2S-tert-butoxycarbonylamino-4-(4-hydroxyphenyl)butanoic acid benzyl ester

Base Information

Chemical Name:2S-tert-butoxycarbonylamino-4-(4-hydroxyphenyl)butanoic acid benzyl ester
CAS No.:296774-56-6
Molecular Formula:C₂₂H₂₇NO₅
Molecular Weight:385.46
Hs Code.:

Synonyms:2S-tert-butoxycarbonylamino-4-(4-hydroxyphenyl)butanoic acid benzyl ester

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Chemical Property of 2S-tert-butoxycarbonylamino-4-(4-hydroxyphenyl)butanoic acid benzyl ester

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Technology Process of 2S-tert-butoxycarbonylamino-4-(4-hydroxyphenyl)butanoic acid benzyl ester

There total 2 articles about 2S-tert-butoxycarbonylamino-4-(4-hydroxyphenyl)butanoic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 100-39-0
benzyl bromide

: 198473-94-8
Boc-hTyr

: 296774-56-6
2S-tert-butoxycarbonylamino-4-(4-hydroxyphenyl)butanoic acid benzyl ester

Guidance literature:: With CsCO₃; In N,N-dimethyl-formamide; at 25 ℃; for 16h;
DOI:10.1016/S0968-0896(00)00097-3

Reference yield:

: 540-38-5
p-Iodophenol

: 119768-48-8
(S)-2-((tert-butoxycarbonyl)amino)-4-iodobutyric acid benzyl ester

: 296774-56-6
2S-tert-butoxycarbonylamino-4-(4-hydroxyphenyl)butanoic acid benzyl ester

Guidance literature:: (S)-2-N-tert-butoxycarbonylamino-4-iodo-butanoic acid benzyl ester; With chloro-trimethyl-silane; zinc; In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h;

p-Iodophenol; With tris-(o-tolyl)phosphine; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In N,N-dimethyl-formamide; at 20 ℃; Further stages.;
DOI:10.1039/b311515a