N-benzyloxycarbonylglycyl-L-4-thia-5,5-dimethylproline

Base Information

Chemical Name:N-benzyloxycarbonylglycyl-L-4-thia-5,5-dimethylproline
CAS No.:869002-29-9
Molecular Formula:C₁₆H₂₀N₂O₅S
Molecular Weight:352.411
Hs Code.:

Synonyms:N-benzyloxycarbonylglycyl-L-4-thia-5,5-dimethylproline

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Chemical Property of N-benzyloxycarbonylglycyl-L-4-thia-5,5-dimethylproline

Chemical Property:

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Technology Process of N-benzyloxycarbonylglycyl-L-4-thia-5,5-dimethylproline

There total 3 articles about N-benzyloxycarbonylglycyl-L-4-thia-5,5-dimethylproline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 67-56-1
methanol

: 67089-92-3
L-(-)-2,2-dimethylthiazolidine-4-carboxylic acid hydrochloride salt

: 133010-18-1
Z-glycine fluoride

: 869002-29-9
N-benzyloxycarbonylglycyl-L-4-thia-5,5-dimethylproline

: 1212-53-9
methyl N-benzyloxycarbonylglycinate

Guidance literature:: L-(-)-2,2-dimethylthiazolidine-4-carboxylic acid hydrochloride salt; Z-glycine fluoride; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

methanol; With chloro-trimethyl-silane; at 20 ℃; for 15h;
DOI:10.1016/j.tet.2005.08.026

Reference yield:

: 67089-92-3
L-(-)-2,2-dimethylthiazolidine-4-carboxylic acid hydrochloride salt

: 133010-18-1
Z-glycine fluoride

: 869002-29-9
N-benzyloxycarbonylglycyl-L-4-thia-5,5-dimethylproline

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 18h; Title compound not separated from byproducts;
DOI:10.1016/j.tet.2005.08.026