trimethylsilyl ether of (1S,2S)-N-trifluoroacetamidonorpseudoephedrine

Base Information

Chemical Name:trimethylsilyl ether of (1S,2S)-N-trifluoroacetamidonorpseudoephedrine
CAS No.:183378-05-4
Molecular Formula:C₁₄H₂₀F₃NO₂Si
Molecular Weight:319.399
Hs Code.:

Synonyms:trimethylsilyl ether of (1S,2S)-N-trifluoroacetamidonorpseudoephedrine

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Chemical Property of trimethylsilyl ether of (1S,2S)-N-trifluoroacetamidonorpseudoephedrine

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Technology Process of trimethylsilyl ether of (1S,2S)-N-trifluoroacetamidonorpseudoephedrine

There total 2 articles about trimethylsilyl ether of (1S,2S)-N-trifluoroacetamidonorpseudoephedrine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2153-98-2
(-)-Norpseudoephedrine hydrochloride

: 183378-05-4
trimethylsilyl ether of (1S,2S)-N-trifluoroacetamidonorpseudoephedrine

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / methanol / 18 h / Ambient temperature

2: Et₃N / CH₂Cl₂ / 4 h / Ambient temperature

With triethylamine; In methanol; dichloromethane;

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 2,2,2-Trifluoro-N-((1S,2S)-2-hydroxy-1-methyl-2-phenyl-ethyl)-acetamide

: 183378-05-4
trimethylsilyl ether of (1S,2S)-N-trifluoroacetamidonorpseudoephedrine

Guidance literature:: With triethylamine; In dichloromethane; for 4h; Yield given; Ambient temperature;

Reference yield: 98.0%

: 97250-25-4
tert-Butyldiphenylsilyl β-hydroxybutanone

: 183378-05-4
trimethylsilyl ether of (1S,2S)-N-trifluoroacetamidonorpseudoephedrine

: 762-72-1
allyl-trimethyl-silane

: 214959-70-3
(3S,1'S,2'S)-1-tert-Butyldiphenylsiloxy-3-methyl-3-(1'-phenyl-2'-trifluoroacetamido-1'-propoxy)hex-5-en

Guidance literature:: With trifluorormethanesulfonic acid; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 ℃; for 5h;
DOI:10.1002/(SICI)1521-3765(19980904)4:9<1862::AID-CHEM1862>3.0.CO;2-C