2-(4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl)-3-hydroxybutanoic acid

Base Information

Chemical Name:2-(4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl)-3-hydroxybutanoic acid
CAS No.:1056555-52-2
Molecular Formula:C₂₀H₂₂Cl₂O₅
Molecular Weight:413.298
Hs Code.:

Synonyms:2-(4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl)-3-hydroxybutanoic acid

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Chemical Property of 2-(4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl)-3-hydroxybutanoic acid

Chemical Property:

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Technology Process of 2-(4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl)-3-hydroxybutanoic acid

There total 7 articles about 2-(4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl)-3-hydroxybutanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1056555-51-1
methyl 2-(4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl)-3-hydroxybutanoate

: 1056555-52-2
2-(4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl)-3-hydroxybutanoic acid

Guidance literature:: methyl 2-(4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl)-3-hydroxybutanoate; With methanol; lithium hydroxide; water; at 20 ℃; for 12h;

With hydrogenchloride; water; pH=~ 2;

Reference yield:

: 921630-64-0
2-(2,6-dichloro-4-methyl-phenoxy)-ethanol

: 1056555-52-2
2-(4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl)-3-hydroxybutanoic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: tributylphosphine; 1,1'-azodicarbonyl-dipiperidine / tetrahydrofuran; toluene / 4 h / 80 °C

2.1: sodium tetrahydroborate / methanol / 0.75 h / 0 - 20 °C

3.1: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 1.75 h / 0 - 20 °C

4.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 - -40 °C

4.2: 15.25 h / -78 - 20 °C

5.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0.5 h / 20 °C

6.1: methanol; lithium hydroxide; water / 12 h / 20 °C

6.2: pH ~ 2

With 1H-imidazole; methanol; lithium hydroxide; sodium tetrahydroborate; tributylphosphine; water; iodine; potassium hexamethylsilazane; triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; methanol; dichloromethane; toluene;

Reference yield:

: 921630-61-7
4-[2-(2,6-dichloro-4-methyl-phenoxy)-ethoxy]-benzaldehyde

: 1056555-52-2
2-(4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl)-3-hydroxybutanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium tetrahydroborate / methanol / 0.75 h / 0 - 20 °C

2.1: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 1.75 h / 0 - 20 °C

3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 - -40 °C

3.2: 15.25 h / -78 - 20 °C

4.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0.5 h / 20 °C

5.1: methanol; lithium hydroxide; water / 12 h / 20 °C

5.2: pH ~ 2

With 1H-imidazole; methanol; lithium hydroxide; sodium tetrahydroborate; water; iodine; potassium hexamethylsilazane; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; toluene;