CAS No.6864-37-5,Dimethyldicyane Suppliers,MSDS download

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Basic Information

Molecular Structure:
CAS No.:	6864-37-5
Name:	Dimethyldicyane
Article Data:	8
Cas Database

Formula:	C15H30 N2
Molecular Weight:	238.417
Synonyms:	Cyclohexylamine,4,4'-methylenebis[2-methyl- (6CI,7CI,8CI);2,2'-Dimethyl-4,4'-methylenebis(cyclohexylamine);3,3'-Dimethyl-4,4'-diaminodicyclohexylmethane;3DCM;4,4'-Diamino-3,3'-dimethyldicyclohexylmethane;4,4'-Methylenebis[2-methylcyclohexanamine];4,4'-Methylenebis[2-methylcyclohexylamine];Ancamine 2049;Bis(3-methyl-4-aminocyclohexyl)methane;Bis(4-amino-3-methylcyclohexyl)methane;Ciba 2976;Dimethyldicykan;Epicure 113;Eporesit T 58;Hardener SL;JER Cure113;Laromin C;Laromin C 260;RF 24;Rutapox SL;SIQ-AMIN 1105;
EINECS:	229-962-1
Density:	0.94 g/mL at 25 °C(lit.)
Melting Point:	-7°C
Boiling Point:	289.6 °C at 760 mmHg
Flash Point:	>230 °F
Solubility:	2.01g/L at 20℃
Appearance:	COLOURLESS TO YELLOW LIQUID
Hazard Symbols:	Moderately toxic by inhalation.
Risk Codes:	22-23/24-35-51/53
Safety:	Moderately toxic by inhalation. When heated to decomposition it emits toxic vapors of NO_x.
Transport Information:	UN 2927 6
PSA:	52.04000
LogP:	4.30410

Synthetic route

: 838-88-0
3,3'-dimethyl-4,4'-diaminodiphenylmethane

: 6864-37-5
bis-(4-amino-3-methylcyclohexyl)-methane

Conditions

Conditions	Yield
With ruthenium on aluminium oxide; ammonium aluminium sulfate; hydrogen In tetrahydrofuran at 160℃; under 60006 Torr; for 4h; Acidic conditions; Large scale;	99.4%
With 1,4-dioxane; ruthenium(IV) oxide at 120 - 125℃; under 102971 - 154457 Torr; Hydrogenation;
With cobalt(III) oxide; sodium carbonate; calcium oxide at 200 - 220℃; under 110326 Torr; Hydrogenation;

: 838-88-0
3,3'-dimethyl-4,4'-diaminodiphenylmethane

A: 1201895-82-0
(4-amino-3-methylcyclohexyl)(4-amino-3-methylphenyl)methane

B: 6864-37-5
bis-(4-amino-3-methylcyclohexyl)-methane

Conditions

Conditions	Yield
With hydrogen; silica gel at 230℃; under 75007.5 - 202520 Torr; for 9h; Product distribution / selectivity; Autoclave; Inert atmosphere;

: 6864-37-5
bis-(4-amino-3-methylcyclohexyl)-methane

: 403-43-0
4-fluorobenzoyl chloride

: N,N'-bis(4-fluorobenzamide)-3,3'-dimethyldicyclohexyl methane

Conditions

Conditions	Yield
With sodium dodecyl-sulfate; sodium hydroxide In dichloromethane; water at 5 - 10℃; for 8h;	82.7%

: 6864-37-5
bis-(4-amino-3-methylcyclohexyl)-methane

: 623-27-8
terephthalaldehyde,

: C31H38N2O2

Conditions

Conditions	Yield
In tetrahydrofuran at 70℃; for 27h; Inert atmosphere; Schlenk technique;	70%

: 90-11-9
1-Bromonaphthalene

: 6864-37-5
bis-(4-amino-3-methylcyclohexyl)-methane

: C35H42N2

Conditions

Conditions	Yield
With tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate In toluene for 1h; Inert atmosphere; Reflux;	50%

: 50-00-0
formaldehyd

: 6864-37-5
bis-(4-amino-3-methylcyclohexyl)-methane

: 97423-00-2
bis-(4-dimethylamino-3-methyl-cyclohexyl)-methane

Conditions

Conditions	Yield
With methanol; water; nickel at 100℃; under 44130.5 Torr; Hydrogenation;

: 38460-95-6
undec-10-enoyl chloride

: 6864-37-5
bis-(4-amino-3-methylcyclohexyl)-methane

: 61796-67-6
Undec-10-enoic acid [2-methyl-4-(3-methyl-4-undec-10-enoylamino-cyclohexylmethyl)-cyclohexyl]-amide

Conditions

Conditions	Yield
With triethylamine
With triethylamine In tetrahydrofuran

: C33H17Cl2N6O12S3(3-)*3Na(1+)

: 6864-37-5
bis-(4-amino-3-methylcyclohexyl)-methane

: C81H62Cl2N14O24S6(6-)*6Na(1+)

Conditions

Conditions	Yield
With sodium hydroxide In water at 50 - 60℃; for 2h; pH=5.7 - 6.3;

: 7154-73-6
1-(2-aminoethyl)pyrrolidine

: 27578-60-5
1-(2-aminoethyl)piperidine

: 140-31-8
aminoethylpiperazine

: 2038-03-1
4-(2-AMINOETHYL)MORPHOLINE

: 25560-00-3
3-(2-Methyl-piperidino)-propylamin

: 123-00-2
4-(3-Aminopropyl)morpholine

: 5036-48-6
3-(1H-imidazol-1-yl)propan-1-amine

: 7663-77-6
1-(3-aminopropyl)-2-pyrrolidone

: 34035-03-5
5-(4-chlorophenyl)-2-furaldehyde

: 1761-71-3
4,4'-diaminodicyclohexylmethane

: 6864-37-5
bis-(4-amino-3-methylcyclohexyl)-methane

: 2213-43-6
1-Aminopiperidine

: 63234-71-9
1-aminopyrrolidine hydrochloride

: 5906-35-4
1-azepanylamine

: 59983-39-0
(S)-1-amino-2-(methoxymethyl)pyrrolidine

: 1664-40-0
N-(2-aminoethyl)benzeneamine

: 6530-09-2, 119904-90-4, 120538-52-5, 123536-14-1, 124577-62-4, 126358-22-3, 137661-30-4, 137661-31-5
(3R)-quinuclidin-3-amine dihydrochloride

: 108-00-9
N,N-dimethylethylenediamine

: 109-55-7
1-amino-3-(dimethylamino)propane

: 51387-90-7
2-(2-AMINOETHYL)-1-METHYLPYRROLIDINE

: 102-83-0
3-dibutylaminopropylamine

A: 849908-66-3
C15H19ClN2O

B: C15H17ClN2O

C: 849908-70-9
C16H21ClN2O

D: 940358-24-7
C17H18ClN3O

E: C16H19ClN2O

F: C19H19ClN2O

G: 849908-71-0
C18H23ClN2O

H: C17H21ClN2O2

I: 849908-67-4
C17H21ClN2O

J: C17H21ClN2O

K: 880815-24-7
C17H21ClN2O2

L: C17H22ClN3O

M: C18H21ClN2O

N: 849908-65-2
C18H23ClN2O

O: 932172-19-5
C18H21ClN2O2

P: 875001-79-9
N-((5-(4-chlorophenyl)furan-2-yl)methyl)-3-morpholinopropan-1-amine

Q: 849908-68-5
C20H27ClN2O

R: 849908-69-6
C22H33ClN2O

S: 849908-81-2
C24H33ClN2O

T: 849908-75-4
C26H37ClN2O

Conditions

Conditions	Yield
With polymer-bound trimethyl ammonium cyanoborohydride; acetic acid In 1,2-dichloro-ethane at 20℃; for 24 - 36h; Polystyrene; Combinatorial reaction / High throughput screening (HTS);

...Expand

: 6864-37-5
bis-(4-amino-3-methylcyclohexyl)-methane

: 2421-28-5
dianhydride of benzophenone-3,4,3',4'-tetracarboxy acid

Reaxys ID: 18804844: Reaxys ID: 18804844

Conditions

Conditions	Yield
In ISOPROPYLAMIDE at 150℃; for 2h;

Raw Materials

838-88-0

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Chemistry

Molecular structure:

MF: C₁₅H₃₀N₂
MW: 238.41
EINECS: 229-962-1
Synonyms: 3,3’-Dimethyl-4,4’-diaminodicyclohexylmethane;4,4’-methylenebis[2-methyl-cyclohexanamin;4,4’-methylenebis[2-methyl-Cyclohexanamine;BIS(4-AMINO-3-METHYLCYCLOHEXYL)METHANE;2,2'-DIMETHYL-4,4'-METHYLENEBIS(CYCLOHEXYLAMINE);4,4'-DIAMINO-3,3'-DIMETHYLDICYCLOHEXYLMETHANE;4,4'-METHYLENEBIS(1-AMINO-2-METHYLCYCLOHEXANE);4,4'-METHYLENEBIS(2-METHYLCYCLOHEXYLAMINE)
Product Categories: Nitrogen Compounds;Organic Building Blocks;Polyamines
Mol File: 6864-37-5.mol
refractive index ： n20/D 1.499(lit.)
Fp ： >230 °F
BIS(4-AMINO-3-METHYLCYCLOHEXYL)METHANE（6864-37-5）'s mp is -7°C, bp is 93-100 °C(lit.) and density is 0.94 g/mL at 25 °C(lit.)

Uses

BIS(4-AMINO-3-METHYLCYCLOHEXYL)METHANE （6864-37-5）is used for organic chemical raw materials.

Safety Profile

Hazard Codes : T,C,N
Risk Statements : 22-23/24-35-51/53
Safety Statements : 26-36/37/39-45-61
RIDADR : UN 2927 6.1/PG 2
WGK Germany : 3
HazardClass : 8
PackingGroup : II