NiPh(Cl)(1,2-bis(diphenylphosphino)ethane)

Base Information

Chemical Name:NiPh(Cl)(1,2-bis(diphenylphosphino)ethane)
CAS No.:88544-62-1
Molecular Formula:C₃₂H₂₉ClNiP₂
Molecular Weight:569.673
Hs Code.:

Synonyms:NiPh(Cl)(1,2-bis(diphenylphosphino)ethane)

Suppliers and Price of NiPh(Cl)(1,2-bis(diphenylphosphino)ethane)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of NiPh(Cl)(1,2-bis(diphenylphosphino)ethane)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of NiPh(Cl)(1,2-bis(diphenylphosphino)ethane)

There total 3 articles about NiPh(Cl)(1,2-bis(diphenylphosphino)ethane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 31387-22-1
dimethylnickel{1,2-bis(diphenylphosphino)ethane}

: 98-88-4
benzoyl chloride

: 34557-54-5,27936-85-2
methane

: 74-84-0
ethane

: 88544-62-1
NiPh(Cl)(1,2-bis(diphenylphosphino)ethane)

: 98-86-2
acetophenone

: 67-64-1
acetone

Guidance literature:: In toluene; toluene and PhCOCl added to Ni complex at -196°C, after evacuation stirred at room temp. for 1 d; ppt. collected by filtration, crystd. from THF-Et2O; GLC anal.;
DOI:10.1246/bcsj.56.2147

Reference yield: 55.0%

: 31387-22-1
dimethylnickel{1,2-bis(diphenylphosphino)ethane}

: 14647-23-5
1,2-bis(diphenylphosphino)ethane nickel(II) chloride

: 74-84-0
ethane

: 88544-62-1
NiPh(Cl)(1,2-bis(diphenylphosphino)ethane)

: 88544-61-0
NiCl(Me)(1,2-bis(diphenylphosphino)ethane)

: 108-88-3,15644-74-3,16713-13-6
toluene

Guidance literature:: With chlorobenzene; In neat (no solvent); mixt. of educt and PhCl stirred at room temp. for 5 d; hexane added, ppt. dissolved in THF, solid recovered by addn. of hexane; GLC, NMR anal.;
DOI:10.1246/bcsj.56.2147