N-[4-(4-fluoro-benzoylamino)-phenyl]-hydrazinecarboxylic acid tert-butyl ester

Base Information

Chemical Name:N-[4-(4-fluoro-benzoylamino)-phenyl]-hydrazinecarboxylic acid tert-butyl ester
CAS No.:862158-40-5
Molecular Formula:C₁₈H₂₀FN₃O₃
Molecular Weight:345.374
Hs Code.:

Synonyms:N-[4-(4-fluoro-benzoylamino)-phenyl]-hydrazinecarboxylic acid tert-butyl ester

Suppliers and Price of N-[4-(4-fluoro-benzoylamino)-phenyl]-hydrazinecarboxylic acid tert-butyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-[4-(4-fluoro-benzoylamino)-phenyl]-hydrazinecarboxylic acid tert-butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-[4-(4-fluoro-benzoylamino)-phenyl]-hydrazinecarboxylic acid tert-butyl ester

There total 2 articles about N-[4-(4-fluoro-benzoylamino)-phenyl]-hydrazinecarboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 403-43-0
4-fluorobenzoyl chloride

: 862158-40-5
N-[4-(4-fluoro-benzoylamino)-phenyl]-hydrazinecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / DMAP; NEt₃ / tetrahydrofuran / 1 h / 20 °C

2: 78 percent / CuI; 1,10-phenanthroline; Cs₂CO₃ / dimethylformamide / 68 h / 80 °C

With dmap; copper(l) iodide; 1,10-Phenanthroline; caesium carbonate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo050464l

Reference yield:

: 540-37-4
p-aminoiodobenzene

: 862158-40-5
N-[4-(4-fluoro-benzoylamino)-phenyl]-hydrazinecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / DMAP; NEt₃ / tetrahydrofuran / 1 h / 20 °C

2: 78 percent / CuI; 1,10-phenanthroline; Cs₂CO₃ / dimethylformamide / 68 h / 80 °C

With dmap; copper(l) iodide; 1,10-Phenanthroline; caesium carbonate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo050464l