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Basic Information
| CAS No.: | 623-17-6 |
|---|---|
| Name: | Furfuryl acetate |
| Article Data: | 52 |
| Molecular Structure: | |
|
|
|
| Formula: | C7H8O3 |
| Molecular Weight: | 140.139 |
| Synonyms: | 2-Furanmethanol acetate;2-Furylcarbinyl acetate;Furfuryl alcohol, acetate;5-17-03-00344 (Beilstein Handbook Reference);Acetic acid furfurylester;2-Acetoxymethylfuran;2-Furfuryl acetate;2-Furanmethanol, acetate;2-Furanmethyl acetate;FEMA No. 2490;Acetic acid furfuryl ester;2-furylmethyl acetate; |
| EINECS: | 210-775-9 |
| Density: | 1.12 g/cm3 |
| Boiling Point: | 177 °C at 760 mmHg |
| Flash Point: | 65.6 °C |
| Solubility: | 0.5-1.0 g/100 mL at 23 °C in water |
| Appearance: | Colorless to light yellow liquid |
| Hazard Symbols: |
 Xi
|
| Risk Codes: | 36/37/38 |
| Safety: | 24/25-37/39-26 |
| PSA: | 39.44000 |
| LogP: | 1.34270 |
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Synthetic route
- 623-17-6
furfurylacetate
- 93-55-0
1-phenyl-propan-1-one
- 1440662-73-6
(E)-(5-(3-oxo-3-phenylprop-1-enyl)furan-2-yl)methyl acetate
Conditions
| Conditions | Yield |
|---|---|
| With silver (II) carbonate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; lithium acetate; palladium diacetate; tricyclohexylphosphine In 1,2-dimethoxyethane at 100℃; for 24h; Schlenk technique; Inert atmosphere; | 56% |
Conditions
| Conditions | Yield |
|---|---|
| With lipase B from Candida antarctica immobilized on Immobead 150 In aq. phosphate buffer at 40℃; for 0.333333h; pH=7.4; | 89% |
| With methanol; potassium permanganate; trimethylsulphonium iodide at 25℃; under 760.051 Torr; chemoselective reaction; | 80% |
| With methanol; potassium permanganate at 25℃; chemoselective reaction; | 78% |
| With [t-Bu2SnOH(Cl)]2 In methanol at 30℃; for 24h; Deacetylation; | 82 % Chromat. |
| [t-Bu2SnOH(Cl)]2 In methanol at 30℃; for 24h; | 82 % Chromat. |
Conditions
| Conditions | Yield |
|---|---|
| With Montmorillonite In dichloromethane at 60℃; Sealed tube; | 35% |
- 108-31-6
maleic anhydride
- 623-17-6
furfurylacetate
- 6331-95-9, 19308-92-0
(+/-)-(1RS,2SR,6RS,7SR)-(3,5-dioxo-4,10-dioxatricyclo[5.2.1.02,6]dec-8-en-1-yl)methyl acetate
Conditions
| Conditions | Yield |
|---|---|
| In toluene at 23℃; | 86% |
| In toluene at 23℃; for 97h; Diels-Alder reaction; | 74% |
| In diethyl ether at 25℃; for 168h; Diels-Alder cycloaddition; | 34% |
| With diethyl ether |
Conditions
| Conditions | Yield |
|---|---|
| With bis(trifluoromethanesulfonyl)amide In dichloromethane at 20℃; for 0.333333h; | 70 %Chromat. |
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: furfurylacetate With 5%-palladium/activated carbon; hydrogen; acetic acid at 100℃; under 7600.51 Torr; for 6h; Autoclave; Stage #2: With methanol; water Reagent/catalyst; Temperature; Pressure; Reflux; | A 24% B 15% C 56% |
...Expand
- 623-17-6
furfurylacetate
Conditions
| Conditions | Yield |
|---|---|
| With manganese triacetate In acetic acid at 80℃; for 3h; | 86% |
Conditions
| Conditions | Yield |
|---|---|
| With gold-nanoparticles supported on TiO2 In 1,4-dioxane at 60℃; for 2h; | 53% |
- 623-17-6
furfurylacetate
- 118-92-3
anthranilic acid
- 117078-27-0
1-acetoxymethyl-11-oxatricyclo[6.2.1.02,7]undeca-2,4,6,9-tetraene
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: anthranilic acid With isopentyl nitrite; trichloroacetic acid In tetrahydrofuran at 0 - 20℃; Stage #2: furfurylacetate With methyloxirane In tetrahydrofuran Heating; Further stages.; | 75% |
| With isopentyl nitrite In 1,2-dimethoxyethane | 45.8% |
- 623-17-6
furfurylacetate
- 137073-16-6
3-tert-butyl-3-methylcycloprop-1-ene
- 1268380-58-0
(3E,5E,7E)-8,9,9-trimethyl-2-oxodeca-3,5,7-trienyl acetate
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: furfurylacetate; 3-tert-butyl-3-methylcycloprop-1-ene With C16H26AuNP(1+)*F6Sb(1-) In dichloromethane at 25℃; for 0.25h; Inert atmosphere; Stage #2: With iodine In dichloromethane for 1h; Inert atmosphere; | 78% |
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Furfuryl acetate
Chemistry
Molecular Formula: C7H8O3 
Formula Weight: 140.14
bp of 2-FURANMETHYL ACETATE (623-17-6): 175-177 °C(lit.)
density : 1.118 g/mL at 25 °C(lit.)
refractive index : n20/D 1.462(lit.)
Fp of 2-FURANMETHYL ACETATE (623-17-6): 150 °F
Water Solubility : 0.5-1.0 g/100 mL at 23 oC
PHYSICAL STATE: Clear to pale yellow liquid
Formula Weight: 140.14
bp of 2-FURANMETHYL ACETATE (623-17-6): 175-177 °C(lit.)
density : 1.118 g/mL at 25 °C(lit.)
refractive index : n20/D 1.462(lit.)
Fp of 2-FURANMETHYL ACETATE (623-17-6): 150 °F
Water Solubility : 0.5-1.0 g/100 mL at 23 oC
PHYSICAL STATE: Clear to pale yellow liquid
Uses
2-FURANMETHYL ACETATE (623-17-6) is used as a solvent and flavor enhancer and modifier in foods and perfumes. Also it is used as intermediate of dyes, resins and spices.
Production
2-FURANMETHYL ACETATE (623-17-6) is derived from furan reaction with acetic anhydride.
Toxicity Data With Reference
| 1. | mmo-sat 1 mg/plate | ENMUDM Environmental Mutagenesis. 8 (Suppl 7)(1986),1. | ||
| 2. | mma-sat 2500 µg/plate | ENMUDM Environmental Mutagenesis. 8 (Suppl 7)(1986),1. |
Consensus Reports
Reported in EPA TSCA Inventory.
Safety Profile
Safety: CAUTION: May irritate eyes, skin, and respiratory tract
Hazard Codes : Xi (Irritant)
Risk Statements : 36/37/38 (Irritating to eyes, respiratory system and skin)
Safety Statements : 24/25-37/39-26 (Avoid contact with skin and eyes; Wear suitable gloves and eye/face protection; In case of contact with eyes, rinse immediately with plenty of water and seek medical advice)
WGK Germany : 3
RTECS : LU9120000
Hazard Note : Irritant
Mutation data reported. When heated to decomposition it emits acrid smoke and irritating vapors.
Hazard Codes : Xi (Irritant)
Risk Statements : 36/37/38 (Irritating to eyes, respiratory system and skin)
Safety Statements : 24/25-37/39-26 (Avoid contact with skin and eyes; Wear suitable gloves and eye/face protection; In case of contact with eyes, rinse immediately with plenty of water and seek medical advice)
WGK Germany : 3
RTECS : LU9120000
Hazard Note : Irritant
Mutation data reported. When heated to decomposition it emits acrid smoke and irritating vapors.
Standards and Recommendations
ASSAY: 98.0% min
ACIDITY: 0.1% max
ACIDITY: 0.1% max
Specification
Storage: Protect from moisture. Store in tightly sealed containers in a cool place.