dispirodithietane-4',2''-adamantane>

Base Information

• Chemical Name: dispirodithietane-4',2''-adamantane>
• CAS No.: 31023-85-5
• Molecular Formula: C₂₀H₂₈S₂
• Molecular Weight: 332.574

Synonyms:dispirodithietane-4',2''-adamantane>

Chemical Property of dispirodithietane-4',2''-adamantane>

Chemical Property:

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Technology Process of dispirodithietane-4',2''-adamantane>

There total 11 articles about dispirodithietane-4',2''-adamantane> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

hexamesitylcyclotrigermane (107824-84-0) + adamantane-2-thione (23695-65-0) → dispirodithietane-4',2''-adamantane> (31023-85-5) + 3-(2-adamantyl)-2,2-dimesityl-1,2-thiagermirane (107824-85-1) + C10H14S(Ge(C6H2(CH3)3)2)2 (117308-60-8)

Guidance literature:

In cyclohexane; Irradiation (UV/VIS); photolysis at room temp.; 2.5h; concd.; sepn. by preparative HPLC; elem. anal.;

DOI:10.1021/om00103a020

Reference yield: 39.0%

3-(2-adamantyl)-2,2-dimesityl-1,2-thiagermirane (107824-85-1) + 2,3-dimethyl-buta-1,3-diene (513-81-5) → dispirodithietane-4',2''-adamantane> (31023-85-5) + 1,1-bis(2,4,6-trimethylphenyl)-3,4-dimethylgermacyclopent-3-ene (83686-73-1)

Guidance literature:

In cyclohexane; Irradiation (UV/VIS); under Ar; photolysis at room temp.; 5h; sepn. by preparative HPLC;

DOI:10.1021/om00103a020

Reference yield: 29.1%

adamantane-2-thione (23695-65-0) → 2-Adamantanone (700-58-3) + dispirodithietane-4',2''-adamantane> (31023-85-5) + C14H20OS (93490-38-1)

Guidance literature:

With trans-Crotonaldehyde; hydroquinone; In toluene; at 140 ℃; for 14h;

DOI:10.1039/P19840001869

upstream raw materials:

3-Methyl-3-buten-2-one

adamantane-2-thione

2-methylpropenal

methyl vinyl ketone

Downstream raw materials:

2-Adamantanone

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