N-trimethylsilyl-4-trifluoromethylbenzaldimine

Base Information

Chemical Name:N-trimethylsilyl-4-trifluoromethylbenzaldimine
CAS No.:199604-04-1
Molecular Formula:C₁₁H₁₄F₃NSi
Molecular Weight:245.32
Hs Code.:

Synonyms:N-trimethylsilyl-4-trifluoromethylbenzaldimine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-trimethylsilyl-4-trifluoromethylbenzaldimine

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Technology Process of N-trimethylsilyl-4-trifluoromethylbenzaldimine

There total 2 articles about N-trimethylsilyl-4-trifluoromethylbenzaldimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 455-19-6
4-Trifluoromethylbenzaldehyde

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 199604-04-1
N-trimethylsilyl-4-trifluoromethylbenzaldimine

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; 1.) 0 deg C, 10 min, 2.) r.t., 1 h;
DOI:10.1002/chem.19970031019

Reference yield:

: 455-19-6
4-Trifluoromethylbenzaldehyde

: 4039-32-1
lithium hexamethyldisilazane

: 199604-04-1
N-trimethylsilyl-4-trifluoromethylbenzaldimine

Guidance literature:: In diethyl ether; at -30 ℃; for 0.5h;
DOI:10.1021/jo971061r

Reference yield: 66.0%

: 563-70-2
bromonitromethane

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 199604-04-1
N-trimethylsilyl-4-trifluoromethylbenzaldimine

: fluoren-9-ylmethyl N-[2-bromo-1-(4-(trifluoromethyl)phenyl)-2-nitroethyl]carbamate

Guidance literature:: bromonitromethane; N-trimethylsilyl-4-trifluoromethylbenzaldimine; With (1R,2R)-N¹,N²-bis[4-(1-pyrrolidinyl)-2-quinolinyl]-1,2-cyclohexanediamine; In toluene; at -78 ℃; for 26h;

(fluorenylmethoxy)carbonyl chloride; In toluene; at 0 ℃; for 3h; stereoselective reaction;
DOI:10.1021/ol501297a