Silane, trimethyl[(2-methyl-1-phenoxy-1-propenyl)oxy]-

Base Information

Chemical Name:Silane, trimethyl[(2-methyl-1-phenoxy-1-propenyl)oxy]-
CAS No.:120615-54-5
Molecular Formula:C13H20O2Si
Molecular Weight:236.386
Hs Code.:
DSSTox Substance ID:DTXSID90466196
Nikkaji Number:J1.652.209K

Synonyms:Silane, trimethyl[(2-methyl-1-phenoxy-1-propenyl)oxy]-;120615-54-5;DTXSID90466196

Suppliers and Price of Silane, trimethyl[(2-methyl-1-phenoxy-1-propenyl)oxy]-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silane, trimethyl[(2-methyl-1-phenoxy-1-propenyl)oxy]-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:236.123256411
Heavy Atom Count:16
Complexity:243

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=C(OC1=CC=CC=C1)O[Si](C)(C)C)C

Technology Process of Silane, trimethyl[(2-methyl-1-phenoxy-1-propenyl)oxy]-

There total 2 articles about Silane, trimethyl[(2-methyl-1-phenoxy-1-propenyl)oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 75-77-4
chloro-trimethyl-silane

: 20279-29-2
phenyl isobutyrate

: 120615-54-5
trimethyl((2-methyl-1-phenoxyprop-1-en-1-yl)oxy)silane

Guidance literature:: With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 9h;
DOI:10.1002/chem.201602150

Reference yield:

: 108-95-2,27073-41-2
phenol

: 120615-54-5
trimethyl((2-methyl-1-phenoxyprop-1-en-1-yl)oxy)silane

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide; tetrabutyl-ammonium chloride / water; dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 1.17 h / -78 °C / Inert atmosphere

2.2: 2 h / -78 - 20 °C / Inert atmosphere

With tetrabutyl-ammonium chloride; sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; water;
DOI:10.1021/acs.orglett.5b03088

Reference yield: 99.0%

: 120615-54-5
trimethyl((2-methyl-1-phenoxyprop-1-en-1-yl)oxy)silane

: 98-86-2
acetophenone

: 1626437-21-5
phenyl 2,2-dimethyl-3-phenyl-3-(trimethylsiloxy)butanoate

Guidance literature:: With solid acid of tin(IV) ion-exchanged montmorillonite; In dichloromethane; at 0 ℃; for 4h; Inert atmosphere; Reflux;
DOI:10.1246/cl.131095