Technology Process of Benzene, 1-ethenyl-2-(2-propenyl)-
There total 4 articles about Benzene, 1-ethenyl-2-(2-propenyl)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
-butyl vinyl ether; phenyllithium;
With
zirconocene methyl chloride;
In
tetrahydrofuran;
at -78 - 80 ℃;
for 3.5h;
3-chloroprop-1-ene;
With
copper(l) chloride;
In
tetrahydrofuran;
at 25 - 80 ℃;
for 1.33333h;
DOI:10.1055/s-2005-872699
- Guidance literature:
-
With
cesium fluoride; bis(dibenzylideneacetone)-palladium(0); tricyclohexylphosphine;
In
1,4-dioxane;
for 48h;
Inert atmosphere;
Reflux;
DOI:10.1039/c2cc17572j
- Guidance literature:
-
2-bromostyrene;
With
magnesium;
In
diethyl ether;
for 0.5h;
Reflux;
Inert atmosphere;
Flow reactor;
allyl bromide;
With
water; ammonium chloride;
at 0 - 20 ℃;
for 24h;
Inert atmosphere;
DOI:10.1021/acs.organomet.5b00218
