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109-78-4

Basic Information
CAS No.: 109-78-4
Name: 3-Hydroxypropanenitrile
Article Data: 71
Molecular Structure:
Molecular Structure of 109-78-4 (3-Hydroxypropanenitrile)
Formula: C3H5NO
Molecular Weight: 71.0788
Synonyms: Hydracrylonitrile(8CI);1-Cyano-2-hydroxyethane;2-Cyanoethanol;2-Cyanoethyl alcohol;2-Hydroxycyanoethane;2-Hydroxyethyl cyanide;3-Hydroxypropanenitrile;Ethylene cyanhydrine;Ethylene cyanohydrin;Glycolcyanohydrin;NSC 2598;b-Cyanoethanol;b-Hydroxyethyl cyanide;b-Hydroxypropionitrile;
EINECS: 203-704-8
Density: 1.04 g/cm3
Melting Point: -46 °C
Boiling Point: 229.6 °C at 760 mmHg
Flash Point: 92.7 °C
Solubility: >=10 g/100 mL at 20 °C in water
Appearance: Colourless or straw-coloured liquid
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36-24/25
Transport Information: 2810
PSA: 44.02000
LogP: -0.10762
Synthetic route
107-13-1

acrylonitrile

A

111-97-7

3,3'-thiobis-propanenitrile

B

109-78-4

3-Hydroxypropionitrile

Conditions
ConditionsYield
With sodium sulfide; benzyltri(n-butyl)ammonium chloride In water for 0.166667h;A 98%
B n/a
75-21-8

oxirane

74-90-8

hydrogen cyanide

109-78-4

3-Hydroxypropionitrile

Conditions
ConditionsYield
With aluminum oxide; boron trifluoride diethyl etherate In propylene glycol at -10 - 10℃; for 28h; Reagent/catalyst; Temperature;97.3%
143-33-9

sodium cyanide

107-07-3

2-chloro-ethanol

109-78-4

3-Hydroxypropionitrile

Conditions
ConditionsYield
With PEG400 for 6h; Heating;93%
107-13-1

acrylonitrile

109-78-4

3-Hydroxypropionitrile

Conditions
ConditionsYield
With sodium hydroxide at 50℃; for 0.2h;92%
With sodium hydroxide In water at 50℃; for 4h;65%
With water; copper(II) oxide
90087-76-6, 89923-32-0

3-((tetrahydro-2H-pyran-2-yl)oxy)propanenitrile

109-78-4

3-Hydroxypropionitrile

Conditions
ConditionsYield
With silica-supported NaHSO4 In methanol at 20℃; for 0.25h;92%
With zinc(II) trifluoromethanesulfonate In methanol at 20℃; for 0.666667h;81%

3-(4-methoxybenzyloxy)propanenitrile

109-78-4

3-Hydroxypropionitrile

Conditions
ConditionsYield
With acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium nitrite at 20℃; for 18h; Green chemistry; chemoselective reaction;84%
151-50-8

potassium cyanide

107-07-3

2-chloro-ethanol

109-78-4

3-Hydroxypropionitrile

Conditions
ConditionsYield
With sodium iodide In ethanol for 5h; Heating;80%
at 100℃;
With ethanol
131379-56-1

3-(1,1,1,3,3,3-hexamethyl-2-(trimethylsilyl)trisilan-2-yl)propanenitrile

109-78-4

3-Hydroxypropionitrile

Conditions
ConditionsYield
With 2,3-dimethyl-1,4-benzoquinone; tetrabutyl ammonium fluoride; oxygen In tetrahydrofuran for 0.833333h; Ambient temperature;71%
107-13-1

acrylonitrile

108-95-2

phenol

A

3055-86-5

3-phenoxypropionitrile

B

109-78-4

3-Hydroxypropionitrile

Conditions
ConditionsYield
With tetramethyl ammoniumhydroxide In water at 60℃; for 0.5h; Temperature; Reagent/catalyst; Time; Michael Addition; Microwave irradiation;A 68%
B n/a
22059-21-8

aminocyclopropane-1-carboxylic acid

A

74-85-1

ethene

B

109-78-4

3-Hydroxypropionitrile

Conditions
ConditionsYield
With lithium hypochlorite In water Ambient temperature;A 9.8%
B 60%
With lithium hypochlorite In water Product distribution; Mechanism; Ambient temperature; other solvent and additives; var. cyclopropanamines;A 9.8%
B 60%
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    Name: 3-Hydroxypropionitrile CAS No. :109-78-4 Molecular formula: C3H5NO Molecular weight: 71.07790 Appearance:Colorless liquid Storage: Preserve in well-closed, light-resistant and airtight containers. Package: 25kgs/drum Application:used in th

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    Product Name: 3-Hydroxypropionitrile CAS: 109-78-4 MF: C3H5NO MW: 71.08 EINECS: 203-704-8 Mol File: 109-78-4.mol 3-Hydroxypropionitrile Structure 3-Hydroxypropionitrile Chemical Properties Melting point -46 °C (lit.) Boili

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  • 109-78-4  CAS NO.109-78-4

  • Casno:

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    109-78-4 CAS NO.109-78-4

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Chemistry

Hydracrylonitrile(109-78-4)'s molecular formula is C3H5NO and its formula weight is 71.08.
The density of hydracrylonitrile(109-78-4) is 1.04 and it has a  melting point of -46°C. The Boiling point is 228°C. The refractive index is about 1.4246-1.4266. Its flash point is 128°C. The water solubility should be  equal to or greater than 10 g/100 mL at 20°C.
Hydracrylonitrile(109-78-4) has the property of being dissolved in water, ethanol, acetone and methyl ethyl ketone(MEK). It is not soluble in benzene, light petroleum, carbon bisulfide and Carbon tetrachloride.
The molecular structure of hydracrylonitrile(109-78-4) :

Uses

Hydracrylonitrile(109-78-4) is used as a solvent for dissolving cellulose esters and some Inorganic salts. 3-Amino-1-propanol  can be produced from hydracrylonitrile(109-78-4) by hydrogenation, which is used to produce synthetic drug( such as cyclophosphamide and inderal).

Toxicity Data With Reference

1.   

skn-rbt 10 mg/24H open

   JIHTAB    Journal of Industrial Hygiene and Toxicology. 26 (1944),269.
2.   

skn-rbt 520 mg open MLD

   UCDS**    Union Carbide Data Sheet. (Industrial Medicine and Toxicology Dept., Union Carbide Corp., 270 Park Ave., New York, NY 10017) 8/18 ,1967.
3.   

eye-rbt 500 mg

   AJOPAA    American Journal of Ophthalmology. 29 (1946),1363.
4.   

orl-rat LD50:3200 mg/kg

   38MKAJ    Pattys Industrial Hygiene and Toxicology. 2C (1982),4875.
5.   

orl-mus LD50:1800 mg/kg

   AMIHBC    AMA Archives of Industrial Hygiene and Occupational Medicine. 8 (1953),371.
6.   

ihl-mus LC33:300 mg/m3/2H

   85GMAT    Toxicometric Parameters of Industrial Toxic Chemicals Under Single Exposure Izmerov, N.F., et al.,Moscow, USSR.: Centre of International Projects, GKNT,1982,66.
7.   

ipr-mus LD50:500 mg/kg

   NTIS**    National Technical Information Service. (Springfield, VA 22161) (Formerly U.S. Clearinghouse for Scientific and Technical Information) AD277-689 .
8.   

orl-rbt LDLo:900 mg/kg

   AMIHBC    AMA Archives of Industrial Hygiene and Occupational Medicine. 8 (1953),371.
9.   

skn-rbt LD50:5000 mg/kg

   UCDS**    Union Carbide Data Sheet. (Industrial Medicine and Toxicology Dept., Union Carbide

Consensus Reports

Reported in EPA TSCA Inventory. Cyanide compounds are on the Community Right-To-Know List.

Safety Profile

Poison by inhalation. Moderately toxic by ingestion and intraperitoneal routes. Mildly toxic by skin contact. A skin and eye irritant. Combustible when exposed to heat or flame. Reacts violently with mineral acids (e.g., chlorosulfonic acid, oleum, sulfuric acid), amines, or inorganic bases (e.g., NaOH). Reacts with water or steam to produce toxic and flammable vapors. To fight fire, use CO2, dry chemical, alcohol foam. When heated to decomposition or on contact with acid or acid fumes it emits highly toxic fumes of CN. See also NITRILES.
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