methyl 2-(4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl)-3-hydroxybutanoate

Base Information

Chemical Name:methyl 2-(4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl)-3-hydroxybutanoate
CAS No.:1056555-51-1
Molecular Formula:C₂₁H₂₄Cl₂O₅
Molecular Weight:427.325
Hs Code.:

Synonyms:methyl 2-(4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl)-3-hydroxybutanoate

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Chemical Property of methyl 2-(4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl)-3-hydroxybutanoate

Chemical Property:

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Technology Process of methyl 2-(4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl)-3-hydroxybutanoate

There total 6 articles about methyl 2-(4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl)-3-hydroxybutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1056555-50-0
methyl 2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}-3-oxobutanoate

: 1056555-51-1
methyl 2-(4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl)-3-hydroxybutanoate

Guidance literature:: methyl 2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}-3-oxobutanoate; With sodium tetrahydroborate; In tetrahydrofuran; methanol; at 20 ℃; for 0.5h;

With sodium hydroxide; water; In diethyl ether;

Reference yield:

: 921630-64-0
2-(2,6-dichloro-4-methyl-phenoxy)-ethanol

: 1056555-51-1
methyl 2-(4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl)-3-hydroxybutanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: tributylphosphine; 1,1'-azodicarbonyl-dipiperidine / tetrahydrofuran; toluene / 4 h / 80 °C

2.1: sodium tetrahydroborate / methanol / 0.75 h / 0 - 20 °C

3.1: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 1.75 h / 0 - 20 °C

4.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 - -40 °C

4.2: 15.25 h / -78 - 20 °C

5.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0.5 h / 20 °C

With 1H-imidazole; sodium tetrahydroborate; tributylphosphine; iodine; potassium hexamethylsilazane; triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; methanol; dichloromethane; toluene;

Reference yield:

: 921630-61-7
4-[2-(2,6-dichloro-4-methyl-phenoxy)-ethoxy]-benzaldehyde

: 1056555-51-1
methyl 2-(4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl)-3-hydroxybutanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tetrahydroborate / methanol / 0.75 h / 0 - 20 °C

2.1: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 1.75 h / 0 - 20 °C

3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 - -40 °C

3.2: 15.25 h / -78 - 20 °C

4.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0.5 h / 20 °C

With 1H-imidazole; sodium tetrahydroborate; iodine; potassium hexamethylsilazane; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; toluene;