(S)-2-(benzyloxy)-2-(3-((benzyloxy)methyl)-2-methoxypyridin-4-yl)butanal

Base Information

Chemical Name:(S)-2-(benzyloxy)-2-(3-((benzyloxy)methyl)-2-methoxypyridin-4-yl)butanal
CAS No.:1201830-88-7
Molecular Formula:C₂₅H₂₇NO₄
Molecular Weight:405.494
Hs Code.:

Synonyms:(S)-2-(benzyloxy)-2-(3-((benzyloxy)methyl)-2-methoxypyridin-4-yl)butanal

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Chemical Property of (S)-2-(benzyloxy)-2-(3-((benzyloxy)methyl)-2-methoxypyridin-4-yl)butanal

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Technology Process of (S)-2-(benzyloxy)-2-(3-((benzyloxy)methyl)-2-methoxypyridin-4-yl)butanal

There total 5 articles about (S)-2-(benzyloxy)-2-(3-((benzyloxy)methyl)-2-methoxypyridin-4-yl)butanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1353579-45-9
(2R,3S)-3-(benzyloxy)-3-(3-((benzyloxy)methyl)-2-methoxypyridin-4-yl)pentane-1,2-diol

: 1201830-88-7
(S)-2-(benzyloxy)-2-(3-((benzyloxy)methyl)-2-methoxypyridin-4-yl)butanal

Guidance literature:: With sodium periodate; In water; acetonitrile; at 20 ℃; for 2h;
DOI:10.1021/jo201974f

Reference yield:

: 1353579-41-5
(S)-1-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-1-(3-(hydroxymethyl)-2-methoxypyridin-4-yl)propan-1-ol

: 1201830-88-7
(S)-2-(benzyloxy)-2-(3-((benzyloxy)methyl)-2-methoxypyridin-4-yl)butanal

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

1.2: 4 h / 70 °C / Inert atmosphere

2.1: hydrogenchloride; water / methanol / 2 h / 20 °C

3.1: sodium periodate / water; acetonitrile / 2 h / 20 °C

With hydrogenchloride; sodium periodate; water; sodium hydride; In tetrahydrofuran; methanol; water; acetonitrile;
DOI:10.1021/jo201974f

Reference yield:

: 1353579-43-7
4-((S)-1-(benzyloxy)-1-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-propyl)-3-((benzyloxy)methyl)-2-methoxypyridine

: 1201830-88-7
(S)-2-(benzyloxy)-2-(3-((benzyloxy)methyl)-2-methoxypyridin-4-yl)butanal

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; water / methanol / 2 h / 20 °C

2: sodium periodate / water; acetonitrile / 2 h / 20 °C

With hydrogenchloride; sodium periodate; water; In methanol; water; acetonitrile;
DOI:10.1021/jo201974f