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118-10-5

Basic Information
CAS No.: 118-10-5
Name: Cinchonine
Article Data: 21
Molecular Structure:
Molecular Structure of 118-10-5 (Cinchonine)
Formula: C19H22N2O
Molecular Weight: 294.396
Synonyms: (S)-[(5R,7R)-5-ethenyl-1-azabicyclo[2.2.2]oct-7-yl]-quinolin-4-yl-methanol;Quinoline alkaloid;.alpha.-Quinidine;Prestwick_501;(9S)-Cinchonan-9-ol;(S)-[(4R,5S,7S)-5-ethenyl-1-azoniabicyclo[2.2.2]oct-7-yl]-quinolin-4-yl-methanol;[(5S,7R)-5-ethenyl-1-azabicyclo[2.2.2]oct-7-yl]-quinolin-4-yl-methanol;D-Cinchonine;Cinchonan-9-ol, (9S)-;2-Quinuclidinemethanol, .alpha.-(5-vinyl-2-quinolyl)-;4-quinolyl(5-vinyl-1-azabicyclo[2.2.2]oct-2-yl)methanol;(+)-Cinconine;
EINECS: 204-234-6
Density: 1.2 g/cm3
Melting Point: 256-266 °C
Boiling Point: 464.5 °C at 760 mmHg
Flash Point: 234.7 °C
Solubility: insoluble in water
Appearance: white to light yellow crystal powder
Hazard Symbols: HarmfulXn
Risk Codes: 20/21/22
Safety: 26-36-36/37
PSA: 36.36000
LogP: 3.10250
Synthetic route
189309-24-8

O-tosylcinchonine

A

1393446-38-2

(Z)-1-(quinolin-4-yl)-3-((3R,4R)-3-vinylpiperidin-4-yl)prop-1-enyl 4-methylbenzene sulfonate

B

118-10-5

Cinchonin

Conditions
ConditionsYield
With salicylic acid In ethylene glycol at 95℃; for 0.5h; Microwave irradiation;A 60%
B 15%
C 15%
560119-43-9

methanesulfonic acid (quinolin-4-yl)(5-vinyl-1-azabicyclo[2.2.2]oct-2-yl)methyl ester

A

118-10-5

Cinchonin

C

560119-45-1

(1S,2R,3S,5S,6R)-2-(quinolin-4-yl)-6-vinyl-1-azabicyclo[3.2.2]nonan-3-ol

D

(E)-cinchene

Conditions
ConditionsYield
With water; tartaric acid at 100℃; Title compound not separated from byproducts;A n/a
B n/a
C 48%
D 1%
64-19-7

acetic acid

iron powder

iron powder

118-10-5

Cinchonin

64-17-5

ethanol

sodium

sodium

118-10-5

Cinchonin

14402-57-4

benzoylcinchonine

alcoholic KOH-solution

alcoholic KOH-solution

A

65-85-0

benzoic acid

B

118-10-5

Cinchonin

Conditions
ConditionsYield
at 60 - 70℃;

(9S,10Ξ)-10-iodo-10,11-dihydro-cinchonan-9-ol; dihydriodide hydrate

water

water

A

118-10-5

Cinchonin

B

7299-23-2

9,10-Epoxy-10,11-dihydro-cinchonan

C

apocinchonine

apocinchonine

Conditions
ConditionsYield
at 150 - 160℃; im Rohr; isomer(ic) I;
118-10-5

Cinchonin

1609-86-5

Tert-butyl isocyanate

(9S)-9-deoxy-cinchonin-9-yl tert-butylcarbamate

Conditions
ConditionsYield
With dibutyltin(II) dilaurate In toluene at 110℃; for 48h;99%
917-54-4

methyllithium

118-10-5

Cinchonin

2'-methylcinchonine

Conditions
ConditionsYield
In tetrahydrofuran at -10 - 50℃; for 6h; Inert atmosphere; Schlenk technique;99%
In tetrahydrofuran at -78.16℃; for 12h; Inert atmosphere;
24463-19-2

anthracenylmethyl chloride

118-10-5

Cinchonin

(2R,5R,1'S)-1-(9-anthracenyl)methyl-5-ethylene-2-[1-hydroxy-1-(quinol-4-yl)]methyl-1-azoniabicyclo[2.2.2]octane chloride

Conditions
ConditionsYield
In toluene at 110℃; for 2h;98%
In toluene Reflux;94%
In toluene for 24h; Heating;80%

(1E,4E)-1,5-bis(4-(bromomethyl)phenyl)penta-1,4-dien-3-one

118-10-5

Cinchonin

C57H60N4O3(2+)*2Br(1-)

Conditions
ConditionsYield
In tetrahydrofuran; N,N-dimethyl-formamide Reflux;98%
Raw Materials
71-41-0
118-10-5
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Chemistry

The molecular formula of Cinchonine(118-10-5) is C19H22N2O and its formula weight is 294.39.
Cinchonine(118-10-5) has a melting point of  260-263 °C.
The chemical synonyms of Cinchonine(118-10-5) are D-CINCHONINE;(+)-CINCHONINE;CINCHONINE;CINCHONAN-9-OL,(9S)-;(+)-cinconine;(8r,9s)-cinchonine;(9s)-cinchonan-9-o;(9S)-Cinchonan-9-ol
The molecular structure of Cinchonine(118-10-5):

Toxicity Data With Reference

1.   

ipr-rat LD50:152 mg/kg

   APTOA6    Acta Pharmacologica et Toxicologica. 4 (1948),265.
2.   

scu-mus LDLo:400 mg/kg

   AEPPAE    Naunyn-Schmiedeberg’s Archiv fuer Experimentelle Pathologie und Pharmakologie. 205 (1948),129.
3.   

scu-frg LDLo:200 mg/kg

   AEPPAE    Naunyn-Schmiedeberg’s Archiv fuer Experimentelle Pathologie und Pharmakologie. 205 (1948),129.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Poison by intraperitoneal and subcutaneous routes. When heated to decomposition it emits toxic fumes of NOx.
Hazard Codes  Xn
Risk Statements  20/22-20/21/22
Safety Statements  26-36-36/37
RIDADR  1544
WGK Germany  3
RTECS  GD3500000
F  8-34
HazardClass  6.1(b)
PackingGroup  III

Specification

Chemical Stability: Stable under normal temperatures and pressures. 
Conditions to Avoid: Incompatible materials, light. 
Incompatibilities with Other Materials Strong oxidizing agents, strong reducing agents, strong bases. 
Hazardous Decomposition Products Nitrogen oxides, carbon monoxide, oxides of sulfur, carbon dioxide. 
Hazardous Polymerization Has not been reported. 
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