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43210-67-9

Basic Information
CAS No.: 43210-67-9
Name: Carbamicacid, N-[6-(phenylthio)-1H-benzimidazol-2-yl]-, methyl ester
Molecular Structure:
Molecular Structure of 43210-67-9 (Carbamicacid, N-[6-(phenylthio)-1H-benzimidazol-2-yl]-, methyl ester)
Formula: C15H13N3O2S
Molecular Weight: 299.35
Synonyms: Carbamicacid, [5-(phenylthio)-1H-benzimidazol-2-yl]-, methyl ester (9CI);2-(Methoxycarbonylamino)-5-(phenylthio)benzimidazole;Axilur;Fenbendazol;Fenbion;HOE 881;Methyl5-(phenylthio)-2-benzimidazolecarbamate;Methyl[5-(phenylthio)-1H-benzimidazol-2-yl]carbamate;Panacur;Safe-Guard;
EINECS: 256-145-7
Density: 1.4 g/cm3
Melting Point: 233 °C
Boiling Point:
Flash Point:
Solubility:
Appearance: Off-white solid
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36
Transport Information:
PSA: 92.31000
LogP: 3.96540
Synthetic route
43156-48-5

1,2-diamino-4-phenylthiobenzene

867-44-7

S-Methylisothiourea sulfate

79-22-1

methyl chloroformate

43210-67-9

Fenbendazole

Conditions
ConditionsYield
Stage #1: S-Methylisothiourea sulfate; methyl chloroformate With sodium hydroxide In water at 3 - 6℃; for 0.666667h;
Stage #2: 1,2-diamino-4-phenylthiobenzene With acetic acid In ethanol; water at 95℃; for 24h;
88%
43156-47-4

2-nitro-5-phenylthioaniline

43210-67-9

Fenbendazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: H2 / Pd/C / ethanol / 20 °C / 3102.89 Torr
2.1: NaOH / H2O / 0.67 h / 3 - 6 °C
2.2: 88 percent / AcOH / H2O; ethanol / 24 h / 95 °C
View Scheme
1635-61-6

5-chloro-2-nitroaniline

43210-67-9

Fenbendazole

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: K2CO3 / dimethylformamide / 6 h / Heating
2.1: H2 / Pd/C / ethanol / 20 °C / 3102.89 Torr
3.1: NaOH / H2O / 0.67 h / 3 - 6 °C
3.2: 88 percent / AcOH / H2O; ethanol / 24 h / 95 °C
View Scheme
108-98-5

thiophenol

43210-67-9

Fenbendazole

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: K2CO3 / dimethylformamide / 6 h / Heating
2.1: H2 / Pd/C / ethanol / 20 °C / 3102.89 Torr
3.1: NaOH / H2O / 0.67 h / 3 - 6 °C
3.2: 88 percent / AcOH / H2O; ethanol / 24 h / 95 °C
View Scheme
(5-phenylsulfanyl-1-phosphonooxymethyl-1H-benzoimidazol-2-yl)carbamic acid methyl ester disodium salt; (6-phenylsulfanyl-1-phosphonooxymethyl-1H-benzoimidazol-2-yl)carbamic acid methyl ester disodium salt; mixture of

(5-phenylsulfanyl-1-phosphonooxymethyl-1H-benzoimidazol-2-yl)carbamic acid methyl ester disodium salt; (6-phenylsulfanyl-1-phosphonooxymethyl-1H-benzoimidazol-2-yl)carbamic acid methyl ester disodium salt; mixture of

43210-67-9

Fenbendazole

Conditions
ConditionsYield
With chicken alkaline phosphatase In water at 39℃; pH=6.5 - 9.0; Enzyme kinetics;
With porcine alkaline phosphatase In water at 37℃; pH=6.5 - 9.0; Enzyme kinetics;
Conditions
ConditionsYield
With dihydrogen peroxide; sodium sulfite In methanol; water98.8%
With urea hydrogen peroxide adduct In formic acid; water at 25 - 45℃; for 5.5h; Temperature; Concentration;98%
43210-67-9

Fenbendazole

53065-28-4

5-(phenylthio)-1H-benzo[d]imidazol-2-amine

Conditions
ConditionsYield
With potassium hydroxide In methanol; water for 48h; Heating;98%
In N,N-dimethyl-formamide for 12h; Heating;50%
541-41-3

chloroformic acid ethyl ester

43210-67-9

Fenbendazole

A

58521-88-3

2-Methoxycarbonylamino-5-phenylsulfanyl-benzoimidazole-1-carboxylic acid ethyl ester

B

58522-05-7

2-Methoxycarbonylamino-6-phenylsulfanyl-benzoimidazole-1-carboxylic acid ethyl ester

Conditions
ConditionsYield
With sodium hydroxide In dichloromethane Ambient temperature;
79-22-1

methyl chloroformate

43210-67-9

Fenbendazole

A

58521-87-2

methyl 1-methoxycarbonyl-5-phenylthiobenzimidazole-2-carbamate

B

58522-04-6

2-Methoxycarbonylamino-6-phenylsulfanyl-benzoimidazole-1-carboxylic acid methyl ester

Conditions
ConditionsYield
With sodium hydroxide In dichloromethane for 20h; Ambient temperature;A 12 g
B 8 g
43210-67-9

Fenbendazole

2941-64-2

Ethyl chlorothioformate

A

104663-11-8

2-Methoxycarbonylamino-5-phenylsulfanyl-benzoimidazole-1-carbothioic acid S-ethyl ester

B

104663-33-4

2-Oxo-5-phenylsulfanyl-benzoimidazole-1,3-dicarbothioic acid di-S-ethyl ester

Conditions
ConditionsYield
With sodium hydroxide In dichloromethane Ambient temperature;
43210-67-9

Fenbendazole

74-88-4

methyl iodide

Methyl-(1-methyl-5-phenylsulfanyl-1H-benzoimidazol-2-yl)-carbamic acid methyl ester

Conditions
ConditionsYield
With AG-MP1 anion exchange resin In carbon dioxide at 80℃; under 150012 Torr; for 0.333333h; Product distribution; further conditions: CH3CN, room temperature, 1 h;
43210-67-9

Fenbendazole

104663-22-1

6-Benzenesulfinyl-2-methoxycarbonylamino-benzoimidazole-1-carboxylic acid methyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 8 g / 1N aq sodium hydroxide / CH2Cl2 / 20 h / Ambient temperature
2: m-chloroperbenzoic acid / CH2Cl2
View Scheme
43210-67-9

Fenbendazole

104663-01-6

1-carbomethoxy-2-carbomethoxyamino-5-phenylsulfinylbenzimidazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 12 g / 1N aq sodium hydroxide / CH2Cl2 / 20 h / Ambient temperature
2: 8 g / m-chloroperbenzoic acid / CH2Cl2 / 16 h / 15 - 20 °C
View Scheme
43210-67-9

Fenbendazole

104663-08-3

1-carbomethoxy-2-carbomethoxyamino-5-phenylsulfonylbenzimidazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 12 g / 1N aq sodium hydroxide / CH2Cl2 / 20 h / Ambient temperature
2: 1.5 g / m-chloroperbenzoic acid / CH2Cl2
View Scheme
43210-67-9

Fenbendazole

104663-29-8

6-Benzenesulfonyl-2-methoxycarbonylamino-benzoimidazole-1-carboxylic acid methyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 8 g / 1N aq sodium hydroxide / CH2Cl2 / 20 h / Ambient temperature
2: m-chloroperbenzoic acid / CH2Cl2
View Scheme
43210-67-9

Fenbendazole

104663-02-7

5-Benzenesulfinyl-2-methoxycarbonylamino-benzoimidazole-1-carboxylic acid ethyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1N aq sodium hydroxide / CH2Cl2 / Ambient temperature
2: m-chloroperbenzoic acid / CH2Cl2
View Scheme
43210-67-9

Fenbendazole

104663-12-9

5-Benzenesulfinyl-2-methoxycarbonylamino-benzoimidazole-1-carbothioic acid S-ethyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1N aq sodium hydroxide / CH2Cl2 / Ambient temperature
2: m-chloroperbenzoic acid / CH2Cl2
View Scheme
43210-67-9

Fenbendazole

104663-23-2

6-Benzenesulfinyl-2-methoxycarbonylamino-benzoimidazole-1-carboxylic acid ethyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1N aq sodium hydroxide / CH2Cl2 / Ambient temperature
2: m-chloroperbenzoic acid / CH2Cl2
View Scheme
43210-67-9

Fenbendazole

59530-20-0

2-amino-5(6)-benzenesulfonylbenzimidazole

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 98 percent / KOH / methanol; H2O / 48 h / Heating
2: 82 percent / pyridine / 1 h / Heating
3: 82.6 percent / KMnO4 / acetic acid / 2 h / Ambient temperature
4: 73.5 percent / aq. NaOH / ethanol / 2 h / Ambient temperature
View Scheme
43210-67-9

Fenbendazole

125422-34-6

2-Acetamido-5(6)-phenylthiobenzimidazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 98 percent / KOH / methanol; H2O / 48 h / Heating
2: 82 percent / pyridine / 1 h / Heating
View Scheme
43210-67-9

Fenbendazole

125422-38-0

5(6)-Phenylthio-2-(carboxamidomethylamino)-benzimidazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 98 percent / KOH / methanol; H2O / 48 h / Heating
2: 50 percent / triethylamine / acetone / 12 h / Heating
View Scheme
43210-67-9

Fenbendazole

125422-41-5

5(6)-Phenylthio-2-chloroacetamidobenzimidazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 98 percent / KOH / methanol; H2O / 48 h / Heating
2: 88 percent / triethylamine / acetone / 3 h / Ambient temperature
View Scheme
43210-67-9

Fenbendazole

125422-35-7

2-Acetamido-5(6)-phenylsulphonobenzimidazole

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 98 percent / KOH / methanol; H2O / 48 h / Heating
2: 82 percent / pyridine / 1 h / Heating
3: 82.6 percent / KMnO4 / acetic acid / 2 h / Ambient temperature
View Scheme
43210-67-9

Fenbendazole

125422-37-9

(5-Phenylsulfanyl-1H-benzoimidazol-2-ylamino)-acetic acid methyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 98 percent / KOH / methanol; H2O / 48 h / Heating
2: 64 percent / triethylamine
View Scheme
43210-67-9

Fenbendazole

125443-69-8

2-(Carbethoxymethylamino)-5(6)-phenylthiobenzimidazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 98 percent / KOH / methanol; H2O / 48 h / Heating
2: 55 percent / triethylamine / acetone / 12 h / Heating
View Scheme
43210-67-9

Fenbendazole

125443-68-7

2,2,2-Trifluoro-N-(5-phenylsulfanyl-1H-benzoimidazol-2-yl)-acetamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 98 percent / KOH / methanol; H2O / 48 h / Heating
2: 71 percent / 3 h / Heating
View Scheme
43210-67-9

Fenbendazole

125422-49-3

2-Chloroacetamido-5(6)-phenylsulphonobenzimidazole

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 98 percent / KOH / methanol; H2O / 48 h / Heating
2: 82 percent / pyridine / 1 h / Heating
3: 82.6 percent / KMnO4 / acetic acid / 2 h / Ambient temperature
4: 73.5 percent / aq. NaOH / ethanol / 2 h / Ambient temperature
5: 80 percent / triethylamine / tetrahydrofuran / 3 h / Ambient temperature
View Scheme
43210-67-9

Fenbendazole

125422-39-1

2-(5-Phenylsulfanyl-1H-benzoimidazol-2-ylamino)-1-piperidin-1-yl-ethanone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 98 percent / KOH / methanol; H2O / 48 h / Heating
2: 56 percent / triethylamine
View Scheme
43210-67-9

Fenbendazole

125422-42-6

2-(1-Pyrrolidinoacetylamino)-5(6)-phenylthiobenzimidazole

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 98 percent / KOH / methanol; H2O / 48 h / Heating
2: 88 percent / triethylamine / acetone / 3 h / Ambient temperature
3: 64 percent / triethylamine / acetone / 12 h / Heating
View Scheme
43210-67-9

Fenbendazole

125422-43-7

N-(5-Phenylsulfanyl-1H-benzoimidazol-2-yl)-2-piperidin-1-yl-acetamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 98 percent / KOH / methanol; H2O / 48 h / Heating
2: 88 percent / triethylamine / acetone / 3 h / Ambient temperature
3: 67 percent / triethylamine
View Scheme
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53716-50-0
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    43210-67-9

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    43210-67-9

    43210-67-9 CAS Fenbendazole

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    Specifications 1.Product name:Albendazole 2.CAS#:54965-21-8 3.Molecular formula:C12H15N3O2S 4.Purity:98%-102% min 5.Best quality from CN Product name: ALBENDAZOLE CAS#: 54965-21-8 Molecular formula: C12H15N3O2S

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    N-[6-(phenylthio)-1H-benzimidazol-2-yl]carbamic acid methyl ester

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  • Casno:

    43210-67-9

    Fenbendazole

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    Product Name Fenbendazole CAS 43210-67-9 Einecs No N/A Appearance Almost white powder

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Chemistry

IUPAC:methyl N-(6-phenylsulfanyl-1H-benzimidazol-2-yl)carbamate
CAS:43210-67-9
The Molecular formula of Fenbendazole(43210-67-9):C15H13N3O2S
The Molecular Weight of Fenbendazole(43210-67-9):299.35
Synonyms:[5-(PHENYLTHIO)-1H-BENZIMIDAZOL-2-YL]CARBAMIC ACID, METHYL ESTER;HOE-881V;FENBENDAZOLE;METHYL 5-(PHENYLTHIO)-2-BENZIMIDAZOLECARBAMATE;SAFEGARD;PANACUR;(5-(phenylthio)-1h-benzimidazol-2-yl)-carbamicacimethylester;5-(phenylthio)-2-benzimidazolecarbamicacimethylester
EINECS:256-145-7
Density:1.4g/cm3
Melting Point:233oC
Appearance:white to yellowish powder
Product Categories:PHARMACEUTICALS;Active Pharmaceutical Ingredients;API;Intermediates & Fine Chemicals;Veterinaries
Mol File:43210-67-9.mol
storage temp.:0-6oC

Uses

Fenbendazole(43210-67-9) is known as a kind of benzimidazole anthelmintics. It is regularly used to eliminate numerous gastrointestinal parasites from animals,and it is quite effective against roundworms, hookworms, whipworms, certain tapeworms and parasites called strongyles and strongyloides.

Toxicity Data With Reference

1.   

oth:hmn:lym 100 mg/L

   ENMUDM    Environmental Mutagenesis. 2 (1980),67.
2.   

oth:hmn:leu 1 mg/L

   THERAP    Therapie. 31 (1976),505.

Safety Profile

Human mutation data reported. When heated to decomposition it emits toxic fumes of SOx and NOx.

Safty informations about Fenbendazole(43210-67-9):
Hazard Codes:Xi
Risk Statements:36/37/38
 36/37/38(Irritating to eyes, respiratory system and skin)
Safety Statements:26-36
 26(In case of contact with eyes, rinse immediately with plenty of water and seek medical advice)
 36(Wear suitable protective clothing)
WGK Germany:2
RTECS:DD6520500

Specification

Storage:Keep tightly closed.