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72287-26-4

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Basic Information
CAS No.: 72287-26-4
Name: [1,1'-Bis(diphenylphosphino)ferrocene]dichloropalladium(II)
Article Data: 25
Molecular Structure:
Molecular Structure of 72287-26-4 ([1,1'-Bis(diphenylphosphino)ferrocene]dichloropalladium(II))
Formula: C34H28Cl2FeP2Pd
Molecular Weight: 851.095
Synonyms: Palladium,[1,1'-bis(diphenylphosphino)ferrocene-P,P']dichloro-, (SP-4-2)-;Ferrocene,1,1'-bis(diphenylphosphino)-, palladium complex;(Bis(h5-(diphenylphosphino)cyclopentadienyl)iron)dichloropalladium;1,1'-Bis(diphenylphosphino)ferrocenedichloropalladium(II);1,1'-Bis(diphenylphosphino)ferrocenepalladium dichloride;Dichloro(diphenylphosphinoferrocene)palladium;Dichloro[1,1'-bis(diphenylphosphine)ferrocene]palladium(II);Dichloro[1,1'-bis(diphenylphosphino)ferrocene]palladium;Pd(dppf)Cl2;PdCl2(dppf);[1,1'-Bis(diphenylphosphino-kP)ferrocene]dichloropalladium;
EINECS: 460-040-3
Melting Point: 275-280 °C(lit.)
Hazard Symbols: HarmfulXn, IrritantXi
Risk Codes: 20/21/22-36/37/38-40
Safety: 23-24/25-26-36/37
PSA: 27.18000
LogP: 7.76790
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Synthetic route
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1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct

Conditions
ConditionsYield
In benzene stirred at room temp. for 12 h; ppt. filtered, washed with benzene, dried in vac., recrystn. (CHCl3); elem. anal.;97%
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chloroform

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1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct

Conditions
ConditionsYield
for 0.5h; Heating;
...Expand

sodium hexaflorophosphate

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1-((5-nitrofuran-2-yl)methylene)-4-phenylthiosemicarbazone

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dichloromethane

[palladium(II)(1,1’-bis(diphenylphosphino)ferrocene)(5-nitrofuryl-N-phenylthiosemicarbazonato)](hexafluorophosphate)*1.5(dichloromethane)

Conditions
ConditionsYield
Stage #1: 1-((5-nitrofuran-2-yl)methylene)-4-phenylthiosemicarbazone; 1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct In methanol at 20℃; for 1h;
Stage #2: sodium hexaflorophosphate In methanol for 24h; Cooling;
Stage #3: dichloromethane In methanol		71%
...Expand

sodium hexaflorophosphate

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4-ethyl-1-(5-nitrofuran2-yl-methylene)thiosemicarbazide

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dichloromethane

[palladium(II)(1,1’-bis(diphenylphosphino)ferrocene)(5-nitrofuryl-N-ethylthiosemicarbazonato)](hexafluorophosphate) dichloromethane disolvate

Conditions
ConditionsYield
Stage #1: 4-ethyl-1-(5-nitrofuran2-yl-methylene)thiosemicarbazide; 1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct In methanol at 20℃; for 1h;
Stage #2: sodium hexaflorophosphate In methanol for 24h; Cooling;
Stage #3: dichloromethane In methanol		64%
...Expand

sodium hexaflorophosphate

24199-84-6

5-nitrofurfural 4-methyl-thiosemicarbazone

72287-26-4

1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct

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dichloromethane

[palladium(II)(1,1’-bis(diphenylphosphino)ferrocene)(5-nitrofuryl-N-methylthiosemicarbazonato)](hexafluorophosphate) dichloromethane disolvate

Conditions
ConditionsYield
Stage #1: 5-nitrofurfural 4-methyl-thiosemicarbazone; 1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct In methanol at 20℃; for 1h;
Stage #2: sodium hexaflorophosphate In methanol for 24h; Cooling;
Stage #3: dichloromethane In methanol		62%
...Expand

sodium hexaflorophosphate

72287-26-4

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dichloromethane

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5-nitro-furfural thiosemicarbazone

[palladium(II)(1,1’-bis(diphenylphosphino)ferrocene)(5-nitrofuryl-thiosemicarbazonato)](hexafluorophosphate) dichloromethane monosolvate

Conditions
ConditionsYield
Stage #1: 1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct; 5-nitro-furfural thiosemicarbazone In methanol at 20℃; for 1h;
Stage #2: sodium hexaflorophosphate In methanol for 24h; Cooling;
Stage #3: dichloromethane In methanol		61%
...Expand

sodium hexaflorophosphate

72287-26-4

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Sodium salt of tropolone

[Pd(Trop)(1,1′-bis(dipheny1phosphino)ferrocene)](hexafluorophosphate)

Conditions
ConditionsYield
Stage #1: 1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct; Sodium salt of tropolone In methanol at 20℃; for 24h;
Stage #2: sodium hexaflorophosphate In methanol for 24h;		49%
...Expand

sodium hexaflorophosphate

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1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct

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sodium salt of 4-isopropyltropolone

[Pd(Hino)(1,1′-bis(dipheny1phosphino)ferrocene)](hexafluorophosphate)

Conditions
ConditionsYield
Stage #1: 1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct; sodium salt of 4-isopropyltropolone In methanol for 6h; Reflux;
Stage #2: sodium hexaflorophosphate In methanol for 24h;		44%
...Expand

sodium hexaflorophosphate

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1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct

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nitroxoline

[PdII(5-nitro-8-quinolinolynate)(1,1’-bis(diphenylphosphino)ferrocene)](PF6)

Conditions
ConditionsYield
Stage #1: 1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct; nitroxoline With triethylamine In methanol for 5h; Reflux;
Stage #2: sodium hexaflorophosphate In methanol for 0.25h;		41%
...Expand

sodium hexaflorophosphate

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1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct

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chloroxine

[PdII(5,7-dichloro-8-quinolinolynate)(1,1’-bis(diphenylphosphino)ferrocene)](PF6)

Conditions
ConditionsYield
Stage #1: 1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct; chloroxine With triethylamine In methanol at 20℃; for 15 - 24h;
Stage #2: sodium hexaflorophosphate In methanol for 0.25h;		37%
...Expand
Raw Materials
12107-56-1
12150-46-8
124268-93-5
532-32-1
75-05-8
14323-43-4
532-31-0
12317-46-3
Downstream Products
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Chemistry

The Molecular Structure of  [1,1'-Bis(diphenylphosphino)ferrocene]dichloropalladium(II) (CAS NO.72287-26-4):

Empirical Formula: C34H28Cl2FeP2Pd
Molecular Weight: 731.7046
Nominal Mass: 730 Da
Average Mass: 731.7046 Da
Monoisotopic Mass: 729.942753 Da 
Melting Point: 275-280 °C(lit.)
Product Categories: Metal Compounds;pharmacetical;API intermediates;Catalysts-Ligands;Catalysts for Organic Synthesis;Classes of Metal Compounds;Fe (Iron) Compounds;Ferrocenes;Homogeneous Catalysts;Metal Complexes;Metallocenes;Pd (Palladium) Compounds;Synthetic Organic Chemistry;Transition Metal Compounds;Catalysis and Inorganic Chemistry;Homogeneous Pd Catalysts;Palladium 

Safety Profile

Hazard Codes: HarmfulXnIrritantXi
Risk Statements: 20/21/22-36/37/38-40 
R20/21/22:Harmful by inhalation, in contact with skin and if swallowed
R36/37/38:Irritating to eyes, respiratory system and skin
Safety Statements: 23-24/25-26-36/37 
S23:Do not breathe vapour
S24/25:Avoid contact with skin and eyes
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
S36/37:Wear suitable protective clothing and gloves
Hazard Note: Irritant

Specification

 [1,1'-Bis(diphenylphosphino)ferrocene]dichloropalladium(II) (CAS NO.72287-26-4) is also called as1,1-Bis(diphenylphosphino)ferrocenedichloropalladium(ii) ; 1,1'-Bis(diphenylphosphino)ferrocene palladium dichloride ; 1,1'-Bis(diphenylphosphino)ferrocenepalladium(ii) dichloride ; Pdcl2(dppf);dichloro(1,1'-bis(diphenylphosphino)ferrocene)palladium (ii) dichloromethane add ; [1,1'-Bis(diphenylphosphino)ferrocene]dichloropalladium ; (ii)Dichloromethane adduct .

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