1-(2-fluorophenyl)-4,4-dimethoxypiperidine

Base Information

Chemical Name:1-(2-fluorophenyl)-4,4-dimethoxypiperidine
CAS No.:115012-48-1
Molecular Formula:C₁₃H₁₈FNO₂
Molecular Weight:239.29
Hs Code.:
Mol file:115012-48-1.mol

Synonyms:1-(2-fluorophenyl)-4,4-dimethoxypiperidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2-fluorophenyl)-4,4-dimethoxypiperidine

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Technology Process of 1-(2-fluorophenyl)-4,4-dimethoxypiperidine

There total 3 articles about 1-(2-fluorophenyl)-4,4-dimethoxypiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 115012-46-9
1-(2-fluorophenyl)piperidin-4-one

: 149-73-5
trimethyl orthoformate

: 115012-48-1
1-(2-fluorophenyl)-4,4-dimethoxypiperidine

Guidance literature:: toluene-4-sulfonic acid; In methanol; for 0.166667h; Heating;

Reference yield:

: 119836-08-7
1-(2-fluorophenyl)piperidin-4-ol

: 115012-48-1
1-(2-fluorophenyl)-4,4-dimethoxypiperidine

Guidance literature:: Multi-step reaction with 2 steps

1: 67.5 percent / DCC, DMSO, pyridine, TFA / benzene / 1) 0 deg C 2) RT, 24 h

2: 75 percent / toluene-4-sulphonic acid / methanol / 0.17 h / Heating

With pyridine; dimethyl sulfoxide; dicyclohexyl-carbodiimide; trifluoroacetic acid; toluene-4-sulfonic acid; In methanol; benzene;