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| CAS No.: | 620-72-4 |
|---|---|
| Name: | Phenyl bromoacetate |
| Article Data: | 32 |
| Molecular Structure: | |
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|
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| Formula: | C8H7BrO2 |
| Molecular Weight: | 215.046 |
| Synonyms: | Aceticacid, bromo-, phenyl ester (6CI,7CI,8CI,9CI);alpha-Phenyl Bromoacetate;Phenyl a-bromoacetate;bromoacetic acidphenyl ester; |
| EINECS: | 805-881-2 |
| Density: | 1.533 g/cm3 |
| Melting Point: | 31-33 °C(lit.) |
| Boiling Point: | 261.9 °C at 760 mmHg |
| Flash Point: | 112.2 °C |
| Solubility: | Soluble in ethanol and ether, insoluble in water. |
| Appearance: | Liquid |
| Safety: | 24/25 |
| PSA: | 26.30000 |
| LogP: | 1.98690 |
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| Conditions | Yield |
|---|---|
| Heating; | 92% |
| With triethylamine In dichloromethane at 0℃; for 1.5h; Inert atmosphere; | 81% |
| at 80℃; for 1h; | 77% |
| Conditions | Yield |
|---|---|
| With zinc(II) chloride at 50 - 70℃; for 3.5h; | 38% |
| Conditions | Yield |
|---|---|
| (i) DCC, THF, (ii) /BRN= 506167/; Multistep reaction; | |
| With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; |
- 620-72-4
phenyl 2-bromoacetate
| Conditions | Yield |
|---|---|
| With acetic acid at 100℃; im geschlossenen Rohr; |
- 620-72-4
phenyl 2-bromoacetate
| Conditions | Yield |
|---|---|
| With water |
- 7647-01-0
hydrogenchloride
- 60-29-7
diethyl ether
- 1600-27-7
mercury(II) diacetate
- 620-72-4
phenyl 2-bromoacetate
| Conditions | Yield |
|---|---|
| at 10℃; |
| Conditions | Yield |
|---|---|
| With sulfuric acid In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; acetic anhydride |
- 620-72-4
phenyl 2-bromoacetate
- 74802-29-2
3S-3-<<(1,1-Dimethylethoxy)carbonyl>amino>-2,5-dioxo-2,3,4,5-tetrahydro-1H-1-benzazepine
- 128776-36-3
Benzyl 2-(3S-3-<<(1,1-Dimethylethoxy)carbonyl>amino>-2,5-dioxo-2,3,4,5-tetrahydro-1H-1-benzazepin-1-yl)-ethanoate
| Conditions | Yield |
|---|---|
| With tetrabutylammomium bromide; potassium carbonate In acetone | 98% |
- 620-72-4
phenyl 2-bromoacetate
- 603-35-0
triphenylphosphine
- 32443-55-3
((triphenyl)-λ5-phosphanylidene)acetic acid phenyl ester
| Conditions | Yield |
|---|---|
| Stage #1: phenyl 2-bromoacetate; triphenylphosphine In chloroform at 23℃; Inert atmosphere; Stage #2: With sodium hydroxide In water | 96% |
| Stage #1: phenyl 2-bromoacetate; triphenylphosphine In benzene at 20℃; for 18h; Stage #2: With sodium hydroxide In dichloromethane; water for 0.5h; | |
| Multi-step reaction with 2 steps 1: toluene / 12 h / Inert atmosphere 2: sodium hydroxide / dichloromethane; water / 0.33 h / 20 °C View Scheme |
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Chemistry
Product Name: Phenyl bromoacetate (CAS NO.620-72-4)
Molecular Formula: C8H7BrO2
Molecular Weight: 215.04g/mol
Mol File: 620-72-4.mol
Melting Point: 31-33 °C(lit.)
Boiling point: 261.9 °C at 760 mmHg
Flash Point: 112.2 °C
Density: 1.533 g/cm3
Surface Tension: 43.8 dyne/cm
Enthalpy of Vaporization: 49.97 kJ/mol
Vapour Pressure: 0.0112 mmHg at 25°C
Product Categories: C8 to C9; Carbonyl Compounds; Esters
Specification
Phenyl bromoacetate , its CAS NO. is 620-72-4, the synonym is alpha-Phenyl Bromoacetate .