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7786-30-3

Basic Information
CAS No.: 7786-30-3
Name: Magnesium chloride
Molecular Structure:
Molecular Structure of 7786-30-3 (Magnesium chloride)
Formula: Cl2Mg
Molecular Weight: 95.21
Synonyms: Magnesiumchloride (6CI,7CI,8CI);Aerotex Accelerator MX;C-TEK;Catalyst G;Ekimac;FIX-Mg;Freecat MX;HMC 23D;Magnesium dichloride;Magnesium(II) chloride;Magnogene;NSC 529832;TMT 2;White Nigari NS;Magnesium chloride anhydrous;
EINECS: 232-094-6
Density: 2.32 g/mL at 25 °C(lit.)
Melting Point: 714 °C(lit.)
Boiling Point: 1412 °C
Flash Point:
Solubility: 400 g/L (20 °C) in water
Appearance: white powder
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38-43-36/37
Safety: 26-36-24/25-22-36/37-39
Transport Information:
PSA: 0.00000
LogP: -5.99200
Synthetic route

Mg(2+)*2Mo(6+)*2Cl(1-)*6O(2-)*4C4H8O=[Mg(ClMoO3)2(C4H8O)4]

A

molybdenum(VI) oxide

B

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In tetrahydrofuran Ar atm.; hot THF;A 100%
B 100%
7439-95-4

magnesium

7646-85-7

zinc(II) chloride

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In melt melting the starting materials in an evacuated silica ampoule at 900°C for 48 h, cracking the ampoule under Ar;95%
In neat (no solvent) reduction of molten ZnCl2 with Mg forming MgCl2;;
In neat (no solvent) reduction of molten ZnCl2 with Mg forming MgCl2;;
10026-11-6

zirconium(IV) chloride

7439-95-4

magnesium

A

7440-67-7

zirconium

B

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In melt heating at 800°C under inert gas in a closed vessel, Kroll-process; apparatus described;; separation of Mg and MgCl2 by vacuum destillation;;A 93%
B n/a
In melt heating at 800°C under inert gas in a closed vessel, Kroll-process; apparatus described;; separation of Mg and MgCl2 by vacuum destillation;;A 93%
B n/a

magnesium silicide

ammonium chloride

silicon nitride

B

7664-41-7

ammonia

C

1333-74-0

hydrogen

D

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In neat (no solvent) High Pressure; mixed, sealed in autoclave under Ar, heated at 450, 500, 550, and 600 °C for 10 h; washed with water, dried in vac. at 70 °C for 12 h; powder XRD;A 93%
B n/a
C n/a
D n/a
194354-14-8

dichlorobis(3,5-di-tert-butylpyrazolylato)titanium(IV)

676-58-4

methylmagnesium chloride

A

222026-71-3

dimethylbis(3,5-di-tert-butylpyrazolylato)titanium(IV)

B

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In tetrahydrofuran; hexane Ar-atmosphere; MeMgCl soln. (THF) addn. (0°C), stirring (room temp., 20 h), evapn. (reduced pressure); extg. (hexane), filtering, evapn. (reduced pressure); elem. anal.;A 93%
B n/a
13170-43-9

(trimethylsilyl)methylmagnesium chloride

7721-01-9

tantalum pentachloride

594-09-2

trimethylphosphane

((CH3)3SiCH2)3Ta(P(CH3)3)(CHSi(CH3)3)

B

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In diethyl ether; hexane under N2 atm. slurry TaCl5 in hexane at -20°C was treated dropwise with Me3SiCH2MgCl in Et2O, solvent was removed in vacuo, residue was taken up in hexane at 0°C and filtered, PMe3 was added and heated to 50°C for 1 h; soln. was filtered, concd. and cooled to -20°C;A 92%
B n/a
154005-14-8, 141724-21-2, 162429-20-1, 100080-82-8, 112243-78-4

rac-ethanediyl-bis(1-indenyl)zirconium dichloride

75-16-1

methylmagnesium bromide

A

rac-ethylenebis(1-indenyl)zirconium dimethyl

B

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In 1,4-dioxane; diethyl ether; hexane (N2); dioxane was added to 3 M soln. MeMgBr in hexane and Et2O, stirred for 1 h, filtered, filtrate was added to soln. of zirconium complex in Et2O at -78°C, warmed to room temp. overnight; evapd., dissolved in benzene, filtered, evapd. in vac., crystd. from toluene/hexanes;A 91%
B n/a
925-90-6

ethylmagnesium bromide

palladium dichloride

A

74-84-0

ethane

B

74-85-1

ethene

C

7440-05-3

palladium

D

magnesium bromide

E

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In tetrahydrofuran To a soln. of anhydrous salt is added C2H5MgBr at 20°C with stirring. The reaction mixture is left for 5 - 6 h at room temp.; decantation, washing with THF, water and ethanol; electron diffraction;A n/a
B n/a
C 90%
D n/a
E n/a
185154-26-1

bis(η5-tetramethyl(trimethylsilyl)cyclopentadienyl)titanium dichloride

7439-95-4

magnesium

14630-40-1

Bis(trimethylsilyl)ethyne

A

195259-28-0

(η2-bis(trimethylsilyl)ethyne)bis(η5-tetramethyl(trimethylsilyl)cyclopentadienyl)titanium(II)

B

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In tetrahydrofuran -18°C (40 h), filtering, evapn. (vac.); extg. (hexane), MgCl2 pptn. (-5°C, overnight), concg., crystn. (-18°C, overnight); elem. anal.;A 80%
B n/a
7440-55-3

gallium

7439-95-4

magnesium

74-88-4

methyl iodide

A

7786-30-3

magnesium chloride

B

1445-79-0

trimethyl gallium

Conditions
ConditionsYield
In neat (no solvent) inert gas atmosphere; mixing, heating in autoclave (100 - 160°C, stirring, 12 h); distillation;A n/a
B 65%
7440-55-3

gallium

7439-95-4

magnesium

75-03-6

ethyl iodide

A

1115-99-7

triethyl gallium

B

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In hexane inert condition; addn. of hexane to mixt. of Mg and Ga (vac.), addn. of hexane, dropwise addn. of EtI (boiling hexane); distillation;A 65%
B n/a
7440-55-3

gallium

7553-56-2

iodine

7439-95-4

magnesium

75-03-6

ethyl iodide

A

1115-99-7

triethyl gallium

B

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In neat (no solvent) inert condition; addn. of I2 to mixt. of Mg and Ga, heating in vac. (150°C), chilling, addn. of EtI (50 - 70°C, 1 h), heating (90 °C, 4 h); distillation;A 61%
B n/a
245491-72-9

[ZrCl2(C32H38N4)]

6928-77-4

dibenzylmagnesium

A

253689-33-7

C39H45N4Zr(C4H8O)(CH2C6H5)

B

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In tetrahydrofuran; toluene stirring (room temp., 1 h); evapn., toluene addn., filtering, evapn., n-pentane addn., filtering, drying (vac.); elem. anal.;A 61%
B n/a
Ga(35),Mg(65) (X%)

Ga(35),Mg(65) (X%)

7553-56-2

iodine

75-03-6

ethyl iodide

A

1115-99-7

triethyl gallium

B

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In neat (no solvent) inert condition; addn. of I2 to alloy Mg-Ga, heating in vac. (150 °C), chilling, addn. of EtI), heating (85°C, 4 h); distillation;A 57%
B n/a
222026-71-3

dimethylbis(3,5-di-tert-butylpyrazolylato)titanium(IV)

75-64-9

tert-butylamine

A

222027-39-6, 210816-30-1

chlorotris(3,5-di-tert-butylpyrazolato)titanium(IV)

B

222027-00-1

(tert-butylimido(chloro)(3,5-di-tert-butylpyrazolato)titanium)2

C

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In hexane byproducts: tert-butylammonium chloride; Ar-atmosphere; stirring (room temp., 16 h); filtering, evapn. (reduced pressure), crystn. (hexane, -15°C, -20°C); elem. anal.;A 56%
B 10%
C n/a
222027-39-6, 210816-30-1

chlorotris(3,5-di-tert-butylpyrazolato)titanium(IV)

676-58-4

methylmagnesium chloride

A

222026-93-9

methyltris(3,5-di-tert-butylpyrazolylato)titanium(IV)

B

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In tetrahydrofuran Ar-atmosphere; MeMgCl soln. (THF) addn. (0°C), stirring (room temp., 20 h), evapn. (reduced pressure); extg. (hexane), filtering, evapn. (reduced pressure); elem. anal.;A 52%
B n/a
7439-95-4

magnesium

calcium chloride

A

1333-74-0

hydrogen

B

7786-30-3

magnesium chloride

C

calcium hydroxide

Conditions
ConditionsYield
With water In neat (no solvent) reduction of dry CaCl2 in H2-atmosphere on calcination with Mg; treatment of the reaction-products with H2O under formation of H2;;A 50%
B n/a
C n/a
With water In neat (no solvent) reduction of dry CaCl2 in H2-atmosphere on calcination with Mg; treatment of the reaction-products with H2O under formation of H2;;A 50%
B n/a
C n/a
With water In neat (no solvent) reduction of dry CaCl2 in CO2-atmosphere on calcination with Mg; treatment of the reaction-products with H2O under formation of H2;;A 30%
B n/a
C n/a
With water In neat (no solvent) reduction of dry CaCl2 in CO2-atmosphere on calcination with Mg; treatment of the reaction-products with H2O under formation of H2;;A 30%
B n/a
C n/a

1-chloro-2,3-dimethyl-1,2,3-arsadicarba-closo-dodecaborane(9)

1068-55-9

isopropylmagnesium chloride

A

1-isopropyl-2,3-dimethyl-1,2,3-arsadicarba-closo-dodecaborane(9)

B

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In diethyl ether under Ar, -80°C, molar ratio arsacarbollyl:(CH3)2CHMgCl=4.50:4.44, 1h stirring at room temp.; colorless ppt. is filtered off, solvent removed, extd. with hot hexane, evapd. to dryness, subl. in high vac. at 50°C, elem. anal.;A 50%
B n/a
131063-11-1, 16997-51-6, 19559-06-9

Vanadium (III) chloride-(tris-tetrahydrofuran)

879-06-1

pentafluorophenylmagnesium chloride

A

(C6F5)4V*2C4H8O

B

25377-37-1, 27790-75-6, 82009-22-1

Tetrakis(pyridin)-dichlorovanadin(II)

C

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In tetrahydrofuran 1 mol of complex was slowly added to an THF soln. of 2 mol RMgCl at -15°C, after 1 h the temp. was raised to room temp. (Ar atm.);; dioxane in Et2O was added, evapd., ppt. was washed with Et2O;;A 43%
B 47%
C n/a
131063-11-1, 16997-51-6, 19559-06-9

Vanadium (III) chloride-(tris-tetrahydrofuran)

13170-43-9

(trimethylsilyl)methylmagnesium chloride

A

25377-37-1, 27790-75-6, 82009-22-1

Tetrakis(pyridin)-dichlorovanadin(II)

B

41572-08-1

tetrakis(trimethylsilylmethyl)vanadium

C

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In diethyl ether 1 mol of complex was slowly added to an ether soln. of 2 mol RMgCl at -15°C, after 1 h the temp. was raised to room temp. (Ar atm.);; dioxane was added, ppt. was extd. with pentane; elem. anal.;;A 43%
B 45%
C n/a
194354-14-8

dichlorobis(3,5-di-tert-butylpyrazolylato)titanium(IV)

6921-34-2

benzylmagnesium chloride

A

222026-78-0

dibenzylbis(3,5-di-tert-butylpyrazolylato)titanium(IV)

B

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In diethyl ether; toluene Ar-atmosphere; BnMgCl soln. (Et2O) addn. (0°C), stirring (room temp., 16 h), evapn. (reduced pressure); extg. (hexane), filtering, concg. (reduced pressure), crystn. (-20°C, 2 d); elem. anal.;A 43%
B n/a
222027-44-3

trichloro-(3,5-di-tert-butylpyrazolylato)titanium(IV)

676-58-4

methylmagnesium chloride

A

222026-71-3

dimethylbis(3,5-di-tert-butylpyrazolylato)titanium(IV)

B

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In tetrahydrofuran; hexane Ar-atmosphere; pptn. on mixing reagents (-78°C, 0.25 h), stirring(room temp., 3 h), evapn. (reduced pressure); extg. (hexane), filtering, evapn. (reduced pressure);A 35%
B n/a
7637-07-2

boron trifluoride

10294-34-5

boron trichloride

A

boron

B

10043-11-5

boron nitride

C

7786-30-3

magnesium chloride

Conditions
ConditionsYield
700-1000°C; diluterd with N2; washing with HCl at 1000°C;A n/a
B 34%
C n/a

1-chloro-2,3-dimethyl-1,2,3-phosphadicarba-closo-dodecaborane(9)

1068-55-9

isopropylmagnesium chloride

A

1-isopropyl-2,3-dimethyl-1,2,3-phosphadicarba-closo-dodecaborane(9)

B

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In diethyl ether under Ar, -80°C, molar ratio ClP((CH3)2C2B9H9):(CH3)2CHMgCl=1:1, warmed to -20°C; colorless ppt. is filtered off, solvent removed, extd. with hot hexane, evapd. to dryness, subl. in high vac. at room temp., elem. anal.;A 33%
B n/a

brucite

7786-30-3

magnesium chloride

Conditions
ConditionsYield
With hydrogenchloride In neat (no solvent) heating of brucite at 383-412 °C in a stream of dry HCl with formation of MgCl2;10.33%
With HCl In neat (no solvent) heating of brucite at 383-412 °C in a stream of dry HCl with formation of MgCl2;10.33%
2386-64-3

ethylmagnesium chloride

993-10-2

methyltrichlorogermane

A

C7H17ClGe

B

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In butyldiglyme; ethyldiglym at 40℃; for 3h;
1068-55-9

isopropylmagnesium chloride

993-10-2

methyltrichlorogermane

A

C4H10Cl2Ge

B

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In butyldiglyme; ethyldiglym at 40℃; for 3h;
1068-55-9

isopropylmagnesium chloride

993-10-2

methyltrichlorogermane

A

C7H17ClGe

B

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In butyldiglyme; ethyldiglym at 40℃; for 3h;

C7H17ClGe

1068-55-9

isopropylmagnesium chloride

A

diethylisopropylmethylgermane

B

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In butyldiglyme; ethyldiglym for 1h;
97-93-8

triethylaluminum

62202-86-2

n-butyl-ethylmagnesium

A

14989-29-8

hydridomagnesium chloride

B

(AlEt3)2*MgEt2

C

693-04-9

butyl magnesium bromide

D

2386-64-3

ethylmagnesium chloride

E

7786-30-3

magnesium chloride

Conditions
ConditionsYield
In 2-Methylpentane for 4383h; Reactivity;
56-81-5

glycerol

7786-30-3

magnesium chloride

Mg(2+)*H(1+)*C3H5O3(3-)=C3H6O3Mg

Conditions
ConditionsYield
With copper In glycerol byproducts: CuCl; Electrolysis; electrolysis of MgCl2 in anhydrous glycerin, copper electrodes, formation of CuCl at the anode and of C3H6O3Mg at the cathode;;100%
With Cu In glycerol byproducts: CuCl; Electrolysis; electrolysis of MgCl2 in anhydrous glycerin, copper electrodes, formation of CuCl at the anode and of C3H6O3Mg at the cathode;;100%

chromium(VI) oxide

7786-30-3

magnesium chloride

magnesium chlorochromate

Conditions
ConditionsYield
In tetrachloromethane stirred vigorously for 3 d under N2; filtd. or evapn. of solvent under reduced pressure;99%

potassium dizirconiumenneaisopropoxide

zirconium isopropoxide

7786-30-3

magnesium chloride

164989-80-4

MgCl(Zr2(OC3H7)9)

Conditions
ConditionsYield
In isopropyl alcohol; benzene byproducts: KCl; reflux (2 h), volatiles removal, stirring (70°C, 10 h), KCl pptn.; filtration, volatiles removal (27°C, red. pressure), pptn., recrystn. (n-hexane/toluene) or volatilization (210°C, 0.01 mmHg); elem. anal.;99%

potassium dizirconiumenneaisopropoxide

zirconium isopropoxide

7786-30-3

magnesium chloride

164989-81-5, 57609-07-1

Mg(Zr2(OC3H7)9)2

Conditions
ConditionsYield
In isopropyl alcohol; benzene byproducts: KCl; reflux (2 h), volatiles removal, stirring (70°C, 10 h), KCl pptn., filtration, volatiles removal, (27°C, red. pressure), pptn.; volatilization (175°C, 0.1 mmHg) (70%); elem. anal.;99%

potassium tetraisopropoxyaluminate

555-31-7

aluminum isopropoxide

7786-30-3

magnesium chloride

164989-79-1

Mg(2+)*Cl(1-)*Al(OC3H7)4(1-)=MgCl(Al(OC3H7)4)

Conditions
ConditionsYield
In isopropyl alcohol; benzene byproducts: KCl; stirring (27°C, 12 h), pptn. (KCl), filtration; volatiles removal (reduced pressure, 27°C), recrystn. (hexane/toluene, -10°C); elem. anal.;99%
16940-66-2

sodium tetrahydroborate

7664-41-7

ammonia

7786-30-3

magnesium chloride

magnesium borohydride - ammonia (1/6)

Conditions
ConditionsYield
In diethyl ether under Ar atm. soln. Mg(BH4)2 in Et2O was prepared by react. MgCl2 and NaBH4 (V.N.Konoplev, Zh.Neorg.Khim., 1980, 25 (7), 1737-1740), anhydrous ammonia was passed through soln. at -10°C; react. mixt. was allowed to warm to room temp., volatiles were removed in vacuo; elem. anal.;99%
1295-35-8

bis(1,5-cyclooctadiene)nickel (0)

C42H33FP2Si

7786-30-3

magnesium chloride

C42H33ClNiP2Si

Conditions
ConditionsYield
In tetrahydrofuran at 20℃; for 1h; Reagent/catalyst; Inert atmosphere; Schlenk technique;99%

tin(IV) oxide

7786-30-3

magnesium chloride

7646-78-8

tin(IV) chloride

Conditions
ConditionsYield
With pyrographite In neat (no solvent) byproducts: MgO; heating of a mixture of SnO2 with double excess of MgCl2 forms 98.3 % SnCl4 at 800°C in presence of C;;98.3%
In neat (no solvent) byproducts: MgO; heating of a mixture of SnO2 with double excess of MgCl2 forms 74.60 % SnCl4 at 800°C;;74.6%
In neat (no solvent) byproducts: MgO; heating of a mixture of SnO2 with double excess of MgCl2 forms 58.79 % SnCl4 at 700°C; equilibrium reaction examinated;;58.79%

tin(IV) oxide

7786-30-3

magnesium chloride

tin(ll) chloride

Conditions
ConditionsYield
With pyrographite In neat (no solvent) byproducts: MgO, CO; formation at reaction of SnO2, MgCl2 and C under exclusion of air for 2 h at 800°C;; collecting of formed SnCl2 at 300-330°C in a condensator at exclusion of air;;98.3%
With C In neat (no solvent) byproducts: MgO, CO; formation at reaction of SnO2, MgCl2 and C under exclusion of air for 2 h at 800°C;; collecting of formed SnCl2 at 300-330°C in a condensator at exclusion of air;;98.3%
With pyrographite In neat (no solvent) byproducts: MgO, CO; heating of a mixture of SnO2 with double excess of MgCl2 in presence of C in 2 h at 523, 548 and 573°C forms liquid SnCl2; examination of the equilibrium reaction;;
1333-74-0

hydrogen

7439-95-4

magnesium

7786-30-3

magnesium chloride

63866-76-2

(HMgCl)2(C4H8O)2

Conditions
ConditionsYield
With tetrahydrofuran In tetrahydrofuran addn. of soln. of MgCl2 in THF to suspn. of Mg powder and catalyst in THF (under Ar), hydrogenation (H2-pressure 40-60 bar, 0°C, 18 h); centrifugation; not isolated;96%
With tetrahydrofuran In tetrahydrofuran addn. of soln. of MgCl2 in THF to suspn. of Mg powder and catalyst in THF (under Ar), hydrogenation (H2-pressure 50-70 bar, 0°C, 8 h); centrifugation; not isolated;59%
With tetrahydrofuran In tetrahydrofuran addn. of soln. of MgCl2 in THF to suspn. of Mg powder and catalyst in THF (under Ar), hydrogenation (H2-pressure 50-70 bar, 25°C, 40 h); centrifugation; not isolated;41%
With catalyst: TiCl4*2THF/ Mg-anthracene In tetrahydrofuran addn. of soln. of MgCl2 in THF to suspn. of Mg powder and catalyst in THF (under Ar), hydrogenation (H2-pressure 50-70 bar, 0°C, 40 h); centrifugation; not isolated;22%
With tetrahydrofuran In tetrahydrofuran addn. of soln. of MgCl2 in THF to suspn. of Mg powder and catalyst in THF (under Ar), hydrogenation (H2-pressure 50-70 bar, 60°C, 48 h); centrifugation; not isolated;15%

Na(1+)*Al(ONC(CH3)2)4(1-)=NaAl(ONC(CH3)2)4

7786-30-3

magnesium chloride

197501-39-6

Mg[Al(ONC(CH3)2)4]2

Conditions
ConditionsYield
In tetrahydrofuran byproducts: NaCl; (moisture free); reflux (4 h), NaCl pptn.; filtration, excess solvent removal (red. pressure), crystn., recrystn. (toluene, -20°C); elem anal.;96%
59-92-7

levodopa

7786-30-3

magnesium chloride

Mg(L-3,4-dioxyphenylalanine)2

Conditions
ConditionsYield
Stage #1: levodopa With potassium tert-butylate In tetrahydrofuran; N,N-dimethyl acetamide for 0.25h;
Stage #2: magnesium chloride In tetrahydrofuran; N,N-dimethyl acetamide
96%
76-05-1

trifluoroacetic acid

7786-30-3

magnesium chloride

38482-84-7, 123333-72-2

magnesium(II) 2,2,2-trifluoroacetate

Conditions
ConditionsYield
at 20 - 100℃; for 1h;95%
7786-30-3

magnesium chloride

sodium trispyrazolylborate

bis{hydrotris(pyrazolyl)borato}magnesium

Conditions
ConditionsYield
In water byproducts: NaCl; Trofimenko, S., J. Am. Chem. Soc., 89 (1967), 3170; crystd. (toluene/CH2Cl2), sublimed (vac.); elem. anal., TGA;94%

[Rh(1,10-phenanthroline)(NH3)4](CF3SO3)3

2051-10-7

5,6-chrysenedione

1310-73-2

sodium hydroxide

7786-30-3

magnesium chloride

[Rh(5,6-chrysenequinone diimmine)(1,10-phenanthroline)(NH3)2]Cl3

Conditions
ConditionsYield
Stage #1: [Rh(1,10-phenanthroline)(NH3)4](CF3SO3)3; 5,6-chrysenedione; sodium hydroxide In water; acetonitrile
Stage #2: magnesium chloride With sephadex QAE anionexchange column
94%
109-99-9

tetrahydrofuran

64770-14-5

tert-butyl acetoacetate sodium salt

7786-30-3

magnesium chloride

C56H94Mg2Na2O20

Conditions
ConditionsYield
at 20℃; for 72h; Inert atmosphere; Schlenk technique; Glovebox;94%
16940-66-2

sodium tetrahydroborate

110-71-4

1,2-dimethoxyethane

7786-30-3

magnesium chloride

Mg(2+)*2BH4(1-)*1.5CH3OCH2CH2OCH3=Mg(BH4)2*1.5CH3OCH2CH2OCH3

Conditions
ConditionsYield
In 1,2-dimethoxyethane mixt. of MgCl2, NaBH4 in DME was stirred for 10 h under inert atm; filtered, washed with DME, solvent was vac. distilled, extd. with CH2Cl2, CH2Cl2 was distilled in vacuo; elem. anal.;93%
for 7 - 22h; Inert atmosphere; Glovebox; Schlenk technique;85%
904693-44-3

2,5‐dihydroxyterephthalate

7786-30-3

magnesium chloride

iron(II) chloride

C8H4O6(2-)*0.1Fe(2+)*0.9Mg(2+)

Conditions
ConditionsYield
Stage #1: 2,5‐dihydroxyterephthalate; magnesium chloride; iron(II) chloride In methanol; N,N-dimethyl-formamide at 120℃; for 16h;
Stage #2: In N,N-dimethyl-formamide at 120℃; for 9h;
Stage #3: In methanol at 60℃;
93%
610-92-4

2,5-dihydroxy-1,4-benzenedicarboxylic acid

7786-30-3

magnesium chloride

iron(II) chloride

Fe0.1Mg1.9(2,5-dioxido-1,4-benzenedicarboxylate)

Conditions
ConditionsYield
In methanol; N,N-dimethyl-formamide at 120℃; for 16h;93%
546-68-9

titanium(IV) isopropylate

7786-30-3

magnesium chloride

1126433-59-7

Mg2Ti4Cl4(OCH(CH3)2)16

Conditions
ConditionsYield
In benzene soln. of Ti(OPr-i)4 (6.37 mol) in benzene added to slurry of MgCl2 (3.15mol) in benzene; stirred at room temp. until dissolution of MgCl2 (24 h ); reflux for 1 h; evapd. (vac. 0.5 mm, room temp.); crystd. at -20°C (hexane/CH2Cl2= 2:1); elem. anal.;91%
16940-66-2

sodium tetrahydroborate

7786-30-3

magnesium chloride

magnesium borohydride

Conditions
ConditionsYield
In diethyl ether ball milled and refluxed in Et2O;90%
In neat (no solvent) (Ar); mechanical action (3 h, room temp.); extn. (Et2O);76%
In not given

potassium heptafluorotantalate

7786-30-3

magnesium chloride

7721-01-9

tantalum pentachloride

Conditions
ConditionsYield
750 °C for 1 h in inert gas, molar ratio of K2TaF4:chloride = 1:2;90%
700-1000 °C in inert gas, molar ratio of K2TaF7:chloride = 1:2;
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    7786-30-3

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Chemistry

Molecule structure of Magnesium chloride anhydrous (CAS NO.7786-30-3):

IUPAC Name: Magnesium dichloride 
Molecular Weight: 95.211 g/mol
Molecular Formula: Cl2Mg 
Density: 2.32 g/mL at 25 °C(lit.)
Melting Point: 714 °C(lit.)
Boiling Point: 1412 °C
Refractive Index: n20/D 1.336
Storage Temp.: 2-8 °C
Water Solubility: 400 G/L (20 °C)
Sensitive: hygroscopic
H-Bond Acceptor: 2
Exact Mass: 93.922747
MonoIsotopic Mass: 93.922747
Heavy Atom Count: 3
Complexity: 2.8
Canonical SMILES: [Mg+2].[Cl-].[Cl-]
InChI: InChI=1S/2ClH.Mg/h2*1H;/q;;+2/p-2
InChIKey: TWRXJAOTZQYOKJ-UHFFFAOYSA-L
EINECS: 232-094-6
Product Categories: Inorganics;Crystal Grade Inorganics;Inorganic Salts;Magnesium Salts;MagnesiumMetal and Ceramic Science;Salts;Synthetic Reagents;G - M;Salt Solutions;Volumetric Solutions;PCR OptimizationMolecular Biology;PCR Reaction Components;PCR/Amplification;Optimization Reagents;BioUltraProtein Structural Analysis;DNA&RNA Purification;Molecular Biology;Molecular Biology Reagents;Optimization ReagentsMolecular Biology;Reagents;X-Ray Crystallography;BiochemicalsSynthetic Reagents;Magnesium;Companion Products and ReagentsSynthetic Reagents;Insect Platform;Serum-free Media

Uses

 Magnesium chloride anhydrous (CAS NO.7786-30-3) is used for the manufacture of metal magnesium, disinfectants, fire extinguishing agents, frozen brine, ceramics and also used in flipper fabric, paper making, and in the manufacture of oxychloride cement, etc.

Production

In the Dow process, Magnesium chloride anhydrous is regenerated from magnesium hydroxide using hydrochloric acid:
Mg(OH)2(s) + 2 HCl → MgCl2(aq) + 2 H2O(l)
It can also be prepared from magnesium carbonate by a similar reaction.

Toxicity Data With Reference

1.    

mmo-omi 8000 ppm

    APMBAY    Applied Microbiology. 6 (1958),45.
2.    

cyt-hmn:hla 2 mmol/L

    JCLLAX    Journal of Cellular Physiology. 78 (1971),217.
3.    

dns-rat-ipr 2500 µmol/kg

    JOENAK    Journal of Endocrinology. 65 (1975),45.
4.    

dni-rat:lvr 3300 µmol/L

    BIJOAK    Biochemical Journal. 146 (1975),697.
5.    

oms-mus:ast 4 mmol/L

    AMOKAG    Acta Medicia Okayama. 33 (1979),141.
6.    

orl-rat LD50:2800 mg/kg

    JPETAB    Journal of Pharmacology and Experimental Therapeutics. 35 (1929),1.
7.    

ipr-rat LDLo:225 mg/kg

    JPETAB    Journal of Pharmacology and Experimental Therapeutics. 35 (1929),1.
8.    

scu-rat LDLo:900 mg/kg

    ENDOAO    Endocrinology (Baltimore). 24 (1939),523.
9.    

ipr-mus LD50:1338 mg/kg

    COREAF    Comptes Rendus Hebdomadaires des Seances de lAcademie des Sciences. 256 (1963),1043.
10.    

ivn-mus LD50:14 mg/kg

    TXAPA9    Toxicology and Applied Pharmacology. 22 (1972),150.
11.    

 

Consensus Reports

Reported in EPA TSCA Inventory. EPA Genetic Toxicology Program.

Safety Profile

Hazard Codes: IrritantXi
Risk Statements: 36/37/38-43-36/37 
R36/37/38:Irritating to eyes, respiratory system and skin. 
R43:May cause sensitization by skin contact. 
R36/37:Irritating to eyes and respiratory system.
Safety Statements: 26-36-24/25-22-36/37-39 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36:Wear suitable protective clothing. 
S24/25:Avoid contact with skin and eyes. 
S22:Do not breathe dust. 
S36/37:Wear suitable protective clothing and gloves. 
S39:Wear eye / face protection.
WGK Germany: 1
RTECS: OM2800000
F: 3-10
Poison by intraperitoneal and intravenous routes. Moderately toxic by ingestion and subcutaneous routes. Human mutation data reported. In humid environments it causes steel to rust very rapidly. When heated to decomposition it emits toxic fumes of Cl. See also MAGNESIUM.

Specification

 Magnesium chloride anhydrous (CAS NO.7786-30-3) is also named as Aerotex Accelerator MX ; CCRIS 3961 ; Caswell No. 531 ; DUS-top ; EPA Pesticide Chemical Code 013902 ; HSDB 657 ; Magnesium chloride ; Magnesium chloride (Mg2Cl4) ; Magnesium chloride (MgCl2) ; Magnogene ; NSC 529832 ; TMT 2 ; UNII-59XN63C8VM . Magnesium chloride anhydrous (CAS NO.7786-30-3) is colorless, odorless and a small piece, particle, block-type monoclinic crystal. Its various hydrates MgCl2(H2O)x. These salts are typical ionic halides, being highly soluble in water.

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