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15307-86-5

Basic Information
CAS No.: 15307-86-5
Name: Benzeneacetic acid,2-[(2,6-dichlorophenyl)amino]-
Molecular Structure:
Molecular Structure of 15307-86-5 (Benzeneacetic acid,2-[(2,6-dichlorophenyl)amino]-)
Formula: C14H11Cl2NO2
Molecular Weight: 296.15
Synonyms: Aceticacid, [o-(2,6-dichloroanilino)phenyl]- (8CI);Diclac;Diclofenac acid;Diclofenamic acid;Diclomelan;Dicloreuma;N-(2,6-Dichlorophenyl)-o-aminophenylacetic acid;Pennsaid;Voltaflan;[o-(2,6-Dichloroanilino)phenyl]acetic acid;
EINECS: 239-348-5
Density: 1.431 g/cm3
Melting Point: 156-158oC
Boiling Point: 412 ºC at 760 mmHg
Flash Point: 203 ºC
Solubility: 1.278mg/L(30 oC)
Appearance: White to yellowish crystalline powder
Hazard Symbols:
Risk Codes:
Safety:
Transport Information:
PSA: 49.33000
LogP: 4.43710
Synthetic route
934548-15-9

[2-(2,6-dichloro-phenylamino)-phenyl]-acetic acid diethylcarbamoylmethylcarbamoyloxymethyl ester

A

34105-57-2

2-amino-N,N-diethylacetamide

B

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
With human plasma In phosphate buffer at 37℃; pH=7.4;A n/a
B 100%
934548-16-0

[2-(2,6-dichloro-phenylamino)-phenyl]-acetic acid 1-diethylcarbamoyl-2-phenyl-ethylcarbamoyloxymethyl ester

A

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

B

40847-09-4

N-(phenylalanyl)-N,N-diethylamine

Conditions
ConditionsYield
With human plasma In phosphate buffer at 37℃; pH=7.4;A 100%
B n/a
15307-79-6

diclofenac sodium

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
With hydrogenchloride In water; acetone at 20 - 45℃; for 3h; pH=1.4 - 1.6; Solvent;99%
With hydrogenchloride In water Cooling with ice;90%
With hydrogenchloride In water at 0 - 20℃;70%
87-65-0

2,6-Dichlorophenol

methyl 2-(2-(2-bromopropionamido)phenyl)acetate

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
With potassium hydroxide In dimethyl sulfoxide at 60 - 100℃; for 8h; Temperature; Reagent/catalyst;95%
21789-06-0

N,N-dimethyl-o-(2,6-dichloroanilino)phenylacetamide

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
With potassium hydroxide In ethanol; water92.9%
70690-44-7

2-[(2,6-dichlorophenyl)-N-benzylamino]-phenylacetic acid

95-50-1

1,2-dichloro-benzene

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
In tetrahydrofuran; hexane; toluene91.2%
83281-95-2

2-<(2,6-dichlorophenyl)amino>-α-(methylthio)phenylacetic acid

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
With nickel In ethanol Heating;85%
15362-40-0

1-(2,6-dichlorophenyl)indolin-2-one

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
In hydrogenchloride; toluene liquid HCl;84.4%
26159-34-2

Naprelan

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
With hydrogenchloride In water at 20℃;82.2%
18698-97-0

ortho-bromophenylacetic acid

608-31-1

2,6-Dichloroaniline

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
With D-myo-inositol; copper; caesium carbonate In water at 100℃; for 30h;82%
2444-36-2

2'-chloro-benzeneacetic acid

608-31-1

2,6-Dichloroaniline

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
With copper(l) iodide; potassium carbonate; potassium iodide In 1,4-dioxane at 130 - 150℃; for 7h; Concentration; Solvent; Inert atmosphere;80%
With copper(l) iodide; potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 165℃; for 12h; Ullmann Condensation; Sealed tube;34%
With copper(I) chloride; potassium carbonate; potassium iodide In N,N-dimethyl-formamide; xylene at 150 - 152℃; for 5h;

rhodium(III) chloride

75294-57-4

o-(N-allyl-2,6-dichloroanilino)phenylacetic acid

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
In 1,2-dimethoxyethane; water; benzene72%
18698-97-0

ortho-bromophenylacetic acid

608-31-1

2,6-Dichloroaniline

111-46-6

diethylene glycol

A

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

B

C12H16O5

Conditions
ConditionsYield
With L-2-O-methyl-chiro-inositol; copper(II) acetate monohydrate; potassium carbonate at 110℃; for 12h; Inert atmosphere;A 72%
B 17%
40400-15-5

2-(2-iodophenyl)acetonitrile

608-31-1

2,6-Dichloroaniline

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
Stage #1: 2-(2-iodophenyl)acetonitrile With potassium hydroxide In ethanol at 80℃; for 12h; Inert atmosphere; Sealed tube;
Stage #2: 2,6-Dichloroaniline With copper(l) iodide; potassium carbonate In toluene at 100℃; for 12h; Inert atmosphere; Sealed tube;
70%
100754-92-5

potassium 2-iodophenylacetate

608-31-1

2,6-Dichloroaniline

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
With 1-methyl-pyrrolidin-2-one; copper(l) iodide; potassium carbonate at 100℃; Ullmann coupling;61%
137138-22-8

2-<(2,6-Dichlorphenacyl)amino>phenylessigsaeure-2-oxopropylester

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
With buffer pH 8.0 In 1,4-dioxane; acetonitrile at 57℃; half-life time of hydrolysis at different pH;

2-(4-morpholino)ethyl<(o-2,6 dichlorophenylanilino)phenyl acetate> hydrochloride

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
at 37℃; Rate constant; t1/2, simulated gastric fluid, rate plasma, further reagents, temperatures;

[2-(2,6-Dichloro-phenylamino)-phenyl]-acetic acid 3-morpholin-4-yl-propyl ester; hydrochloride

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
at 37℃; Rate constant; t1/2, simulated gastric fluid, rate plasma, further reagents;

[2-(2,6-Dichloro-phenylamino)-phenyl]-acetic acid 4-morpholin-4-yl-butyl ester; hydrochloride

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
at 37℃; Rate constant; t1/2, simulated gastric fluid, rate plasma, further reagents;

[2-(2,6-dichloro-phenylamino)-phenyl]-acetic acid (benzoyl-ethoxycarbonylmethyl-amino)-methyl ester

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
With NADPH-generating system; rat liver homogenate at 37℃; Enzyme kinetics; Hydrolysis; Enzymatic reaction;
15307-79-6

diclofenac sodium

A

59-48-3

2-oxoindole

B

87-65-0

2,6-Dichlorophenol

C

15362-40-0

1-(2,6-dichlorophenyl)indolin-2-one

D

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
In phosphate buffer at 45℃; Kinetics; Thermodynamic data; Further Variations:; pH-values; Temperatures;
89796-99-6

aceclofenac

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
With sodium hydroxide for 3h; Heating;
15307-93-4

N-phenyl-2,6-dichloroaniline

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: benzene / 6 h / Heating
2: 91 percent / m-chloroperbenzoic acid / CH2Cl2 / 1 h / Ambient temperature
3: 84 percent / p-toluenesulfonic acid / benzene / 0.5 h / Heating
4: 91 percent / 2N NaOH / ethanol / 48 h / Heating
5: 85 percent / Raney nickel / ethanol / Heating
View Scheme
Multi-step reaction with 5 steps
1: benzene / 6 h / Heating
2: N-chlorosuccinimide / CCl4 / 1 h / Ambient temperature
3: SnCl4 / CCl4 / 0.83 h / Ambient temperature
4: 91 percent / 2N NaOH / ethanol / 48 h / Heating
5: 85 percent / Raney nickel / ethanol / Heating
View Scheme
83281-93-0

N-(2,6-dichlorophenyl)-α-(methylthio)acetanilide

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 91 percent / m-chloroperbenzoic acid / CH2Cl2 / 1 h / Ambient temperature
2: 84 percent / p-toluenesulfonic acid / benzene / 0.5 h / Heating
3: 91 percent / 2N NaOH / ethanol / 48 h / Heating
4: 85 percent / Raney nickel / ethanol / Heating
View Scheme
Multi-step reaction with 4 steps
1: N-chlorosuccinimide / CCl4 / 1 h / Ambient temperature
2: SnCl4 / CCl4 / 0.83 h / Ambient temperature
3: 91 percent / 2N NaOH / ethanol / 48 h / Heating
4: 85 percent / Raney nickel / ethanol / Heating
View Scheme
83281-94-1

1-(2,6-dichlorophenyl)-3-(methylthio)oxindole

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 91 percent / 2N NaOH / ethanol / 48 h / Heating
2: 85 percent / Raney nickel / ethanol / Heating
View Scheme
83281-96-3

N-(2,6-dichlorophenyl)-α-(methylsulfinyl)acetanilide

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 84 percent / p-toluenesulfonic acid / benzene / 0.5 h / Heating
2: 91 percent / 2N NaOH / ethanol / 48 h / Heating
3: 85 percent / Raney nickel / ethanol / Heating
View Scheme

α-chloro-N-(2,6-dichlorophenyl)-α-(methylthio)acetanilide

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: SnCl4 / CCl4 / 0.83 h / Ambient temperature
2: 91 percent / 2N NaOH / ethanol / 48 h / Heating
3: 85 percent / Raney nickel / ethanol / Heating
View Scheme
1224508-84-2

4-((3,3-dimethylbutoxy)carbonyloxy)benzyl 2-(2-(2,6-dichlorophenylamino)phenyl)acetate

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

Conditions
ConditionsYield
With water at 37℃; pH=7.4; Kinetics;
5292-43-3

bromoacetic acid tert-butyl ester

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

139272-68-7

2-((2,6-dichlorophenyl)amino)phenylacetoxyacetic acid tert-butyl ester

Conditions
ConditionsYield
With sodium hydrogencarbonate In DMF (N,N-dimethyl-formamide) at 20℃;100%
15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

144830-14-8

(+)-O-Demethyltramadol

(+)-O-desmethyl-tramadol diclofenac salt

Conditions
ConditionsYield
With water In acetonitrile at 20℃; under 760.051 Torr; Product distribution / selectivity;100%
15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

73986-53-5, 80456-81-1, 144830-14-8, 144830-15-9

(±)-cis-2-[(dimethylamino)methyl]-1-(3-hydroxyphenyl)cyclohexanol

(rac)-O-desmethyl-tramadol diclofenac salt

Conditions
ConditionsYield
In isopropyl alcohol at 20℃; Product distribution / selectivity;100%
15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

73986-53-5

O-desmethyltramadol

O-desmethyl-tramadol-diclofenac

Conditions
ConditionsYield
In isopropyl alcohol at 20℃; Product distribution / selectivity;100%
15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

768-94-5

1-Adamantanamine

C10H17N*C14H11Cl2NO2

Conditions
ConditionsYield
In methanol at 20℃;100%
15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

2,2'-dimethyl-[1,1'-biphenyl]iodonium trifluoromethanesulfonate salt

C28H22Cl2INO2

Conditions
ConditionsYield
With copper diacetate; sodium carbonate; (3aR,3a'R,8aS,8a'S)-2,2'-(propane-2,2-diyl)bis(8,8a-dihydro-3aH-indeno[1,2-d]oxazole) In dichloromethane; water at 30℃; for 12h; enantioselective reaction;99%
15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

C10H20N2O2S

C24H29Cl2N3O3S

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0℃; for 0.5h; Acylation;98%
15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

4407-36-7

(2E)-3-phenyl-2-propen-1-ol

cinnamyl 2-(2-(2,6-dichlorophenylamino)phenyl)acetate

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide at 20℃; for 4h;98%
15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

18107-18-1

diazomethyl-trimethyl-silane

15307-78-5

2-[(2,6-dichlorophenyl)amino]phenylacetic acid methyl ester

Conditions
ConditionsYield
In methanol; hexane; benzene at 25℃; for 1h;96%
With methanol In Dimethyl ether
67-56-1

methanol

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

15307-78-5

2-[(2,6-dichlorophenyl)amino]phenylacetic acid methyl ester

Conditions
ConditionsYield
With sulfuric acid for 0.25h; Reflux;96%
Stage #1: methanol; [2-(2,6-dichloroanilino)phenyl]acetic acid With hydrogenchloride In water for 6h; Reflux;
Stage #2: With sodium carbonate In water
91%
Stage #1: methanol; [2-(2,6-dichloroanilino)phenyl]acetic acid With hydrogenchloride In water for 6h; Reflux;
Stage #2: With sodium hydrogencarbonate In water Cooling with ice; Saturated solution;
91%
6066-82-6

1-hydroxy-pyrrolidine-2,5-dione

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

104425-36-7

acetic acid N-oxysuccinimide ester

Conditions
ConditionsYield
With dicyclohexyl-carbodiimide In 1,4-dioxane for 8h; Ambient temperature;95%
With dicyclohexyl-carbodiimide In dichloromethane for 1h;90%
With dicyclohexyl-carbodiimide In tetrahydrofuran at 5℃;
Stage #1: 1-hydroxy-pyrrolidine-2,5-dione; [2-(2,6-dichloroanilino)phenyl]acetic acid In tetrahydrofuran at 0 - 5℃; for 0.166667h; Inert atmosphere;
Stage #2: With dicyclohexyl-carbodiimide In tetrahydrofuran at 20℃; Inert atmosphere;
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; Inert atmosphere;
49715-04-0

chlorosulfuric acid chloromethyl ester

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

chloromethyl 2-(2-((2,6-dichlorophenyl)amino)phenyl)acetate

Conditions
ConditionsYield
With tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate In dichloromethane; water at 20℃; for 1h;95%
With Bu4HSO4 In dichloromethane; water at 20℃; for 1h;
15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

1528768-73-1

(5-methyl-2-phenyl-1,3-dioxan-5-yl)methyl 4-hydroxybenzoate

1528768-90-2

(5-methyl-2-phenyl-1,3-dioxan-5-yl)methyl 4-(2-(2-((2,6-dichlorophenyl)amino)phenyl)acetoxy)benzoate

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In tetrahydrofuran; dichloromethane at 0 - 20℃; for 18h;95%
15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

255735-88-7

[(2R)-2-aminopropyl]carbamic acid,1,1-dimethylethyl ester

Boc-propylamide-diclofenac

Conditions
ConditionsYield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 1.5h; Cooling with ice;95%
15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

15362-40-0

1-(2,6-dichlorophenyl)indolin-2-one

Conditions
ConditionsYield
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 0.5h;94%
With thionyl chloride In dichloromethane; ethyl acetate at 50℃; for 2h; Concentration; Temperature;92%
With hydrogenchloride In acetonitrile at 78.85℃; for 5h; Rate constant; Kinetics; Mechanism; energy data: ΔH(activ.), ΔS(activ.); ΔE(activ.)var. amount of acetonitrile, var. temp.;
15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

306776-45-4

3-{Methyl{[(nitrosothio)cyclohexyl]methyl}amino)propan-1-ol

3-{Methyl{[(nitrosothio)cyclohexyl]methyl}amino)propyl 2-{2-[(2,6-dichlorophenyl)amino]phenyl}acetate

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0℃; for 0.5h; Acylation;94%
15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

109-89-7

diethylamine

diclofenac diethylamine

Conditions
ConditionsYield
In acetone at 50 - 55℃; for 2h; pH=8.5 - 10.0;93.7%
2916-31-6

2,2-dimethyl-1,3-dioxolane

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

A

15362-40-0

1-(2,6-dichlorophenyl)indolin-2-one

B

5-(2,6-dichloro-phenyl)-6,6-dimethyl-5,9-dihydro-6H-7-oxa-5-aza-benzocyclohepten-8-one

Conditions
ConditionsYield
With toluene-4-sulfonic acid In ethanol Cyclization;A n/a
B 93%
2955-88-6

1-pyrrolidineethanol

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

diclofenac epolamine

Conditions
ConditionsYield
In acetone92%
528-43-8

Magnolol

15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

5,5'-diallyl-2'-hydroxy-[1,1'-biphenyl]-2-yl-2-(2-((2,6-dichlorophenyl)amino)phenyl) acetate

Conditions
ConditionsYield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 1h;92%
With dmap In dichloromethane at 25 - 30℃;92%
15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

2-fluoro-1-phenyl-2-(pyrimidin-2-ylsulfonyl)ethan-1-one

2-((2,6-dichlorophenyl)amino)phenethyl (Z)-4-((1-fluoro-2-phenyl-2-(pyrimidin-2-yloxy)vinyl)sulfonyl)butanoate

Conditions
ConditionsYield
With tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine In N,N-dimethyl acetamide at 100℃; for 12h; Inert atmosphere; Molecular sieve;92%
15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

159982-36-2

2-ethyl-2-(nitrosothio)butan-1-ol

C20H22Cl2N2O3S

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0℃; for 0.5h; Acylation;91%
15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

141-43-5

ethanolamine

diclofenac/monoethanolamine

Conditions
ConditionsYield
In acetone90%
15307-86-5

[2-(2,6-dichloroanilino)phenyl]acetic acid

139115-91-6

2-(2-tert-butyloxycarbonylaminoethoxy)ethanol

1133407-62-1

[2-(2,6-dichlorophenylamino)phenyl]acetic acid 2-(2-tert-butoxycarbonylaminoethoxy)ethyl ester

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 1h;90%
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane for 4h; Cooling with ice;1.166 g
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 35℃; for 2h;2.44 g
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    15307-86-5

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    15307-86-5

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    Business Type:Trading Company

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    Business Type:Lab/Research institutions

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    15307-86-5

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    15307-86-5

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    15307-86-5

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

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    Address:13th Floor, Tower B, Century Plaza, Zhongnan Road, Wuchang District, Wuhan, China.

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86 15868163694

    Address:Room 622, Building 11, Yifeng City, Nanyuan Street, Yuhang District

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    15307-86-5

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    Business Type:Trading Company

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    Address:Room 302, 47 Changping Street, Chaoyang District, Changchun, Jilin Province,China

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    15307-86-5

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    AFINE CHEMICALS LIMITED is specialized in the fine chemicals and pharmaceuticals and we have enjoyed great popularity in world markets. Since 2005, we have been rapidly growing to

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-85134551

    Address:No. 206 Zhen Hua Road, Hangzhou 310030, Zhejiang, China

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    Zhengzhou Efelt Chemical Products Co., Ltd. is a high-tech enterprise specializing in the production, development and technology transfer services of fine chemicals, pharmaceut

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    Business Type:Lab/Research institutions

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    15307-86-5

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    Business Type:Trading Company

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    15307-86-5

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    Business Type:Lab/Research institutions

    Tel:18369939125

    Address:95A, Xingyuan East Road, Zhangdian District

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    15307-86-5

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    Business Type:Lab/Research institutions

    Tel:+86-371-86658258

    Address:Building 3 of Innovation Park, East District of the National University Science Park

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    15307-86-5

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    Business Type:Lab/Research institutions

    Tel:+86-571-87396432

    Address:No.200 Zhenhua Rd.Xihu Industrial Park, Hangzhou 310030, China

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    15307-86-5

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

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    Address:shandong qingdao

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    15307-86-5

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    Address:Room1701, Tianxing Building,Licheng district, jinan, Shandong, China

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    15307-86-5

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    Business Type:Trading Company

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    15307-86-5

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    Business Type:Other

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    Address:No.31 Pingshan South Road, HaiCang District, Xiamen, China

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    15307-86-5

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-371-65511936

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    15307-86-5

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    Topbatt Chemical Co., Ltd., Established in 2019, located in Shenzhen, Guangdong Province, is a Manufacturer and Trading company which specialized in fine chemicals like Pharmaceutical Reference Standards and Stable Isotopes. Our Stable Isotopes pro

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-755-86210921

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    15307-86-5

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    Wuhan Lwax Pharma Tech Co.,LTD dedicated to the development, production and marketing of chemicals which is specialized in Organic compounds; Active Pharmaceutical Ingredient(s); N

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    15307-86-5

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    Tel:+86-29-86106815

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    15307-86-5

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    China (Mainland)  |  Contact Details

    Business Type:Trading Company

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    15307-86-5

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     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

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    Address:Zhang zhe, guangzong county, xingtai city, hebei province

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  • 1-(2,6-Dichlorophenyl)-2-indolinone cas 15307-86-5CAS NO.: 15307-86-5

  • Casno:

    15307-86-5

    1-(2,6-Dichlorophenyl)-2-indolinone cas 15307-86-5CAS NO.: 15307-86-5

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Specification

The IUPAC name of Benzeneacetic acid,2-[(2,6-dichlorophenyl)amino]- is 2-[2-(2,6-dichloroanilino)phenyl]acetic acid. With the CAS registry number 15307-86-5, it is also named as Diclofenac. The product's categories are Indoles and Derivatives; Pharmacetical. It is a non-steroidal anti-inflammatory drug which originated from Ciba-Geigy (now Novartis) in 1973. And it was first introduced in the UK in 1979. Additioanlly, this drug may be supplied as either the sodium or potassium salt in the United Kingdom, India, Brazil and the United States. And most often as the sodium salt in China.

The other characteristics of this product can be summarized as: (1)ACD/LogP: 4.55; (2)# of Rule of 5 Violations: 0; (3)ACD/LogD (pH 5.5): 3.206; (4)ACD/LogD (pH 7.4): 1.437; (5)ACD/BCF (pH 5.5): 76.63; (6)ACD/BCF (pH 7.4): 1.305; (7)ACD/KOC (pH 5.5): 322.878; (8)ACD/KOC (pH 7.4): 5.501; (9)#H bond acceptors: 3; (10)#H bond donors: 2; (11)#Freely Rotating Bonds: 4; (12)Index of Refraction: 1.662; (13)Molar Refractivity: 76.531 cm3; (14)Molar Volume: 206.819 cm3; (15)Polarizability: 30.339×10-24 cm3; (16)Surface Tension: 57.998 dyne/cm; (17)Enthalpy of Vaporization: 70.067 kJ/mol; (18)Vapour Pressure: 0 mmHg at 25°C; (19)Rotatable Bond Count: 4; (20)Exact Mass: 295.016684; (21)MonoIsotopic Mass: 295.016684; (22)Topological Polar Surface Area: 49.3; (23)Heavy Atom Count: 19; (24)Complexity: 304.

Uses of Benzeneacetic acid,2-[(2,6-dichlorophenyl)amino]-: It is used to reduce inflammation and as an analgesic reducing pain in conditions such as arthritis or acute injury. It can also be used to reduce menstrual pain, dysmenorrhea. What's more, this drug is often used to treat chronic pain associated with cancer, particularly if inflammation is also present. It is used for musculoskeletal complaints. The Benzeneacetic acid,2-[(2,6-dichlorophenyl)amino]- is better tolerated NSAIDs. Though 20% of patients on long-term treatment experience side effects, only 2% have to discontinue the drug.   

People can use the following data to convert to the molecule structure. 
1. SMILES:c1ccc(c(c1)CC(=O)O)Nc2c(cccc2Cl)Cl
2. InChI:InChI=1/C14H11Cl2NO2/c15-10-5-3-6-11(16)14(10)17-12-7-2-1-4-9(12)8-13(18)19/h1-7,17H,8H2,(H,18,19)

The following are the toxicity data which has been tested.

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
man TDLo intramuscular 1070ug/kg (1.07mg/kg) SKIN AND APPENDAGES (SKIN): "DERMATITIS, OTHER: AFTER SYSTEMIC EXPOSURE" Annals of Internal Medicine. Vol. 117, Pg. 1058, 1992.
man TDLo oral 29mg/kg (29mg/kg) BLOOD: "CHANGES IN SERUM COMPOSITION (E.G., TP, BILIRUBIN, CHOLESTEROL)" Journal of Toxicology, Clinical Toxicology. Vol. 33, Pg. 173, 1995.
mouse LD50 intraperitoneal 345mg/kg (345mg/kg)   Arzneimittel-Forschung. Drug Research. Vol. 43, Pg. 44, 1993.
mouse LD50 oral 170mg/kg (170mg/kg)   Pharmazie. Vol. 37, Pg. 148, 1982.
rat LD50 oral 62500ug/kg (62.5mg/kg)   Arzneimittel-Forschung. Drug Research. Vol. 30, Pg. 1398, 1980.