1-(4-bromo-3-methyl-phenyl)-3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-3-mercapto-butan-1-one

Base Information

• Chemical Name: 1-(4-bromo-3-methyl-phenyl)-3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-3-mercapto-butan-1-one
• CAS No.: 1427274-60-9
• Molecular Formula: C₁₇H₁₂BrCl₂F₃OS
• Molecular Weight: 472.153

Synonyms:1-(4-bromo-3-methyl-phenyl)-3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-3-mercapto-butan-1-one

Chemical Property of 1-(4-bromo-3-methyl-phenyl)-3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-3-mercapto-butan-1-one

Chemical Property:

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Technology Process of 1-(4-bromo-3-methyl-phenyl)-3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-3-mercapto-butan-1-one

There total 10 articles about 1-(4-bromo-3-methyl-phenyl)-3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-3-mercapto-butan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.7%

1-(4-bromo-3-methylphenyl)-3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-2-en-1-one (943437-03-4) → 1-(4-bromo-3-methyl-phenyl)-3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-3-mercapto-butan-1-one (1427274-60-9)

Guidance literature:

With hydrogen sulfide; triethylamine; In dichloromethane; at 0 ℃; for 0.5h;

Reference yield:

(E)-1-(4-bromo-3-methyl-phenyl)-3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-but-2-en-1-one (1154739-81-7) + tiolacetic acid (507-09-5) → 1-(4-bromo-3-methyl-phenyl)-3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-3-mercapto-butan-1-one (1427274-60-9) + thioacetic acid 3-(4-bromo-3-methyl-phenyl)-1-(3,5-dichloro-phenyl)-3-oxo-1-trifluoromethyl-propyl ester

Guidance literature:

With triethylamine; at 20 ℃; for 96h; Inert atmosphere;

Reference yield:

(E)-1-(4-bromo-3-methyl-phenyl)-3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-but-2-en-1-one (1154739-81-7) + tiolacetic acid (507-09-5) → 1-(4-bromo-3-methyl-phenyl)-3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-3-mercapto-butan-1-one (1427274-60-9) + thioacetic acid 3-(4-bromo-3-methyl-phenyl)-1-(3,5-dichloro-phenyl)-3-oxo-1-trifluoromethyl-propyl ester

Guidance literature:

With triethylamine; at 20 ℃; for 96h; Inert atmosphere;

upstream raw materials:

tert-butyl 4-carbamoyl-2-methyl-benzoate

(E)-1-(4-bromo-3-methyl-phenyl)-3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-but-2-en-1-one

tiolacetic acid

4-bromo-2-methylbenzoic acid

Downstream raw materials:

3-(4-bromo-3-methyl-phenyl)-5-(3,5-dichloro-phenyl)-5-trifluoromethyl-4,5-dihydro-isothiazole

C₁₉H₁₄Cl₂F₃NO₂S

N-[[4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]-2-methylphenyl]methyl]-N-ethyl-2-ethylsulfanylacetamide

[4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]-2-methylphenyl]methanol

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