2',4'-Dichlorobutyrophenone

Base Information

Chemical Name:2',4'-Dichlorobutyrophenone
CAS No.:66353-47-7
Molecular Formula:C10H10Cl2O
Molecular Weight:217.095
Hs Code.:2914700090
DSSTox Substance ID:DTXSID10524848
Nikkaji Number:J2.229.885B
Wikidata:Q72465837
Mol file:66353-47-7.mol

Synonyms:66353-47-7;2',4'-Dichlorobutyrophenone;1-(2,4-dichlorophenyl)butan-1-one;MFCD09028060;2,4-Dichlorophenyl Propyl Ketone;1-Butanone, 1-(2,4-dichlorophenyl)-;2,4-Dichloro butyrophenone;2`,4`-Dichlorobutyrophenone;SCHEMBL2125979;DTXSID10524848;AKOS010522895;AC-8764;AS-31021;SY015391;AM20040981;CS-0224136;D3468;EN300-117961;Z802544640;2 inverted exclamation mark pound not4 inverted exclamation mark -Dichlorobutyrophenone;2 inverted exclamation mark ,4 inverted exclamation mark -Dichlorobutyrophenone

Suppliers and Price of 2',4'-Dichlorobutyrophenone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TCI Chemical
2',4'-Dichlorobutyrophenone >96.0%(GC)
25g
$ 29.00

Crysdot
1-(2,4-Dichlorophenyl)butan-1-one 97%
1000g
$ 461.00

American Custom Chemicals Corporation
2',4'-DICHLOROBUTYROPHENONE 95.00%
10G
$ 1334.03

American Custom Chemicals Corporation
2',4'-DICHLOROBUTYROPHENONE 95.00%
5G
$ 909.56

Alichem
1-(2,4-Dichlorophenyl)butan-1-one
1000g
$ 479.44

Alichem
1-(2,4-Dichlorophenyl)butan-1-one
100g
$ 318.50

AK Scientific
2,4-Dichlorobutyrophenone
25g
$ 101.00

AHH
2,4-Dichlorobutyrophenone 96%
500g
$ 325.00

Total 79 raw suppliers

Chemical Property of 2',4'-Dichlorobutyrophenone

Chemical Property:

Vapor Pressure:0.004mmHg at 25°C
Refractive Index:1.535
Boiling Point:280.687 °C at 760 mmHg
Flash Point:116.849 °C
PSA：17.07000
Density:1.22 g/cm³
LogP:3.97620
XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:216.0108703
Heavy Atom Count:13
Complexity:182

Purity/Quality:

99% ^*data from raw suppliers

2',4'-Dichlorobutyrophenone >96.0%(GC) ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC(=O)C1=C(C=C(C=C1)Cl)Cl

Technology Process of 2',4'-Dichlorobutyrophenone

There total 5 articles about 2',4'-Dichlorobutyrophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 53066-18-5
1-(2,4-dichlorophenyl)butan-1-ol

: 66353-47-7
1-(2,4-dichlorophenyl)butan-1-one

Guidance literature:: With chromium(VI) oxide; sulfuric acid; In acetone; at 0 ℃; for 0.5h;
DOI:10.1021/jm020980t

Reference yield:

: 2234-82-4
1-propylmagnesium chloride

: 7681-65-4
copper(I) iodide

: 89-75-8
2,4-dichlorobenzoyl chloride

: 66353-47-7
1-(2,4-dichlorophenyl)butan-1-one

Guidance literature:: In tetrahydrofuran; water;

Reference yield:

: 874-42-0
2,4-dichlorobenzaldeyhde

: 66353-47-7
1-(2,4-dichlorophenyl)butan-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / diethyl ether / 24 h / 20 °C

2: 90 percent / aq. H₂SO₄; CrO₃ / acetone / 0.5 h / 0 °C

With chromium(VI) oxide; sulfuric acid; In diethyl ether; acetone; 2: Jones oxidation;
DOI:10.1021/jm020980t