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3221-15-6

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Basic Information
CAS No.: 3221-15-6
Name: EPITHIOCHLORHYDRIN
Article Data: 51
Molecular Structure:
Molecular Structure of 3221-15-6 (EPITHIOCHLORHYDRIN)
Formula: C3H5 Cl S
Molecular Weight: 108.592
Synonyms: Propane,1-chloro-2,3-epithio- (6CI,7CI,8CI); Thiirane, (chloromethyl)- (9CI);(Chloromethyl)thiirane; 1-Chloro-2,3-epithiopropane; 2-(Chloromethyl)thiirane;2-Thiiranylmethyl chloride; 3-Chloro-1,2-propylene sulfide; 3-Chloropropenesulfide; 3-Chloropropylene sulfide; Epithiochlorohydrin; NSC 36644;Thioepichlorohydrin
Density: 1.275g/cm3
Boiling Point: 159.6°Cat760mmHg
Flash Point: 57.5°C
Hazard Symbols:
Risk Codes: 43-34-23/24/25
Safety:
Hazard Codes T
Risk Statements 43-34-23/24/25
Safety Statements 45-38-36/37/39-28A-26-24
PSA: 25.30000
LogP: 1.34060
Related products
Synthetic route
106-89-8

epichlorohydrin

3221-15-6

2-(chloromethyl)thiirane

Conditions
ConditionsYield
With ammonium thiocyanate; bismuth(lll) trifluoromethanesulfonate In acetonitrile for 0.416667h; Heating;99%
With tin(IV)tetraphenylporphyrinato trifluoromethanesulfonate; ammonium thiocyanate In acetonitrile for 0.416667h; Heating;99%
With bismuth(III) chloride; ammonium thiocyanate In acetonitrile for 0.333333h; Heating;98%

N-(tert-butyl)-5-(chloromethyl)-1,3-oxathiolan-2-imine

A

3221-15-6

2-(chloromethyl)thiirane

B

1609-86-5

Tert-butyl isocyanate

Conditions
ConditionsYield
In quinoline at 230℃;A 12%
B 81%
333-20-0

potassium thioacyanate

106-89-8

epichlorohydrin

3221-15-6

2-(chloromethyl)thiirane

Conditions
ConditionsYield
With methanol
With methanol
17356-08-0

thiourea

106-89-8

epichlorohydrin

3221-15-6

2-(chloromethyl)thiirane

Conditions
ConditionsYield
With methanol
102-08-9

N,N-diphenylthiourea

106-89-8

epichlorohydrin

3221-15-6

2-(chloromethyl)thiirane

Conditions
ConditionsYield
With benzene
1147550-11-5

ammonium thiocyanate

106-89-8

epichlorohydrin

A

3221-15-6

2-(chloromethyl)thiirane

B

147194-24-9

3-chloro-2-hydroxypropyl thiocyanate

Conditions
ConditionsYield
With 2,6-bis[2-(o-aminophenoxy)methyl]-4-bromo-1-methoxybenzene In dichloromethane; acetonitrile at 70℃; for 1.25h;A n/a
B 78 % Chromat.
...Expand
3221-15-6

2-(chloromethyl)thiirane

29027-25-6

chloromethylthiirane-S-monooxide

Conditions
ConditionsYield
With water; fluorine; acetonitrile; propiononitrile In methanol at -78℃;95%
3221-15-6

2-(chloromethyl)thiirane

93703-24-3

3-methyl-8-bromoxanthine

1005482-51-8

8-bromo-3-methyl-7-(thietan-3-yl)-3,7-dihydro-1H-pyrine-2,6-dione

Conditions
ConditionsYield
With potassium hydroxide In water; N,N-dimethyl-formamide at 0 - 20℃;94.3%
3221-15-6

2-(chloromethyl)thiirane

chloromethylthiirane-S,S-dioxide

Conditions
ConditionsYield
With water; fluorine; acetonitrile In dichloromethane at -15 - 0℃;90%
3221-15-6

2-(chloromethyl)thiirane

75-36-5

acetyl chloride

16621-53-7

thioacetic acid S-(2-chloro-1-chloromethyl-ethyl) ester

Conditions
ConditionsYield
With CoCl2 In dichloromethane at 20℃; for 4h;81%
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