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CAS No.: | 3006-93-7 |
---|---|
Name: | N,N'-1,3-Phenylene bismaleimide |
Article Data: | 14 |
Molecular Structure: | |
Formula: | C14H8N2O4 |
Molecular Weight: | 268.229 |
Synonyms: | N,N-m-phenylenedimaleimide;Maleimide,N,N'-m-phenylenedi- (6CI,7CI,8CI);1,1'-(1,3-Phenylene)bis[1H-pyrrole-2,5-dione];1,3-Bismaleimidobenzene;1,3-Dimaleimidobenzene;1,3-Phenylenebismaleimide;Actor PBM-R;BMI 3000;BMI-MP;Burnock PM;HVA 2;N,N'-1,3-Phenylenebismaleimide;N,N'-1,3-Phenylenedimaleimide;N,N'-m-Phenylenebis[maleimide];N,N'-m-Phenylenedimaleimide;NSC 19639;PMI;SR 525;SR 525A;Sanfel BM-G;Sumifine BM;Sumilizer BM;Vanax MBM;Vulkanox PM;Vulnoc PM;Vulnoc PM-P;m-Dimaleimidobenzene;m-Phenylenebismaleimide;m-Phenylenedimaleimide; |
EINECS: | 221-112-8 |
Density: | 1.567 g/cm3 |
Melting Point: | 198-201 °C(lit.) |
Boiling Point: | 499.3 °C at 760 mmHg |
Flash Point: | 250.7 °C |
Solubility: | negligible soluble in water |
Appearance: | yellow crystalline powder |
Hazard Symbols: | Xi, T, T+ |
Risk Codes: | 23/24/25-36/37/38-26-22 |
Safety: | 27-28-36/37/39-45-38-28A |
Transport Information: | UN 2811 6.1/PG 2 |
PSA: | 74.76000 |
LogP: | 0.67540 |
maleic anhydride
magnesium(II) acetate tetrahydrate
N,N'-(1,3-phenylene)dimaleimide
Conditions | Yield |
---|---|
With acetic anhydride In water; acetone | 84% |
N,N'-(1,3-phenylene)dimaleimide
Conditions | Yield |
---|---|
With sodium acetate; acetic anhydride |
Conditions | Yield |
---|---|
In ethyl acetate; toluene at 60℃; for 5h; Time; Temperature; |
N,N'-(1,3-phenylene)dimaleimide
Conditions | Yield |
---|---|
With sulfuric acid; toluene-4-sulfonic acid Reflux; |
5-p-tolyloxy-furan-2-carboxylic acid
N,N'-(1,3-phenylene)dimaleimide
C36H24N2O6
Conditions | Yield |
---|---|
With trifluoroacetic acid In chloroform-d1 at 100℃; | 96% |
N,N'-(1,3-phenylene)dimaleimide
Conditions | Yield |
---|---|
With tetrahexylammonium bromide; sodium carbonate In dichloromethane at 20℃; for 0.133333h; diastereoselective reaction; | 92% |
N,N'-(1,3-phenylene)dimaleimide
Conditions | Yield |
---|---|
With silver orthophosphate; cobalt(II) diacetate tetrahydrate; sodium pivalate In 1,2-dichloro-ethane at 140℃; for 24h; Inert atmosphere; Sealed tube; | 84% |
Conditions | Yield |
---|---|
With benzoic acid; L-proline In toluene at 80℃; for 15h; | 83% |
2-vinyloxy-1,3-butadiene
N,N'-(1,3-phenylene)dimaleimide
1,3-bis-(4-vinyloxy-Δ4-tetrahydrophthalimido)benzene
Conditions | Yield |
---|---|
at 100℃; for 0.5h; | 76.1% |
N,N'-(1,3-phenylene)dimaleimide
phenylhydrazone of ethyl ester of glyoxalic acid
Conditions | Yield |
---|---|
With copper(l) chloride In N,N-dimethyl-formamide at 80℃; for 2h; | 76% |
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IUPAC Name: 1-[3-(2,5-Dioxopyrrol-1-yl)phenyl]pyrrole-2,5-dione
Synonyms of 1,3-Bismaleimido benzene (CAS NO.3006-93-7): 1,3-Bismaleimidobenzene ;1,3-Dimaleimidobenzene ; 1,3-Phenylenebismaleimide ;1H-Pyrrole-2,5-dione, 1,1'-(phenylene)bis- ; N,N'-(m-Phenylene)bismaleimide ; N,N'-1,3-Phenylenedimaleimide ; N,N'-m-Phenylenemaleimide
CAS NO: 3006-93-7
Molecular Formula: C14H8N2O4
Molecular Weight: 268.23
Molecular Structure:
EINECS: 221-112-8
H bond acceptors: 6
H bond donors: 0
Freely Rotating Bonds: 2
Polar Surface Area: 74.76 Å2
Index of Refraction: 1.703
Molar Refractivity: 66.39 cm3
Molar Volume: 171 cm3
Surface Tension: 80.2 dyne/cm
Density: 1.567 g/cm3
Flash Point: 250.7 °C
Enthalpy of Vaporization: 76.77 kJ/mol
Boiling Point: 499.3 °C at 760 mmHg
Vapour Pressure: 4.2E-10 mmHg at 25°C
Melting point:198-201 °C(lit.)
Storage temp: Poison room
Water Solubility: negligible soluble
Appearance: yellow crystalline powder
Product Categories of 1,3-Bismaleimido benzene (CAS NO.3006-93-7): Curing Agent;N-Substituted Maleimides;N-Substituted Maleimides, Succinimides & Phthalimides;Acrylic Monomers;Maleimide;Monomers
Organism | Test Type | Route | Reported Dose (Normalized Dose) | Effect | Source |
---|---|---|---|---|---|
mouse | LD50 | oral | 250mg/kg (250mg/kg) | Gigiena i Sanitariya. For English translation, see HYSAAV. Vol. 40(11), Pg. 109, 1975. | |
rat | LC50 | inhalation | 55mg/m3/4H (55mg/m3) | United States Environmental Protection Agency, Office of Pesticides and Toxic Substances. Vol. 8EHQ-0790-1023S, | |
rat | LD50 | oral | 1370mg/kg (1370mg/kg) | Gigiena i Sanitariya. For English translation, see HYSAAV. Vol. 40(11), Pg. 109, 1975. | |
rat | LDLo | intraperitoneal | 50mg/kg (50mg/kg) | National Academy of Sciences, National Research Council, Chemical-Biological Coordination Center, Review. Vol. 5, Pg. 22, 1953. |
Reported in EPA TSCA Inventory.
Safety Information about 1,3-Bismaleimido benzene (CAS NO.3006-93-7):
Hazard Codes: T,T+.Xi
Risk Statements: 23/24/25-36/37/38-26-22
R22: Harmful if swallowed.
R26: Very toxic by inhalation.
R36/37/38: Irritating to eyes, respiratory system and skin.
R23/24/25: Toxic by inhalation, in contact with skin and if swallowed.
Safety Statements: 27-28-36/37/39-45-38
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S28: After contact with skin, wash immediately with plenty of soap-suds.
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection.
S38: In case of insufficient ventilation, wear suitable respiratory equipment.
S45: In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
RIDADR: UN 2811 6.1/PG 2
WGK Germany: 3
RTECS: ON6125000
Hazard Note: Irritant
Poison by ingestion, inhalation, and intraperitoneal routes. When heated to decomposition it emits toxic fumes of NOx.
General Information: As in any fire, wear a self-contained breathing apparatus in pressure-demand, MSHA/NIOSH (approved or equivalent), and full protective gear.
Extinguishing Media: Use foam, dry chemical, or carbon dioxide.
Handling: Do not breathe dust, vapor, mist, or gas. Do not get in eyes, on skin, or on clothing. Use only in a chemical fume hood.
Storage: Store in a cool, dry place. Store in a tightly closed container. Poison room locked.