecular Weight: 210.372

Synonyms:O-(trimethylsilyl) thiobenzoate

Chemical Property of O-(trimethylsilyl) thiobenzoate

Chemical Property:

Purity/Quality:

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Technology Process of O-(trimethylsilyl) thiobenzoate

There total 4 articles about O-(trimethylsilyl) thiobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.5%

thiobenzoic acid (98-91-9) + 1,1,1,3,3,3-hexamethyl-disilazane (999-97-3) → O-(trimethylsilyl) thiobenzoate (7528-43-0)

Guidance literature:

With <(C6H5O)PO>2NH; In dichloromethane; for 0.5h; Heating;

DOI:10.1021/jo00141a031

Reference yield:

thiobenzoic acid (98-91-9) + chloro-trimethyl-silane (75-77-4) → O-(trimethylsilyl) thiobenzoate (7528-43-0)

Guidance literature:

With triethylamine; In diethyl ether;

DOI:10.1039/P19760000564

Reference yield:

chloro-trimethyl-silane (75-77-4) + benzoyl chloride (98-88-4) → O-(trimethylsilyl) thiobenzoate (7528-43-0)

Guidance literature:

Multistep reaction; (i) nPrNH₂, Et₃N, THF, CS₂, (ii) /BRN= 1209232/;

DOI:10.1055/s-1971-21817

upstream raw materials:

thiobenzoic acid

chloro-trimethyl-silane

benzoyl chloride

thiobenzoic acid

Downstream raw materials:

benzoyl sulfide

S-benzoyl O,O-diisopropyl phosphorothioite

diisopropyl thiobenzoyl phosphite

Benzoylsulfenyl bromide

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