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110-58-7

Basic Information
CAS No.: 110-58-7
Name: Amylamine
Article Data: 130
Cas Database
Molecular Structure:
Molecular Structure of 110-58-7 (Amylamine)
Formula: C5H13N
Molecular Weight: 87.1649
Synonyms: Pentylamine(8CI);1-Aminopentane;1-Pentylamine;Monoamylamine;Monopentylamine;NSC 7906;Norleucamine;n-Amylamine;n-Pentylamine;1-Pentanamine;
EINECS: 203-780-2
Density: 0.755 g/cm3
Melting Point: -55 °C(lit.)
Boiling Point: 105.5 °C at 760 mmHg
Flash Point: 4.4 °C
Solubility: soluble
Appearance: clear colourless to very slightly yellow liquid
Hazard Symbols: FlammableF,CorrosiveC
Risk Codes: 11-22-34-42/43-20/21/22
Safety: 16-26-36/37/39-45-33
Transport Information: UN 1106 3/PG 2
PSA: 26.02000
LogP: 1.83560
Synthetic route
110-59-8

pentanonitrile

110-58-7

1-pentanamine

Conditions
ConditionsYield
With borane-ammonia complex; C15H30Cl2CoN3P In hexane at 120℃; for 16h; Sealed tube; Inert atmosphere; chemoselective reaction;86%
With hydrogen; sodium methylate; nickel In methanol hydrogen generated in situ electrochemically on Raney nickel electrode;72%
With lithium aluminium tetrahydride71%
110-62-3

pentanal

110-58-7

1-pentanamine

Conditions
ConditionsYield
With ammonia; hydrogen In methanol at 30℃; for 15h; Autoclave;94%
With ammonium hydroxide; ammonium acetate; hydrogen; [Ru(cod)Cl]2; trisodium tris(3-sulfophenyl)phosphine In toluene at 145℃; under 48754.9 Torr; for 10h;47 % Chromat.
With ammonium hydroxide; hydrogen at 65℃; under 11251.1 Torr; for 12h; Autoclave; Green chemistry;
With pyridoxal 5'-phosphate; Amine transaminase 117; rac-methylbenzylamine; N-2-hydroxyethylpiperazine-N'-2-ethanesulfonic acid In water; dimethyl sulfoxide at 30℃; Reagent/catalyst; Enzymatic reaction;
26330-06-3

pentyl azide

110-58-7

1-pentanamine

Conditions
ConditionsYield
With hydrogen; MCM-silylamine Pd(II) In methanol at 20℃; for 2h; Reduction;90%
1119-46-6

5-chloro-valeric acid

A

110-89-4

piperidine

B

675-20-7

piperidin-2-one

C

110-58-7

1-pentanamine

D

109-73-9

N-butylamine

Conditions
ConditionsYield
Stage #1: 5-chloro-valeric acid With cyclopentyl methyl ether; ammonia at 200℃; under 4500.45 Torr; Sealed tube; Green chemistry;
Stage #2: With cyclopentyl methyl ether; ammonia; hydrogen at 200℃; under 42004.2 Torr; for 6.5h; Cooling with ice; Green chemistry;
A 85%
B 9%
C 2%
D 2%
628-02-4

Caproamide

110-58-7

1-pentanamine

Conditions
ConditionsYield
With sodium hydroxide; benzyltrimethylazanium tribroman-2-uide In water at 70℃; for 2h;80%
With sodium hydroxide; sodium bromite In water at 75℃; for 0.5h;60%
With sodium hypochlorite
71-41-0

pentan-1-ol

A

110-58-7

1-pentanamine

B

109-52-4

valeric acid

Conditions
ConditionsYield
With carbonylchlorohydrido(4,5-bis((diisopropylphosphino)methyl)acridine)ruthenium(II); ammonia; water In 1,4-dioxane at 135℃; under 5700.38 Torr; for 30h; Inert atmosphere;A 70.0 %Chromat.
B n/a
60169-95-1

N,N'-dipentyl-oxalamide

110-58-7

1-pentanamine

Conditions
ConditionsYield
With potassium tert-butylate; hydrogen; [Ru(PtBuNNHBn)H(CO)Cl] In toluene at 135℃; under 30003 Torr; for 24h;97 %Spectr.
110-58-7

1-pentanamine

Conditions
ConditionsYield
With ethanol; nickel kieselguhr at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation;
With diethyl ether; nickel kieselguhr at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation;
With palladium on activated charcoal; acetic acid Hydrogenation;

A

110-58-7

1-pentanamine

B

2050-92-2

Di-n-amylamine

Conditions
ConditionsYield
With nickel kieselguhr; methyl cyclohexane at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation;
With diethyl ether; nickel kieselguhr at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation;
With ethanol; nickel kieselguhr at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation;
628-02-4

Caproamide

A

110-58-7

1-pentanamine

B

142-62-1

hexanoic acid

Conditions
ConditionsYield
With sodium hydroxide; sodium persulfate; sodium chloride In water at 85 - 90℃; for 7h;A 36%
B 56%
With sodium hydroxide; sodium persulfate; copper dichloride In water at 85 - 90℃; for 7h;A 36%
B 56%
With sodium hydroxide; sodium persulfate; sodium chloride In water at 85 - 90℃; for 7h;A 36%
B 52%
With sodium hydroxide; sodium persulfate; sodium chloride In water at 85 - 90℃; for 7h;A 36%
B 52%
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Chemistry

Molecular Formula: C5H13N
Molecular Weight: 87.16
Density: 0.755
Melting point: -50 oC
Boiling point: 104 oC
VAPOR DENSITY: 3.0
AUTOIGNITION: 435 oC
FLASH POINT: 20 oC
Refractive index: 1.41-1.412
Flash point: 4 oC
Water solubility: soluble
Soluble: alcohol
PHYSICAL STATE OF Amylamine (110-58-7): clear liquid
ODOR OF Amylamine (110-58-7): ammonia odor

Uses

Amylamine (110-58-7) can be used for medicine, dyes, emulsifiers, thiofide, anticorrosive agent, flotation agent and so on.

Production

In the presence of catalyst, sodium azide reacts with caproic acid. After alkali neutralization, wet distillation and then extracting distillate by aether. Extract liquor is refined to Amylamine (110-58-7) by ectification.

Toxicity Data With Reference

1.   

ipr-rat LDLo:37,500 µg/kg

   FATOAO    Farmakologiya i Toksikologiya (Moscow). 31 (1968),238.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Hazard Symbols: F;C (Flammable; Corrosive) 
Risk Codes: R11;R20/21/22;R34 (Highly flammable; Harmful by inhalation, in contact with skin and if swallowed; Causes burns.)
Safety Description: S16;S26;S36/37/39;S45 (Keep away from sources of ignition; In case of contact with eyes, rinse immediately with plenty of water and seek medical advice; Wear suitable protective clothing, gloves and eye/face protection; In case of accident or if you feel unwell, seek medical advice immediately) 
Transport Information: UN 1106
Poison by intraperitoneal route. A corrosive. A flammable liquid. When heated to decomposition it emits toxic vapors of NOx.

Standards and Recommendations

DOT Classification:  8; Label: Corrosive, Flammable Liquid (UN 2734); DOT Class: 3; Label: Flammable Liquid, Corrosive (UN 2733)
PURITY (GC): 98.0% min
SPECIFIC GRAVITY: 0.75 - 0.76
MOISTURE: 0.1% max
COLOR (AHHA): 30 max

Specification

STORAGE: Store with flammable liquids. Store outside or in a detached building. Keep separated from incompatible substances. Protect from physical damage.  Avoid heat, flames, sparks and other sources of ignition.