Hexadecanoic acid, (1S)-1-bis(1-methylethyl)amino(phenylmethoxy)phosphinooxymethyl-1,2-ethanediyl ester

Base Information

• Chemical Name: Hexadecanoic acid, (1S)-1-bis(1-methylethyl)amino(phenylmethoxy)phosphinooxymethyl-1,2-ethanediyl ester
• CAS No.: 196304-47-9
• Molecular Formula: C₄₈H₈₈NO₆P
• Molecular Weight: 806.204

Synonyms:Hexadecanoic acid, (1S)-1-bis(1-methylethyl)amino(phenylmethoxy)phosphinooxymethyl-1,2-ethanediyl ester

Chemical Property of Hexadecanoic acid, (1S)-1-bis(1-methylethyl)amino(phenylmethoxy)phosphinooxymethyl-1,2-ethanediyl ester

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

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Technology Process of Hexadecanoic acid, (1S)-1-bis(1-methylethyl)amino(phenylmethoxy)phosphinooxymethyl-1,2-ethanediyl ester

There total 15 articles about Hexadecanoic acid, (1S)-1-bis(1-methylethyl)amino(phenylmethoxy)phosphinooxymethyl-1,2-ethanediyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

1,2-dipalmitoyl-sn-glycerol (30334-71-5) + benzyl-N,N,N',N'-tetraisopropylphosphorodiamidite (108549-21-9) → (+)-benzyloxy(N,N-diisopropylamino)(1,2-di-O-hexadecanoyl-sn-glycer-3-yl)phosphine (120595-85-9,196304-47-9)

Guidance literature:

With 1H-tetrazole; In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1039/b909306k

Reference yield: 92.0%

1,2-di-O-palmitoyl-sn-glycerol (6076-30-8) + benzyl-N,N,N',N'-tetraisopropylphosphorodiamidite (108549-21-9) → 1,2-di-O-hexadacanoyl-sn-glycerobenzyl (N,N-diisopropylamino)phopshoramidite (120595-85-9,196304-47-9)

Guidance literature:

With 1H-tetrazole; In dichloromethane; acetonitrile; at 20 ℃; for 0.5h;

DOI:10.1016/S0040-4039(00)82387-4

Reference yield: 90.0%

1,2-di-O-palmitoyl-sn-glycerol (6076-30-8) + (benzyloxy)chloro(diisopropylamino)phosphane (128753-68-4) → 1,2-di-O-hexadacanoyl-sn-glycerobenzyl (N,N-diisopropylamino)phopshoramidite (120595-85-9,196304-47-9)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 2h;

DOI:10.1021/jo980501r

upstream raw materials:

1,2-di-O-palmitoyl-sn-glycerol

benzyl-N,N,N',N'-tetraisopropylphosphorodiamidite

(benzyloxy)chloro(diisopropylamino)phosphane

bis(diisopropylamino)chlorophosphine

Downstream raw materials:

3,4,5,6-tetra-O-benzyl-2-O-(2',3',4',6'-tetra-O-benzyl-α-D-mannopyranosyl)-1-O-(1,2-di-O-palmitoyl-sn-glycero)-D-myo-inositol benzylphosphate

1D-2,4,6-tri-O-benzyl-1-<1',2'-di-O-hexadecanoyl-sn-glycero(3')benzylphsophonato>-myo-inositol 3,5-bis(dibenzyl phosphate)

dipalmitoyl PtdIns₄P

C₁₀₄H₁₃₆O₂₂P₄

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