5-bromo-3-(2-chloro-4-hydroxybenzyl)-2-methyl-3H-imidazo[4,5-b]pyridine

Base Information

Chemical Name:5-bromo-3-(2-chloro-4-hydroxybenzyl)-2-methyl-3H-imidazo[4,5-b]pyridine
CAS No.:275384-13-9
Molecular Formula:C₁₄H₁₁BrClN₃O
Molecular Weight:352.618
Hs Code.:

Synonyms:5-bromo-3-(2-chloro-4-hydroxybenzyl)-2-methyl-3H-imidazo[4,5-b]pyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-bromo-3-(2-chloro-4-hydroxybenzyl)-2-methyl-3H-imidazo[4,5-b]pyridine

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Technology Process of 5-bromo-3-(2-chloro-4-hydroxybenzyl)-2-methyl-3H-imidazo[4,5-b]pyridine

There total 7 articles about 5-bromo-3-(2-chloro-4-hydroxybenzyl)-2-methyl-3H-imidazo[4,5-b]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 275384-12-8
2-[N-(4-acetoxy-2-chlorobenzyl)acetamido]-6-bromo-3-nitropyridine

: 7439-89-6
iron

: 144-55-8
sodium hydrogencarbonate

: 275384-13-9
5-bromo-3-(2-chloro-4-hydroxybenzyl)-2-methyl-3H-imidazo[4,5-b]pyridine

Guidance literature:: With acetic acid; In ethanol; chloroform; ethyl acetate;

Reference yield:

: 55304-80-8
2,6-dibromo-3-nitropyridine

: 275384-13-9
5-bromo-3-(2-chloro-4-hydroxybenzyl)-2-methyl-3H-imidazo[4,5-b]pyridine

Guidance literature:: Multi-step reaction with 4 steps

1: ethanol; water

2: sulfuric acid; acetic anhydride / acetic acid

3: water; ethyl acetate; N,N-dimethyl-formamide

4: acetic acid / ethanol; chloroform; ethyl acetate

With sulfuric acid; acetic anhydride; acetic acid; In ethanol; chloroform; water; acetic acid; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 129930-85-4
3-Chloro-4-methylphenyl acetate

: 275384-13-9
5-bromo-3-(2-chloro-4-hydroxybenzyl)-2-methyl-3H-imidazo[4,5-b]pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide / tetrachloromethane; hexane

2: water; ethyl acetate; N,N-dimethyl-formamide

3: acetic acid / ethanol; chloroform; ethyl acetate

With N-Bromosuccinimide; acetic acid; In tetrachloromethane; ethanol; hexane; chloroform; water; ethyl acetate; N,N-dimethyl-formamide;