N-tert-Butylpivalamide

Base Information

Chemical Name:N-tert-Butylpivalamide
CAS No.:686-96-4
Molecular Formula:C9H19NO
Molecular Weight:157.256
Hs Code.:2924199090
NSC Number:172142
DSSTox Substance ID:DTXSID10305851
Nikkaji Number:J119.392I
Wikidata:Q82052617
Mol file:686-96-4.mol

Synonyms:N-tert-Butylpivalamide;686-96-4;N-tert-Butyl-2,2-dimethylpropionamide;Propionamide, N-tert-butyl-2,2-dimethyl-;N-tert-Butylpivalic acid amide;Propanamide, N-(1,1-dimethylethyl)-2,2-dimethyl-;NSC172142;pivaloyl t-butylamine;SCHEMBL153717;SCHEMBL13657953;DTXSID10305851;AKOS003849982;NSC-172142;Propanamide, N-tert-butyl-2,2-dimethyl;N-(tert-Butyl)-2,2-dimethylpropanamide #;Propanamide,1-dimethylethyl)-2,2-dimethyl-;N-TERT-BUTYL-2,2-DIMETHYL-PROPIONAMIDE

Suppliers and Price of N-tert-Butylpivalamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 9 raw suppliers

Chemical Property of N-tert-Butylpivalamide

Chemical Property:

Vapor Pressure:0.112mmHg at 25°C
Melting Point:117-118 °C
Boiling Point:220.7°C at 760 mmHg
PKA:16.60±0.46(Predicted)
Flash Point:122°C
PSA：29.10000
Density:0.858g/cm³
LogP:2.33810
XLogP3:1.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:157.146664230
Heavy Atom Count:11
Complexity:148

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C)C(=O)NC(C)(C)C

Technology Process of N-tert-Butylpivalamide

There total 2 articles about N-tert-Butylpivalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 507-19-7
t-butyl bromide

: 56741-04-9
S-phenyl tert-butylcarbamothioate

: 686-96-4
N-tert-butyltrimethylacetamide

: 882-33-7
diphenyldisulfane

Guidance literature:: t-butyl bromide; With iodine; magnesium; In 2-methyltetrahydrofuran; at 60 ℃; for 1h; Schlenk technique; Inert atmosphere;

S-phenyl tert-butylcarbamothioate; In 2-methyltetrahydrofuran; at 0 - 20 ℃; for 2h; Inert atmosphere; Schlenk technique;

With ammonium hydroxide; oxygen; In 2-methyltetrahydrofuran; water; for 18h; under 760.051 Torr;
DOI:10.1021/acs.orglett.8b01654

Reference yield:

: 4195-17-9
4-nitrophenyl pivalate

: 75-64-9
tert-butylamine

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 686-96-4
N-tert-butyltrimethylacetamide

Guidance literature:: In acetonitrile; at 25.4 ℃; Rate constant;
DOI:10.1021/ja00347a036

Reference yield: 77.0%

: 636-98-6
p-nitrobenzene iodide

: 686-96-4
N-tert-butyltrimethylacetamide

: N-(tert-butyl)-2,2-dimethyl-3-(4-nitrophenyl)propanamide

Guidance literature:: p-nitrobenzene iodide; N-tert-butyltrimethylacetamide; With palladium diacetate; silver trifluoroacetate; In 2,2,2-trifluoroethanol; at 120 ℃; for 16h; Sealed tube;

p-nitrobenzene iodide; With silver trifluoroacetate; In 2,2,2-trifluoroethanol; at 120 ℃; for 16h;

p-nitrobenzene iodide; With silver trifluoroacetate; In 2,2,2-trifluoroethanol; at 120 ℃; for 16h;
DOI:10.1021/acs.organomet.8b00325