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Basic Information
CAS No.: 128-58-5
Name: Vat Green 1
Molecular Structure:
Molecular Structure of 128-58-5 (Vat Green 1)
Formula: C36H20O4
Molecular Weight: 516.552
Synonyms: CaledonJade Green XN (6CI);Ahcovat Jade Green B;Ahcovat Printing Jade Green B;Amanthrene Green JF;Belanthrene Jade Green;Benzadone Jade GreenX;Benzadone Jade Green XBN;Brilliant Green S;C.I. Pigment Green 47;Calcoloid Jade Green N;Calcoloid Jade GreenNP;Caledon Jade Green XBN;Caledon Printing Jade Green XN;CarbanthreneBrilliant Green G;Cibanone Brilliant Green FBF;Dimethoxyviolanthrone;Indanthrene BrilliantGreen BN;Indanthrene Green FFB;Mikethrene Brilliant Green B;Mikethrene Brilliant Green FFB Superfine;Navinon Green FFB;PalanthreneJade Green;Paradone JadeGreen B New;Pigment Green 47;
EINECS: 204-896-6
Density: 1.455 g/cm3
Boiling Point: 521.39°C (rough estimate)
Appearance: solid
PSA: 52.60000
LogP: 8.17720
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Synthetic route
6535-67-7

2-methoxy-benz[de]anthracen-7-one

128-58-5

Jade Green XBN

Conditions
ConditionsYield
With potassium hydroxide; ethanol at 130 - 140℃; Behandeln des Reaktionsprodukts mit Luft;
With potassium hydroxide; potassium chlorate; potassium acetate at 125℃; Reagens 4:Methanol; Reagens 5:Naphtalin; anschlissendes Erhitzen auf 200grad und Behandeln einer Suspension des Reaktionsprodukts in Wasser mit Luft;
116-71-2

isoviolanthrone

80-48-8

methyl p-toluene sulfonate

128-58-5

Jade Green XBN

Conditions
ConditionsYield
With tetralin; sodium carbonate auf Siedetemperatur;
With potassium carbonate; 1,2,3-trichlorobenzene unter Zusatz von Phenol, Naphthol-(1) oder Hydrochinon auf 180grad;
With sodium carbonate; 1,2,3-trichlorobenzene unter Zusatz von Phenol, Naphthol-(1) oder Hydrochinon auf 180grad;
116-71-2

isoviolanthrone

77-78-1

dimethyl sulfate

128-58-5

Jade Green XBN

Conditions
ConditionsYield
With potassium carbonate; 1,2,3-trichlorobenzene unter Zusatz von Phenol, Naphthol-(1) oder Hydrochinon auf 180grad;
With sodium carbonate; 1,2,3-trichlorobenzene unter Zusatz von Phenol, Naphthol-(1) oder Hydrochinon auf 180grad;
77-78-1

dimethyl sulfate

16.17-dihydroxy-violanthrenedione-(5.10)

16.17-dihydroxy-violanthrenedione-(5.10)

128-58-5

Jade Green XBN

Conditions
ConditionsYield
With potassium carbonate; nitrobenzene
77-78-1

dimethyl sulfate

bz2.bz2'-dioxy-violanthrone

bz2.bz2'-dioxy-violanthrone

128-58-5

Jade Green XBN

Conditions
ConditionsYield
With sodium carbonate; nitrobenzene
7664-93-9

sulfuric acid

3951-01-7

16,17-dimethoxy-anthra[9,1,2-cde]benzo[rst]pentaphene-5,10-diol

128-58-5

Jade Green XBN

5,10-bis-(5-carboxy-valeryloxy)-16,17-dimethoxy-anthra[9,1,2-cde]benzo[rst]pentaphene

aqueous alkaline solution

aqueous alkaline solution

air

air

128-58-5

Jade Green XBN

...Expand
67764-33-4

cyclopentyl nitrite

5,10-bis-(5-carboxy-valeryloxy)-16,17-dimethoxy-anthra[9,1,2-cde]benzo[rst]pentaphene

aqueous alkaline solution

aqueous alkaline solution

mineral acid

mineral acid

128-58-5

Jade Green XBN

...Expand
108-31-6

maleic anhydride

128-58-5

Jade Green XBN

(16.17-dimethoxy-anthra[9.1.2-cde]benzo[rst]pentaphenediyl-(5.10))-bis-hydrogen maleate

Conditions
ConditionsYield
With pyridine; copper at 70℃; unter Kohlendioxyd; anschliessendes Erwaermen auf 100grad;
128-58-5

Jade Green XBN

3951-01-7

16,17-dimethoxy-anthra[9,1,2-cde]benzo[rst]pentaphene-5,10-diol

Conditions
ConditionsYield
With sodium hydroxide; sodium dithionite at 50℃;
With sodium hydroxide; sodium dithionite; sodium hydrogensulfite at 55 - 60℃;
Raw Materials
77-78-1
6535-67-7
116-71-2
80-48-8
7664-93-9
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Chemistry

CAS: 128-58-5
EINECS: 204-896-6
Product Categories: Organics
Following is the Molecular Structure of Jade green base (CAS NO.128-58-5):

SMILES: O=C2c9c1c8c(c(OC)cc1c3ccccc23)c6c(OC)cc5c4ccccc4C(=O)c7c5c6c(cc7)c8cc9
InChI: InChI=1/C36H20O4/c1-39-27-15-25-17-7-3-5-9-21(17)35(37)23-13-11-19-20-12-14-24-30-26(18-8-4-6-10-22(18)36(24)38)16-28(40-2)34(32(20)30)33(27)31(19)29(23)25/h3-16H,1-2H3
InChIKey: JXUKQCUPTNLTCS-UHFFFAOYAK
Std.InChI: InChI=1S/C36H20O4/c1-39-27-15-25-17-7-3-5-9-21(17)35(37)23-13-11-19-20-12-14-24-30-26(18-8-4-6-10-22(18)36(24)38)16-28(40-2)34(32(20)30)33(27)31(19)29(23)25/h3-16H,1-2H3
Std.InChIKey: JXUKQCUPTNLTCS-UHFFFAOYSA-N
Molecular Formula: C36H20O4
Molecular Weight: 516.54
Molar Volume: 354.8 cm3
Density: 1.455g/cm3
Molar Refractivity: 159.01cm3
Index of Refraction: 1.853
Surface Tension: 74.3dyne/cm

Toxicity Data With Reference

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
rat LD50 intraperitoneal 2600mg/kg (2600mg/kg) BEHAVIORAL: SOMNOLENCE (GENERAL DEPRESSED ACTIVITY)

BEHAVIORAL: ATAXIA

LUNGS, THORAX, OR RESPIRATION: OTHER CHANGES		 Gigiena i Sanitariya. For English translation, see HYSAAV. Vol. 52(10), Pg. 88, 1987.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

 Jade green base (CAS NO.128-58-5) is an eye irritant.When heated to decomposition it emits acrid smoke and fumes.

Specification

 Jade green base (CAS NO.128-58-5),which also can be called for Brilliant Green S ; Mayvat Jade Green ; Caledon Jade Green ; Dimethoxyviolanthrone ; Helanthrene Green B ; Zelen kypova 1 ; Amanthrene Green JF ; Mikethrene Green FFB ; Ostanthren Green FFB . Jade green base (CAS NO.128-58-5) is a solid, it's stable and incompatible with strong oxidizing agents. It's insoluble in water, Alcohol , Chloroform , Toluene ,slightly soluble in Acetone , O-chlorophenol  and Nitrobenzene , Pyridine (heat).