4-NITROPHENANTHRENE

Base Information

• Chemical Name: 4-NITROPHENANTHRENE
• CAS No.: 82064-15-1
• Molecular Formula: C14H9NO2
• Molecular Weight: 223.22676
• Mol file: 82064-15-1.mol

Synonyms:4-Nitro-phenanthren,x-Nitro-phenanthren vom F:73-75grad;4-nitro-phenanthrene;Phenanthrene, 4-nitro-;4-Nitro-phenanthren;Phenanthrene,4-nitro;

Chemical Property of 4-NITROPHENANTHRENE

Chemical Property:

• Vapor Pressure: 1.16E-06mmHg at 25°C
• Boiling Point: 413.3°C at 760 mmHg
• Flash Point: 207.5°C
• PSA: 45.82000
• Density: 1.316g/cm³
• LogP: 4.42440

Purity/Quality:

4-NITROPHENANTHRENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-NITROPHENANTHRENE

There total 10 articles about 4-NITROPHENANTHRENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenanthrene (85-01-8) → 9-nitrophenanthrene (954-46-1) + 6-nitro-3,4-benzocoumarin (6623-66-1) + 4-Nitrophenanthrene (82064-15-1) + 1-nitrophenanthrene (17024-17-8)

Guidance literature:

With nitrate radical; at 22.85 ℃; under 740 Torr; Further Variations:; Reagents; Kinetics; gas phase;

DOI:10.1021/es00052a027

Reference yield:

phenanthrene (85-01-8) → 10-acetoxy-9,9',10,10'-tetrahydro-10'-nitro-9,9'-biphenanthrene (69618-73-1,127305-25-3) + 9-nitrophenanthrene (954-46-1) + 4-Nitrophenanthrene (82064-15-1) + 3-nitro-phenanthrene (17024-19-0) + 2-nitrophenanthrene (17024-18-9) + 1-nitrophenanthrene (17024-17-8)

Guidance literature:

With acetic anhydride; copper(II) nitrate; at 22 - 41 ℃; for 1h; Product distribution; other nitrating agents, other times;

Reference yield:

phenanthrene (85-01-8) + nitric acid (7697-37-2,78989-43-2) + acetic anhydride (108-24-7) + acetic acid (64-19-7,77671-22-8) → 9-nitrophenanthrene (954-46-1) + 4-Nitrophenanthrene (82064-15-1) + 3-nitro-phenanthrene (17024-19-0) + 2-nitrophenanthrene (17024-18-9)

Guidance literature:

upstream raw materials:

phenanthrene

nitric acid

acetic anhydride

acetic acid

Downstream raw materials:

4-nitrophenanthrene-9,10-dione

4-phenanthrenamine

1-aminophenanthrene

Refernces

• 1、 Kwok,Harger,Arey,Atkinson. "Reactions of gas-phase phenanthrene under simulated atmospheric conditions". . p. 521 - 527. Retrieved 2007/10/03.