tetrakis(acetonitrile)copper(I) hexafluorophosphate

Base Information

• Chemical Name: tetrakis(acetonitrile)copper(I) hexafluorophosphate
• CAS No.: 99536-59-1
• Molecular Formula: C₈H₁₂CuN₄*F₆P
• Molecular Weight: 372.72

Synonyms:tetrakis(acetonitrile)copper(I) hexafluorophosphate

Chemical Property of tetrakis(acetonitrile)copper(I) hexafluorophosphate

Chemical Property:

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Technology Process of tetrakis(acetonitrile)copper(I) hexafluorophosphate

There total 6 articles about tetrakis(acetonitrile)copper(I) hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Cu(NCCH3)5(2+)*2PF6(1-)={Cu(NCCH3)5}{PF6}2 + dimethylsulfide (75-18-3) → (CH3)2SSCH3(1+)*PF6(1-)={(CH3)2SSCH3}{PF6} (124213-61-2) + tetrakis(acetonitrile)copper(I) hexafluorophosphate (99536-59-1) + ethane (74-84-0)

Guidance literature:

In acetonitrile; in Pyrex vacuum line or N2; mixt. of Cu-complex, SMe2 and MeCN slowly warmed from 77 K to room temp., deep green as SMe2 melted and flowed into the frozen soln., agitated (colorless soln.), monitored by UV; evapn. (183 K, ethane), evapn. (room temp.);

Reference yield:

Cu(NCCH3)5(2+)*2PF6(1-)={Cu(NCCH3)5}{PF6}2 + trimethylamine (75-50-3) → (CH3)3NN(CH3)2(1+)*PF6(1-)={(CH3)3NN(CH3)2}{PF6} (124213-62-3) + tetrakis(acetonitrile)copper(I) hexafluorophosphate (99536-59-1) + ethane (74-84-0)

Guidance literature:

In acetonitrile; in Pyrex vacuum line or N2; mixt. of Cu-complex, amine and MeCN slowly warmed from 77 K to room temp., deep green as NMe3 melted and flowed into the frozen soln., agitated (colorless soln.), monitored by UV; evapn. (183 K, ethane), evapn. (room temp.);

Reference yield:

tetrakis(actonitrile)copper(I) hexafluorophosphate (64443-05-6) + methyl isocyanate (593-75-9,685498-28-6) + 4,4'-diisocyanobiphenyl (952-28-3) + (cyclopentadienyl)(CO)(PPh3)Fe(CH3) + (C5H4N(CH2)2NCH3CH2)2C6H2(O)CH3(1-) + C6H3OH(CH2N(CH2CH2C5H4N)2)2 (117553-00-1) → tetrakis(acetonitrile)copper(I) hexafluorophosphate (99536-59-1) + dicarbonyl(cyclopentadienyl)methyliron(II) + Cu(1+)*2(CN)2C6H4*PF6(1-)={Cu((CN)2C6H4)2}{PF6}

Guidance literature:

In tetrahydrofuran; byproducts: CH3CN; (N2); solid Cu(NCCH3)4PF6 added to a cooled soln. of Cp2MoH2 (molar ratio 1:2); stirred for 1 h at low temp.; allowed to warm to room temp.; filtered; washed with THF; dried in vacuo;

DOI:10.1016/S0020-1693(00)92409-5

upstream raw materials:

tetrakis(actonitrile)copper(I) hexafluorophosphate

methyl isocyanate

4,4'-diisocyanobiphenyl

C₆H₃OH(CH₂N(CH₂CH₂C₅H₄N)2)2

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