rccc-2,8,14,20-tetrakis-(iso-butyl)-phosphonito cavitant

Base Information

Chemical Name:rccc-2,8,14,20-tetrakis-(iso-butyl)-phosphonito cavitant
CAS No.:635753-30-9
Molecular Formula:C₆₈H₆₈O₈P₄
Molecular Weight:1137.18
Hs Code.:

Synonyms:rccc-2,8,14,20-tetrakis-(iso-butyl)-phosphonito cavitant

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Chemical Property of rccc-2,8,14,20-tetrakis-(iso-butyl)-phosphonito cavitant

Chemical Property:

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Technology Process of rccc-2,8,14,20-tetrakis-(iso-butyl)-phosphonito cavitant

There total 1 articles about rccc-2,8,14,20-tetrakis-(iso-butyl)-phosphonito cavitant which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118600-20-7,134731-86-5
rccc-2,8,14,20-tetrakis-(iso-butyl)-resorcin[4]arene

: 644-97-3
Dichlorophenylphosphine

: 635753-30-9
rccc-2,8,14,20-tetrakis-(iso-butyl)-phosphonito cavitant

Guidance literature:: With pyridine; at 80 ℃; for 4h; Inert atmosphere;
DOI:10.1080/24701556.2020.1749073

Reference yield: 94.0%

: 110-86-1
pyridine

: 67-56-1
methanol

: 635753-30-9
rccc-2,8,14,20-tetrakis-(iso-butyl)-phosphonito cavitant

: 7732-18-5
water

: silver(I) chloride

: [C₅H₅NH]⁽¹⁺⁾*[(C₄₄H₄₈O₈P₄(C₆H₅)4)Ag₄(Cl)4(Cl)]^(1-)*2CH₃CN*CH₃OH*H₂O=C₇₃H₇₄NO₈P₄Cl₅Ag₄*2CH₃CN*CH₃OH*H₂O

Guidance literature:: In dichloromethane; mixt. of AgCl, P compd. and pyridine in CH2Cl2 was stirred at room temp.overnight; filtered; solvent pumped off; recrystd. (CH2Cl2/CH3OH); elem. anal.;
DOI:10.1016/j.molstruc.2003.08.015

Reference yield: 91.0%

: 110-86-1
pyridine

: 75-09-2
dichloromethane

: 635753-30-9
rccc-2,8,14,20-tetrakis-(iso-butyl)-phosphonito cavitant

: 75-05-8,26809-02-9
acetonitrile

: copper(l) chloride

: 855304-15-3
[pyridinium][(rccc-2,8,14,20-tetrakis-(iso-butyl)-phosphonito cavitant)Cu4(mu-Cl)4(μ4-Cl)]*CH3CN*CH2Cl2

Guidance literature:: In dichloromethane; under N2 atm. using Schlenk techniques; mixt. of excess CuCl, phosphonitocavitand, pyridine in CH2Cl2 was stirred at room temp. overnight; soln. filtered; solvent was pumped off; residue recrystd. (CH2Cl2/MeOH);elem. anal.;
DOI:10.1016/j.molstruc.2005.02.002