N′-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}propionohydrazide

Base Information

Chemical Name:N′-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}propionohydrazide
CAS No.:1237587-30-2
Molecular Formula:C₁₉H₁₅Cl₃F₃N₃O₂
Molecular Weight:480.701
Hs Code.:

Synonyms:N′-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}propionohydrazide

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Chemical Property of N′-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}propionohydrazide

Chemical Property:

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Technology Process of N′-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}propionohydrazide

There total 6 articles about N′-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}propionohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1237587-85-7
5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenylhydrazine

: 79-03-8
propionyl chloride

: 1237587-30-2
N′-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}propionohydrazide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃;

Reference yield:

: 864725-22-4
1,3-dichloro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene

: 1237587-30-2
N′-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}propionohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 60 °C

1.2: 6 h

2.1: acetic acid; iron / ethanol; water / 0.83 h / 75 °C

3.1: hydrogenchloride / 1,4-dioxane; water / 0.33 h / 20 °C

3.2: 0.25 h / 0 °C

4.1: triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C

With hydrogenchloride; N-chloro-succinimide; iron; acetic acid; triethylamine; In tetrahydrofuran; 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 1071928-04-5
5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chloronitrobenzene

: 1237587-30-2
N′-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}propionohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid; iron / ethanol; water / 0.83 h / 75 °C

2.1: hydrogenchloride / 1,4-dioxane; water / 0.33 h / 20 °C

2.2: 0.25 h / 0 °C

3.1: triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C

With hydrogenchloride; iron; acetic acid; triethylamine; In tetrahydrofuran; 1,4-dioxane; ethanol; water;