- Triisopropyl borate
- Triisopropyl orthoformate
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Cas Database |
| Name |
Triisopropyl orthoformate |
EINECS | 224-688-9 |
| CAS No. | 4447-60-3 | Density | 0.888 g/cm3 |
| PSA | 27.69000 | LogP | 2.54500 |
| Solubility | N/A | Melting Point |
N/A |
| Formula | C10H22O3 | Boiling Point | 166.999 °C at 760 mmHg |
| Molecular Weight | 190.283 | Flash Point | 63.43 °C |
| Transport Information | UN 3272 3/PG 3 | Appearance | clear colorless liquid |
| Safety | 26-36-37/39-16 | Risk Codes | 10-36/37/38 |
| Molecular Structure |
|
Hazard Symbols |
 Xi
|
| Synonyms |
Orthoformicacid, triisopropyl ester (6CI,7CI,8CI);Tri-iso-propyl orthoformate; |
Article Data | 11 |
Triisopropyl orthoformate Synthetic route
| Conditions | Yield |
|---|---|
| With sodium hydride In mineral oil at 120℃; under 2585.81 Torr; for 24h; | 90% |
| Conditions | Yield |
|---|---|
| With boron trifluoride In Hexadecane at 110℃; for 8h; Autoclave; | 88% |
| Conditions | Yield |
|---|---|
| Stage #1: hydrogen cyanide With hydrogenchloride In isopropyl alcohol; mineral oil at -3 - 30℃; for 2.33333h; Stage #2: isopropyl alcohol In mineral oil at 35 - 53℃; for 5h; Inert atmosphere; | 71.84% |
| Conditions | Yield |
|---|---|
| With benzoyl chloride In Petroleum ether at 0 - 40℃; for 2.25h; | 58% |
| Conditions | Yield |
|---|---|
| With sodium hydroxide at 120℃; under 2585.81 Torr; for 24h; | A 10% B 40% |
- 5780-15-4
4-(Methoxymethylene)-morpholinium methyl sulfate
- 67-63-0
isopropyl alcohol
- 4447-60-3
Triisopropoxymethan
| Conditions | Yield |
|---|---|
| 1) 16h, 2) 4h, 40 deg C; | 2.9% |
| Conditions | Yield |
|---|---|
| With cerium triflate In isopropyl alcohol; toluene at 20℃; for 0.5h; | 99% |
- 4447-60-3
Triisopropoxymethan
- 1428963-73-8
tert-butyl 2'-bromo-5'-formyl-4'-methoxybiphenyl-2-ylcarbamate
- 1428963-58-9
tert-butyl 2'-bromo-5'-(diisopropoxymethyl)-4'-methoxybiphenyl-2-ylcarbamate
| Conditions | Yield |
|---|---|
| With N-Bromosuccinimide In dichloromethane; isopropyl alcohol at 20℃; for 6h; | 99% |
- 104-53-0
3-phenyl-propionaldehyde
- 4447-60-3
Triisopropoxymethan
- 64245-42-7
3-phenylpropionaldehyde diisopropyl acetal
| Conditions | Yield |
|---|---|
| With cerium triflate In isopropyl alcohol; toluene at 20℃; for 0.0833333h; | 98% |
- 4447-60-3
Triisopropoxymethan
| Conditions | Yield |
|---|---|
| With hydrogenchloride In dichloromethane; isopropyl alcohol at 0 - 20℃; | 97% |
Triisopropyl orthoformate Specification
The Triisopropyl orthoformate, with the cas registry number 4447-60-3, has the IUPAC name of 2-[di(propan-2-yloxy)methoxy]propane and the systematic name of 2-[bis(propan-2-yloxy)methoxy]propane. This is a kind of clear colourless liquid, and its product categories are including Orthoesters; Acetals/Ketals/Ortho Esters; Organic Building Blocks; Oxygen Compounds.
The characteristics of this chemical are as below: (1)ACD/LogP: 3.19; (2)ACD/LogD (pH 5.5): 3.19; (3)ACD/LogD (pH 7.4): 3.19; (4)ACD/BCF (pH 5.5): 155.82; (5)ACD/BCF (pH 7.4): 155.82; (6)ACD/KOC (pH 5.5): 1291.5; (7)ACD/KOC (pH 7.4): 1291.5; (8)#H bond acceptors: 3; (9)#H bond donors: 0; (10)#Freely Rotating Bonds: 6; (11)Polar Surface Area: 27.69; (12)Index of Refraction: 1.413; (13)Molar Refractivity: 53.44 cm3; (14)Molar Volume: 214.1 cm3; (15)Polarizability: 21.18 ×10-24 cm3; (16)Surface Tension: 24.9 dyne/cm; (17)Density: 0.888 g/cm3; (18)Flash Point: 63.4 °C; (19)Enthalpy of Vaporization: 38.69 kJ/mol; (20)Boiling Point: 167 °C at 760 mmHg; (21)Vapour Pressure: 2.29 mmHg at 25°C; (22)Exact Mass: 190.156895; (23)MonoIsotopic Mass: 190.156895; (24)Topological Polar Surface Area: 27.7; (25)Heavy Atom Count: 13; (26)Formal Charge: 0; (27)Complexity: 97.6.
Use of Triisopropyl orthoformate: Triisopropyl orthoformate could react to produce diisopropoxymethinium; tetrafluoroborate, with the following condition: reagent: BF3-Et2O; solvent: CH2Cl2; reaction temp.: 30 ℃.
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When you are using this chemical, please be very cautious, and then take some measures to protect yourself. Being a kind of irritant chemical, it is irritating to eyes, respiratory system and skin and it may cause inflammation to the skin or other mucous. Therefore, you should take the following instructions. Wear suitable protective clothing, gloves and eye/face protection, and if in case of contacting with eyes, rinse immediately with plenty of water and seek medical advice. While storing, keep away from sources of ignition - No smoking.
Additionally, you could convert the following datas into the molecular structure:
(1)Canonical SMILES: CC(C)OC(OC(C)C)OC(C)C
(2)InChI: InChI=1S/C10H22O3/c1-7(2)11-10(12-8(3)4)13-9(5)6/h7-10H,1-6H3
(3)InChIKey: FPIVAWNGRDHRSQ-UHFFFAOYSA-N
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