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Basic Information
CAS No.: 116-17-6
Name: Triisopropyl phosphite
Molecular Structure:
Molecular Structure of 116-17-6 (Triisopropyl phosphite)
Formula: C9H21O3P
Molecular Weight: 208.238
Synonyms: Isopropylphosphite ((C3H7O)3P) (6CI,7CI);Phosphorous acid, triisopropyl ester (8CI);Isopropyl phosphite;NSC 6516;Tri-2-propyl phosphite;Triisopropoxyphosphine;
EINECS: 204-130-0
Density: 0.844 g/cm3
Boiling Point: 181.4 °C at 760 mmHg
Flash Point: 67.8 °C
Solubility: insoluble in water
Appearance: clear to slightly turbid colorless liquid
Hazard Symbols: ToxicT, FlammableF
Risk Codes: 25-38-68
Safety: 37-46-45-36/37
Transport Information: UN 3278 6.1/PG 3
PSA: 41.28000
LogP: 3.48830
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Synthetic route
117965-98-7

S-acetyl O,O-diisopropyl phosphorothioite

67-63-0

isopropyl alcohol

116-17-6

triisopropyl phosphite

Conditions
ConditionsYield
at 0℃;64%
67-63-0

isopropyl alcohol

A

41662-51-5

diisopropyl phosphorochloridite

B

116-17-6

triisopropyl phosphite

Conditions
ConditionsYield
With pyridine; phosphorus trichloride In Petroleum ether for 3h; Ambient temperature;A 34%
B n/a
67-63-0

isopropyl alcohol

116-17-6

triisopropyl phosphite

Conditions
ConditionsYield
With pyridine; diethyl ether; phosphorus trichloride
With diethyl ether; 2,3-Dimethylaniline; phosphorus trichloride
With triethylamine; Petroleum ether; phosphorus trichloride
60-29-7

diethyl ether

121-69-7

N,N-dimethyl-aniline

67-63-0

isopropyl alcohol

7719-12-2, 52843-90-0

phosphorus trichloride

116-17-6

triisopropyl phosphite

...Expand
110-82-7

cyclohexane

121-69-7

N,N-dimethyl-aniline

67-63-0

isopropyl alcohol

7719-12-2, 52843-90-0

phosphorus trichloride

116-17-6

triisopropyl phosphite

Conditions
ConditionsYield
at 22 - 23℃;
...Expand
121-44-8

triethylamine

67-63-0

isopropyl alcohol

7719-12-2, 52843-90-0

phosphorus trichloride

petroleum ether

petroleum ether

116-17-6

triisopropyl phosphite

...Expand
67-63-0

isopropyl alcohol

211055-34-4

O,O'-diisopropyl N,N-diisopropylphosphoramidite

116-17-6

triisopropyl phosphite

Conditions
ConditionsYield
With N,N-dimethylbenzylammonium fluoride In acetonitrile at 20℃; Kinetics; Further Variations:; Reagents;
41662-51-5

diisopropyl phosphorochloridite

116-17-6

triisopropyl phosphite

Conditions
ConditionsYield
Multi-step reaction with 2 steps
2: 64 percent / 0 °C
View Scheme

Fe2(η-Cp)(CO)2(P(OPr-i)3)

121-45-9

phosphorous acid trimethyl ester

A

{(C5H5)Fe(CO)P(OCH3)3}2

B

116-17-6

triisopropyl phosphite

Conditions
ConditionsYield
In cyclohexane byproducts: CO; Irradiation (UV/VIS); irradn. of Fe complex and phosphite ligand in cyclohexane at room temp.; not isolated, detected by IR;
...Expand
116-17-6

triisopropyl phosphite

513-02-0

triisopropyl phosphate

Conditions
ConditionsYield
With water; 7,7',8,8'-tetracyanoquinodimethane In acetonitrile at 25℃; Rate constant;100%
With water; 7,7',8,8'-tetracyanoquinodimethane In acetonitrile100%
With 1-methyl-3-(4-((2,4,6-triisopropylphenyl)tellanyl)benzyl)-1H-imidazol-3-ium hexafluorophosphate; Rose Bengal lactone at 15℃; for 2.5h; Irradiation; Ionic liquid;99%
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  • Casno:

    116-17-6

    Triisopropyl phosphite

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Chemistry

Triisopropyl phosphitet is also called phosphorous acid tris(1-methylethyl) ester or triisopropoxyphosphine

Molecular Formula: C9H21O3P
Formula Weight: 208.24 
Boiling point : 63-64 °C  11 mm Hg(lit.) 
Density : 0.914  
Vapor pressure : <2 mm Hg ( 20 °C)
Refractive index : n20/D 1.411(lit.) 
Fp : 154 °F 
Water Solubility : Insoluble  
Sensitive : Moisture Sensitive  
BRN : 1701528
 

 

 

Safety Profile

Hazard Codes : T,F  
Risk Statements : 25-38-68  
Safety Statements : 37-46-45-36/37  
RIDADR : UN 3278 6.1/PG 3 
WGK Germany : 3 
RTECS : TH2800000 
F : 1-10  
Hazard Note : Toxic/Flammable/Moisture Sensitive/  
HazardClass : 3  
PackingGroup : III
 

 

Specification

FIRE FIGHTING MEASURES 
When triisopropyl phosphite is in any fire,please wear a self-contained breathing apparatus in pressure-demand, and full protective gear.It will burn if involved in a fire because it's combustible liquid.
Extinguishing Method:Use water spray, dry chemical, carbon dioxide, or chemical foam.