C₂₂H₂₀N₂O₄

Base Information

• Chemical Name: C₂₂H₂₀N₂O₄
• CAS No.: 1618102-42-3
• Molecular Formula: C₂₂H₂₀N₂O₄
• Molecular Weight: 376.412
• Mol file: 1618102-42-3.mol

Synonyms:

Chemical Property of C₂₂H₂₀N₂O₄

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₂₀N₂O₄

There total 1 articles about C₂₂H₂₀N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

succinic acid anhydride (108-30-5) + N-(3-aminopropionyl)-5,6-dihydro-11,12-didehydrodibenzo[b,f]azocine (1255942-06-3) → C22H20N2O4 (1618102-42-3)

Guidance literature:

With triethylamine; In chloroform; for 4h; Reagent/catalyst;

DOI:10.1002/chem.201402573

Reference yield: 80.0%

N-(3-(2-(2-(3-aminopropoxy)ethoxy)ethoxy)propyl)-2,4-dinitroaniline (1058165-51-7) + C22H20N2O4 (1618102-42-3) → C38H44N6O10

Guidance literature:

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

DOI:10.1039/d0cc04474a

Reference yield: 64.7%

1-hydroxy-pyrrolidine-2,5-dione (6066-82-6) + C22H20N2O4 (1618102-42-3) → DBCO-NHS ester (1787252-03-2)

Guidance literature:

With dicyclohexyl-carbodiimide; In chloroform; at 20 ℃;

upstream raw materials:

succinic acid anhydride

N-(3-aminopropionyl)-5,6-dihydro-11,12-didehydrodibenzo[b,f]azocine

Downstream raw materials:

DBCO-NHS ester