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Basic Information
CAS No.: 1451-83-8
Name: 2-bromo-3-methylpropiophenone
Article Data: 13
Molecular Structure:
Molecular Structure of 1451-83-8 (2-bromo-3-methylpropiophenone)
Formula: C10H11 Br O
Molecular Weight: 227.101
Synonyms: Propiophenone,2-bromo-3'-methyl- (7CI,8CI)
Density: 1.357±0.06 g/cm3(Predicted)
Boiling Point: 134-135 °C(Press: 8 Torr)
PSA: 17.07000
LogP: 2.96110
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Synthetic route
51772-30-6

3'-Methylpropiophenone

1451-83-8

2-bromo-1-(3-methylphenyl)propan-1-one

Conditions
ConditionsYield
With bromine In dichloromethane at 20℃; for 0.5h;100%
With bromine In dichloromethane for 10h; Inert atmosphere;59%
Stage #1: 3'-Methylpropiophenone With bromine In dichloromethane for 10h; Inert atmosphere;
Stage #2: In dichloromethane		59%
108-88-3

toluene

1451-83-8

2-bromo-1-(3-methylphenyl)propan-1-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: aluminum (III) chloride / dichloromethane
2: bromine / dichloromethane
View Scheme
1451-83-8

2-bromo-1-(3-methylphenyl)propan-1-one

75-64-9

tert-butylamine

1193779-18-8

2-(N-tert-butylamino)-3'-methylpropiophenone

Conditions
ConditionsYield
at 70℃; for 2h;98%
at 70℃; for 2h;98%
1451-83-8

2-bromo-1-(3-methylphenyl)propan-1-one

536-74-3

phenylacetylene

2,7-dimethyl-2-(1-oxo-1-(m-tolyl)propan-2-yl)-4-phenylnaphthalen-1(2H)-one

Conditions
ConditionsYield
With 1,10-Phenanthroline; tetrakis(actonitrile)copper(I) hexafluorophosphate; potassium carbonate In toluene at 120℃; for 16h; Schlenk technique; Inert atmosphere;63%
With 1,10-Phenanthroline; tetrakis(actonitrile)copper(I) hexafluorophosphate; potassium carbonate In toluene at 120℃; for 16h; Schlenk technique; Sealed tube; Inert atmosphere;63%
1451-83-8

2-bromo-1-(3-methylphenyl)propan-1-one

765-30-0

Cyclopropylamine

2-(cyclopropylamino)-1-(3’-tolyl)-1-oxopropane

Conditions
ConditionsYield
In tetrahydrofuran at 50℃; for 18h; Sealed tube;45%
1451-83-8

2-bromo-1-(3-methylphenyl)propan-1-one

141-43-5

ethanolamine

1350768-23-8

PAL-589

Conditions
ConditionsYield
In acetonitrile at 20 - 40℃; Inert atmosphere;20%
1451-83-8

2-bromo-1-(3-methylphenyl)propan-1-one

75-31-0

isopropylamine

(+/-)-1-Isopropylamino-1-<3-methyl-benzoyl>-aethan

Conditions
ConditionsYield
In acetonitrile at 20℃; for 7h;
1451-83-8

2-bromo-1-(3-methylphenyl)propan-1-one

(+/-)-threo-1-(3'-methylphenyl)-1-oxy-brompropan

Conditions
ConditionsYield
With sodium tetrahydroborate In methanol
123-75-1

pyrrolidine

1451-83-8

2-bromo-1-(3-methylphenyl)propan-1-one

1214940-01-8

2-(N-pyrrolidinyl)-3'-methylpropiophenone

Conditions
ConditionsYield
In water; acetonitrile at 20℃; for 4h;
1451-83-8

2-bromo-1-(3-methylphenyl)propan-1-one

1003-03-8

Cyclopentamine

1214939-96-4

2-(N-cyclopentylamino)-3'-methylpropiophenone

Conditions
ConditionsYield
In acetonitrile at 40℃; for 6h;226 mg
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