bis(para-tolyl)antimony acetate

Base Information

• Chemical Name: bis(para-tolyl)antimony acetate
• CAS No.: 109533-99-5
• Molecular Formula: C₁₆H₁₇O₂Sb
• Molecular Weight: 363.06

Synonyms:bis(para-tolyl)antimony acetate

Chemical Property of bis(para-tolyl)antimony acetate

Chemical Property:

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Technology Process of bis(para-tolyl)antimony acetate

There total 5 articles about bis(para-tolyl)antimony acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

antimony (7440-36-0) + (4-CH3C6H4)2ICl + antimony(III) chloride (10025-91-9) → bis(para-tolyl)antimony acetate (109533-99-5) + di(p-tolyl)antimony(V) trichloride (71512-07-7) + tri-p-tolylantimony dichloride (26508-67-8)

Guidance literature:

In acetone; mole ratio of (4-CH3C6H4)2ICl : SbCl3 : Sb 2:1:3, boiling in acetone for 3 h;

DOI:10.1021/ja01330a056

Reference yield: 20.0%

{4-CH3C6H4NN}SbCl4 + ethyl acetate (141-78-6) → bis(para-tolyl)antimony acetate (109533-99-5) + tri-p-tolylantimony dichloride (26508-67-8) + p-tolylstibine oxide

Guidance literature:

With zinc; In acetone; mole ratio of (CH3-4-C6H4NN)SbCl4 and Zn dust 1:1.5, at 65-70°C;

Reference yield: 18.0%

{4-CH3C6H4NN}SbCl4 → bis(para-tolyl)antimony acetate (109533-99-5) + tri-p-tolylantimony dichloride (26508-67-8) + p-tolylstibine oxide

Guidance literature:

With zinc; In acetone; refluxing;

upstream raw materials:

bis(di-p-tolylantimony)oxide

acetic acid

antimony

antimony(III) chloride

Downstream raw materials:

(4-CH₃C₆H₄)2SbI

tetra-p-tolyldistibane

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