<(bis-methoxymethylenoxy-2',3' phenyl)-1 epoxy-2,3β cyclohexyl-1>-2 N,N-dimethylacetamide

Base Information

Chemical Name:<(bis-methoxymethylenoxy-2',3' phenyl)-1 epoxy-2,3β cyclohexyl-1>-2 N,N-dimethylacetamide
CAS No.:117570-01-1
Molecular Formula:C₂₀H₂₉NO₆
Molecular Weight:379.453
Hs Code.:

Synonyms:<(bis-methoxymethylenoxy-2',3' phenyl)-1 epoxy-2,3β cyclohexyl-1>-2 N,N-dimethylacetamide

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Chemical Property of <(bis-methoxymethylenoxy-2',3' phenyl)-1 epoxy-2,3β cyclohexyl-1>-2 N,N-dimethylacetamide

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Technology Process of <(bis-methoxymethylenoxy-2',3' phenyl)-1 epoxy-2,3β cyclohexyl-1>-2 N,N-dimethylacetamide

There total 7 articles about <(bis-methoxymethylenoxy-2',3' phenyl)-1 epoxy-2,3β cyclohexyl-1>-2 N,N-dimethylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 117569-99-0
(bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 N,N-dimethylacetamide

: 117570-01-1
<(bis-methoxymethylenoxy-2',3' phenyl)-1 epoxy-2,3β cyclohexyl-1>-2 N,N-dimethylacetamide

Guidance literature:: With dihydrogen peroxide; potassium hydrogencarbonate; trichloroacetonitrile; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1016/S0040-4020(01)85896-8

Reference yield:

: 930-68-7
cyclohexenone

: 117570-01-1
<(bis-methoxymethylenoxy-2',3' phenyl)-1 epoxy-2,3β cyclohexyl-1>-2 N,N-dimethylacetamide

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) n-butyllithium / 1.) THF, r.t., 2 h; 2.) THF, 48 h, 20 deg C

2: 93 percent / PCC / CH₂Cl₂ / 2 h / Ambient temperature

3: 100 percent / LiAlH₄ / tetrahydrofuran / 2 h / 20 °C

4: 73 percent / xylene / 6 h / Heating

5: 80 percent / trichloroacetonitrile, KHCO₃, 30 percent H₂O₂ / CH₂Cl₂ / 24 h / Ambient temperature

With lithium aluminium tetrahydride; n-butyllithium; dihydrogen peroxide; potassium hydrogencarbonate; trichloroacetonitrile; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; xylene;
DOI:10.1016/S0040-4020(01)85896-8

Reference yield:

: 3688-89-9
bis-methoxymethylenoxy-1,2 benzene

: 117570-01-1
<(bis-methoxymethylenoxy-2',3' phenyl)-1 epoxy-2,3β cyclohexyl-1>-2 N,N-dimethylacetamide

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) n-butyllithium / 1.) THF, r.t., 2 h; 2.) THF, 48 h, 20 deg C

2: 93 percent / PCC / CH₂Cl₂ / 2 h / Ambient temperature

3: 100 percent / LiAlH₄ / tetrahydrofuran / 2 h / 20 °C

4: 73 percent / xylene / 6 h / Heating

5: 80 percent / trichloroacetonitrile, KHCO₃, 30 percent H₂O₂ / CH₂Cl₂ / 24 h / Ambient temperature

With lithium aluminium tetrahydride; n-butyllithium; dihydrogen peroxide; potassium hydrogencarbonate; trichloroacetonitrile; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; xylene;
DOI:10.1016/S0040-4020(01)85896-8