30-benzyl-18β-glycyrrhizin

Base Information

• Chemical Name: 30-benzyl-18β-glycyrrhizin
• CAS No.: 87918-99-8
• Molecular Formula: C₄₉H₆₈O₁₆
• Molecular Weight: 913.069
• Mol file: 87918-99-8.mol

Synonyms:30-benzyl-18β-glycyrrhizin

Chemical Property of 30-benzyl-18β-glycyrrhizin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 30-benzyl-18β-glycyrrhizin

There total 3 articles about 30-benzyl-18β-glycyrrhizin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.5%

6',6'',30-tribenzyl-18β-glycyrrhizin (87918-95-4) → 30-benzyl-18β-glycyrrhizin (87918-99-8)

Guidance literature:

With potassium hydroxide; In methanol; for 4h; Ambient temperature;

Reference yield:

O-benzyl-N,N'-dicyclohexylisourea (6738-17-6) → 30-benzyl-18β-glycyrrhizin (87918-99-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 22.6 percent / CHCl₃; dimethylformamide / 72 h / Ambient temperature

2: 76.5 percent / 5percent potassium hydroxide / methanol / 4 h / Ambient temperature

With potassium hydroxide; In methanol; chloroform; N,N-dimethyl-formamide;

Reference yield:

glycyrrizhin (83896-44-0,103000-77-7,119479-05-9,142394-43-2,1405-86-3) → 30-benzyl-18β-glycyrrhizin (87918-99-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 22.6 percent / CHCl₃; dimethylformamide / 72 h / Ambient temperature

2: 76.5 percent / 5percent potassium hydroxide / methanol / 4 h / Ambient temperature

With potassium hydroxide; In methanol; chloroform; N,N-dimethyl-formamide;

upstream raw materials:

6',6'',30-tribenzyl-18β-glycyrrhizin

O-benzyl-N,N'-dicyclohexylisourea

glycyrrizhin

Downstream raw materials:

6',6''-di-tert-butyl-30-benzyl-18β-glycyrrhizin

hydroxysuccinimidyl N-(6',6''-di-tert-butyl-18β-glycyrrhizinyl)-trans-4-aminomethylcyclohexanecarboxylate

benzyl N-(6',6''-di-tert-butyl-18β-glycyrrhizinyl)-trans-4-aminomethylcyclohexanecarboxylate

benzyl N-(6',6''-di-tert-butyl-18β-glycyrrhizinyl)-ε-aminohexanoate