Brn 1446024

Base Information

• Chemical Name: Brn 1446024
• CAS No.: 98527-29-8
• Molecular Formula: CH₄O₃S
• Molecular Weight: 96.107
• Mol file: 98527-29-8.mol

Synonyms:

Chemical Property of Brn 1446024

Chemical Property:

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Technology Process of Brn 1446024

There total 67 articles about Brn 1446024 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1-(methanesulfonoyloxy)-2(1H)-quinolone (1404369-05-6) → methanesulfonic acid (75-75-2,98527-29-8) + 2-quinolone (59-31-4,70254-42-1,493-62-9)

Guidance literature:

In methanol; water; Quantum yield; UV-irradiation; Photolysis;

DOI:10.1002/chem.201104065

Reference yield:

p-nitrophenyl methanesulfonate (20455-07-6) → 4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + methanesulfonic acid (75-75-2,98527-29-8)

Guidance literature:

With water; hydroxide; In 1,4-dioxane; at 25 ℃; Rate constant;

DOI:10.1021/jo00350a032

Reference yield:

Florfenicol (73231-34-2) → methanesulfonic acid (75-75-2,98527-29-8) + para-methanesulfonylbenzaldehyde (5398-77-6) + C4H4Cl2FNO2 + C12H13Cl3FNO4S + C11H11Cl3FNO2 + C11H12Cl2FNO2 + (1R,2S)-2-amino-3-fluoro-1-<4-(methylsulphonyl)phenyl>-1-propanol (76639-93-5,105182-37-4,118015-48-8) + benzaldehyde (100-52-7) + benzoic acid (65-85-0,8013-63-6)

Guidance literature:

With water; hypochloric acid; at 15 ℃; for 0.5h; pH=5.7; Reagent/catalyst; Kinetics;

DOI:10.1039/c6ra23342b

upstream raw materials:

methane

Dimethyldisulphide

O,O-diethyl S-methyl phosphorothioate

ethanol

Downstream raw materials:

sec-butyl methanesulfonate

α-methanesulfonyloxy-p-bromoacetophenone

(1R,2R)-2-amino-3-dichloroacetoxy-1-(4-nitro-phenyl)-propan-1-ol

5-cyano-2-methyl-6-oxo-4-phenoxymethyl-3,4,5,6-tetrahydro-pyridine-3-carboxylic acid ethyl ester

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