[(R)-1-(4-bromobenzyl)-2-(2,2,5-trimethyl-4,6-dioxo-[1,3]dioxan-5-yl)ethyl]carbamic acid t-butyl ester

Base Information

Chemical Name:[(R)-1-(4-bromobenzyl)-2-(2,2,5-trimethyl-4,6-dioxo-[1,3]dioxan-5-yl)ethyl]carbamic acid t-butyl ester
CAS No.:1562404-79-8
Molecular Formula:C₂₁H₂₈BrNO₆
Molecular Weight:470.36
Hs Code.:

Synonyms:[(R)-1-(4-bromobenzyl)-2-(2,2,5-trimethyl-4,6-dioxo-[1,3]dioxan-5-yl)ethyl]carbamic acid t-butyl ester

Suppliers and Price of [(R)-1-(4-bromobenzyl)-2-(2,2,5-trimethyl-4,6-dioxo-[1,3]dioxan-5-yl)ethyl]carbamic acid t-butyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [(R)-1-(4-bromobenzyl)-2-(2,2,5-trimethyl-4,6-dioxo-[1,3]dioxan-5-yl)ethyl]carbamic acid t-butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [(R)-1-(4-bromobenzyl)-2-(2,2,5-trimethyl-4,6-dioxo-[1,3]dioxan-5-yl)ethyl]carbamic acid t-butyl ester

There total 5 articles about [(R)-1-(4-bromobenzyl)-2-(2,2,5-trimethyl-4,6-dioxo-[1,3]dioxan-5-yl)ethyl]carbamic acid t-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1394050-15-7
[(S)-1-(4-bromobenzyl)-2-(2,2-dimethyl-4,6-dioxo-[1,3]dioxan-5-yl)ethyl]carbamic acid t-butyl ester

: 74-88-4
methyl iodide

: 1562404-79-8
[(R)-1-(4-bromobenzyl)-2-(2,2,5-trimethyl-4,6-dioxo-[1,3]dioxan-5-yl)ethyl]carbamic acid t-butyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 0 - 23 ℃;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1562404-79-8
[(R)-1-(4-bromobenzyl)-2-(2,2,5-trimethyl-4,6-dioxo-[1,3]dioxan-5-yl)ethyl]carbamic acid t-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide / water; acetonitrile / 0.5 h / 0 °C

1.2: 0 - 23 °C

2.1: dmap / dichloromethane / 0.5 h / 0 °C

2.2: -20 - 23 °C / Inert atmosphere

3.1: acetic acid / dichloromethane / 0.5 h / -5 °C / Inert atmosphere

3.2: 3.5 h / -5 - 23 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 0 - 23 °C

With dmap; potassium carbonate; acetic acid; sodium hydroxide; In dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1383027-95-9
C₂₀H₂₄BrNO₇

: 1562404-79-8
[(R)-1-(4-bromobenzyl)-2-(2,2,5-trimethyl-4,6-dioxo-[1,3]dioxan-5-yl)ethyl]carbamic acid t-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / dichloromethane / 0.5 h / -5 °C / Inert atmosphere

1.2: 3.5 h / -5 - 23 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 0 - 23 °C

With potassium carbonate; acetic acid; In dichloromethane; N,N-dimethyl-formamide;