diphenylstibane

Base Information

• Chemical Name: diphenylstibane
• CAS No.: 5865-81-6
• Molecular Formula: C₁₂H₁₁Sb
• Molecular Weight: 276.969
• Mol file: 5865-81-6.mol

Synonyms:diphenylstibane

Chemical Property of diphenylstibane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of diphenylstibane

There total 8 articles about diphenylstibane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

triphenylantimony (603-36-1) + potassium (7440-09-7) → diphenylstibane (5865-81-6)

Guidance literature:

In ammonia; acetone; byproducts: C6H6;

DOI:10.1021/ja00808a018

Reference yield: 70.0%

diphenyl(trimethylsilyl)stibine (69561-88-2) → Trimethylmethoxysilane (1825-61-2) + diphenylstibane (5865-81-6)

Guidance literature:

With methanol; In benzene; To methanol is added stibane compound in benzene under Ar and the soln. is stirred at 25°C for 2 h.; removal of volatiles under vac.;

Reference yield: 65.0%

diphenylantimony(III) chloride (2629-47-2) → diphenylstibane (5865-81-6)

Guidance literature:

With lithium borohydride; In diethyl ether; byproducts: LiCl, B2H6; at -60°C, in a high-vac. system;

upstream raw materials:

triphenylantimony

potassium

diphenylantimony(III) chloride

diphenylantimony trichloride

Downstream raw materials:

tetraphenyldistibane

diphenylantimony(III) chloride

(C₆H₅)2Sb(O)OH

diphenyliodostibine