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CAS No.: | 7450-69-3 |
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Name: | PHENYLPHOSPHORODIAMIDATE |
Article Data: | 11 |
Molecular Structure: | |
Formula: | C6H9 N2 O2 P |
Molecular Weight: | 172.123 |
Synonyms: | Phenylphosphorodiamidate (6CI,7CI); Diamidophosphoric acid phenyl ester; Phenyldiamidophosphate; Phenyl phosphate diamide; Phosphoric acid phenyl esterdiamide |
Density: | 1.34g/cm3 |
Melting Point: | 183-185 °C |
Boiling Point: | 313.8ºC at 760 mmHg |
Flash Point: | 143.6ºC |
Solubility: | 5.6g/L at 20℃ |
Appearance: | white to grey powder and flakes |
Risk Codes: | R25; R36/37/38 |
Safety: | 608629 |
PSA: | 88.15000 |
LogP: | 2.49150 |
Conditions | Yield |
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With ammonium hydroxide at -10℃; for 2.5h; | 90% |
With ammonia In water at 5 - 20℃; | 88% |
With ammonia In dichloromethane for 0.166667h; | 17.4% |
Conditions | Yield |
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With pyridine; chloroform; trichlorophosphate at -2℃; Eintragen des Reaktionsgemisches in fluessiges NH3; |
Conditions | Yield |
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In sodium hydroxide boiling phenyl ester for 5 min in 4 M NaOH; cooling, addn. of EtOH, pptn., recrystn. (H2O-EtOH), drying (air, room temp.); elem. anal.; | 80% |
phenyl diamidophosphate
malonoyl dichloride
2-Phenyloxy-4,6-dioxo-hexahydro-1,3,2-diazphosphorin-2-oxid
Conditions | Yield |
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In diethyl ether 1.) R.T., 3 h, 2.) reflux, 1 h; | 17% |
Conditions | Yield |
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With sodium hydroxide In isopropyl alcohol |
methyltrimethylsilylamine
phenyl diamidophosphate
N,N'-Bis-trimethylsilyl-diamidophosphorsaeure-phenylester
Conditions | Yield |
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In diethyl ether |
phenyl diamidophosphate
1,1,1,3,3,3-hexamethyl-disilazane
N,N'-Bis-trimethylsilyl-diamidophosphorsaeure-phenylester
methanol
phenyl diamidophosphate
A
Diamidophosphorsaeuremethylester
B
phenol
Conditions | Yield |
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With water; manganese(ll) chloride at 25℃; methanolysis, also without H2O; |
Conditions | Yield |
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In water at 30℃; libratation from carboxymethylcellulose and hydrolysis; |