tetra methyl 4,4′,4″,4′″-(copperporphyrin-5,10,15,20-tetrayl)tetrabenzoate

Base Information

• Chemical Name: tetra methyl 4,4′,4″,4′″-(copperporphyrin-5,10,15,20-tetrayl)tetrabenzoate
• CAS No.: 853568-53-3
• Molecular Formula: C₅₂H₃₆CuN₄O₈
• Molecular Weight: 908.426
• Mol file: 853568-53-3.mol

Synonyms:tetra methyl 4,4′,4″,4′″-(copperporphyrin-5,10,15,20-tetrayl)tetrabenzoate

Chemical Property of tetra methyl 4,4′,4″,4′″-(copperporphyrin-5,10,15,20-tetrayl)tetrabenzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tetra methyl 4,4′,4″,4′″-(copperporphyrin-5,10,15,20-tetrayl)tetrabenzoate

There total 5 articles about tetra methyl 4,4′,4″,4′″-(copperporphyrin-5,10,15,20-tetrayl)tetrabenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

copper(II) acetate monohydrate (6046-93-1) + 5,10,15,20-tetrakis(4-methoxycarbonylphenyl)porphyrin (22112-83-0) → tetra methyl 4,4′,4″,4′″-(copperporphyrin-5,10,15,20-tetrayl)tetrabenzoate (853568-53-3)

Guidance literature:

In methanol; chloroform; at 60 ℃; for 0.75h;

DOI:10.1016/j.molliq.2020.114668

Reference yield: 83.0%

pyrrole (109-97-7,30604-81-0) + methyl 4-formylbenzoate (1571-08-0) → tetra methyl 4,4′,4″,4′″-(copperporphyrin-5,10,15,20-tetrayl)tetrabenzoate (853568-53-3)

Guidance literature:

With 2,6-dimethylpyridine; silica gel; copper dichloride; at 180 ℃; for 0.133333h; Microwave irradiation;

DOI:10.3390/molecules15053731

Reference yield: 76.0%

methanol (67-56-1) + copper(II) choride dihydrate + 5,10,15,20-tetra(4-carboxyphenyl)porphyrin → tetra methyl 4,4′,4″,4′″-(copperporphyrin-5,10,15,20-tetrayl)tetrabenzoate (853568-53-3)

Guidance literature:

In ethanol; High Pressure; Cu salt, free base porphyrin (1:1) and EtOH heated in an autoclave at 453 K for 1 d; slowly cooled to room temp. (6K/h), elem. anal.;

DOI:10.1002/ejic.200900801

upstream raw materials:

methanol

pyrrole

methyl 4-formylbenzoate

5,10,15,20-tetrakis(4-methoxycarbonylphenyl)porphyrin