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| CAS No.: | 693-04-9 |
|---|---|
| Name: | Butylmagnesium chloride |
| Molecular Structure: | |
|
|
|
| Formula: | C4H9ClMg |
| Molecular Weight: | 116.873 |
| Synonyms: | Butylmagnesiumchloride (6CI);Butylchloromagnesium;Butylmagnesiumm chloride;n-Butylmagnesium chloride; |
| EINECS: | 211-739-5 |
| Density: | 0.962 g/mL at 25 °C |
| Melting Point: | -17°C |
| Boiling Point: | 66 °C |
| Flash Point: | 115 °F |
| Solubility: | reacts with water |
| Appearance: | green-brown to brown solution |
| Hazard Symbols: |
 F, C
|
| Risk Codes: | 11-14/15-19-34-48/20-63-65-67 |
| Safety: | 16-26-29-36/37/39-45-46-62 |
| Transport Information: | UN 3399 4.3/PG 2 |
| PSA: | 0.00000 |
| LogP: | 2.44360 |
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| Conditions | Yield |
|---|---|
| With magnesium In tetrahydrofuran-d8 at 80℃; under 5171.62 Torr; Inert atmosphere; Flow reactor; | 95% |
| With magnesium anthracene * 3 THF 1.) toluene, 90 deg C, 2.) r.t., 12 h; Yield given. Multistep reaction; | |
| With magnesium In tetrahydrofuran at 23℃; Kinetics; |
- 109-69-3
n-Butyl chloride
- 86901-19-1
9,10-dihydro-9,10-anthracendiyl-tris(THF)magnesium
A
- 47205-57-2
9,10-dibutyl-9,10-dihydro-anthracene
B
- 10394-60-2
9-butyl-9,10-dihydro-anthracene
C
- 693-04-9
butyl magnesium bromide
D
- 126694-91-5
2-butyl-1,2-dihydroanthracene
| Conditions | Yield |
|---|---|
| In toluene for 24h; Ambient temperature; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts; |
- 109-69-3
n-Butyl chloride
A
- 47205-57-2
9,10-dibutyl-9,10-dihydro-anthracene
B
- 10394-60-2
9-butyl-9,10-dihydro-anthracene
C
- 693-04-9
butyl magnesium bromide
D
- 126694-91-5
2-butyl-1,2-dihydroanthracene
| Conditions | Yield |
|---|---|
| With magnesium anthracene * 3 THF In toluene at 50 - 80℃; for 2h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts; |
| Conditions | Yield |
|---|---|
| Einfluss verschiedener Aktivatoren; |
- 97-93-8
triethylaluminum
- 62202-86-2
n-butyl-ethylmagnesium
A
- 14989-29-8
hydridomagnesium chloride
C
- 693-04-9
butyl magnesium bromide
D
- 2386-64-3
ethylmagnesium chloride
E
- 7786-30-3
magnesium chloride
| Conditions | Yield |
|---|---|
| In 2-Methylpentane for 4383h; Reactivity; |
| Conditions | Yield |
|---|---|
| In tetrahydrofuran | |
| With iodine In tetrahydrofuran for 0.5h; Heating / reflux; | |
| With dibutyl ether at 50 - 60℃; for 5h; |
| Conditions | Yield |
|---|---|
| In tert-butyl methyl ether; toluene at 20℃; Equilibrium constant; Solvent; Inert atmosphere; |
| Conditions | Yield |
|---|---|
| With diethyl ether |
| Conditions | Yield |
|---|---|
| With buta-1,3-diene; nickel dibromide In tetrahydrofuran at 0℃; for 0.25h; Kinetics; Reagent/catalyst; Temperature; Concentration; | 100% |
| With 1-Phenylprop-1-yne; copper dichloride In tetrahydrofuran at 25℃; for 0.25h; | 99 % Chromat. |
| With LaFe0.80Ni0.20O3; buta-1,3-diene at 20℃; for 5h; | 91 %Chromat. |
| With 1-Phenylprop-1-yne; copper dichloride In tetrahydrofuran at 40℃; for 48h; Catalytic behavior; Temperature; | 40 %Chromat. |
| With dicarbonyl(cyclopentadienyl)iron(II) chloride; buta-1,3-diene In tetrahydrofuran at 0 - 20℃; for 24h; Grignard Reaction; Inert atmosphere; Schlenk technique; | 54 %Chromat. |
- 1071227-13-8
[3S,5S,7aR]-5-isopropyl-3-phenyl-hexahydropyrrolo[2,1-b]oxazole
- 693-04-9
butyl magnesium bromide
- 1071226-98-6
(2S)-2-((2R,5S)-2-butyl-5-isopropylpyrrolidin-1-yl)-2-phenylethanol
| Conditions | Yield |
|---|---|
| Stage #1: [3S,5S,7aR]-5-isopropyl-3-phenyl-hexahydropyrrolo[2,1-b]oxazole; butyl magnesium bromide In tetrahydrofuran at 0 - 20℃; Inert atmosphere; Stage #2: With ammonium chloride In tetrahydrofuran optical yield given as %de; | 100% |
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Specification
This chemical is called Magnesium, butylchloro-, and its CAS registry number is 693-04-9. With the molecular formula of C4H9ClMg, its product categories are Classes of Metal Compounds; Grignard Reagents; Grignard Reagents & Alkyl Metals; Mg (Magnesium) Compounds; Synthetic Organic Chemistry;T ypical Metal Compounds; AlkylChemical Synthesis; Organic Bases; Organometallic Reagents; Synthetic Reagents. In addition, this chemical should be sealed in the cool and dry place, away from oxides, acid , H2O, CO2.
Other characteristics of the Magnesium, butylchloro- can be summarised as followings: (1)#H bond acceptors: 0 #H bond donors: 0; (2)#Freely Rotating Bonds: 3.
Uses of this chemical: The Magnesium, butylchloro- could react with benzoic acid methyl ester, and obtain the 5-phenyl-nonan-5-ol. This reaction needs the solvent of diethyl ether. The yield is 60 %.
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When you are using this chemical, please be cautious about it as the following: This chemical is flammable. It causes burns. You should wear suitable protective clothing if you use it. In case of contacting with eyes, rinse immediately with plenty of water and seek medical advice.
You can still convert the following datas into molecular structure:
1.SMILES: CCCC[Mg]Cl
2.InChI: InChI=1/C4H9.ClH.Mg/c1-3-4-2;;/h1,3-4H2,2H3;1H;/q;;+1/p-1/rC4H9ClMg/c1-2-3-4-6-5/h2-4H2,1H3
3.InChIKey: UUNGXYVLXYGZKH-PEDMJPSNAP