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7632-51-1

Basic Information
CAS No.: 7632-51-1
Name: VANADIUM (IV) CHLORIDE
Article Data: 110
Molecular Structure:
Molecular Structure of 7632-51-1 (VANADIUM (IV) CHLORIDE)
Formula: Cl4V
Molecular Weight: 192.754
Synonyms: Vanadiumchloride (VCl4) (8CI); Tetrachlorovanadium; Vanadium tetrachloride;Vanadium(IV) chloride
EINECS: 231-561-1 VCl4
Density: 1.816 g/mL at 25 °C(lit.)
Melting Point: -28 C
Boiling Point: 148 - 153 C
Flash Point: 148.5°C/755mm
Solubility: soluble alcohol, ether [HAW93]
Appearance: red to brown liquid
Hazard Symbols: 8 (Packing Group: I) UN NO.
Risk Codes: 14-23/24/25-34
Transport Information: 8 (Pack
PSA: 0.00000
LogP: 2.75800
Synthetic route
7440-62-2

vanadium

7782-50-5

chlorine

7632-51-1

vanadiumtetrachloride

Conditions
ConditionsYield
In neat (no solvent) heating 97% V and Cl2 at 200 - 250°C; reaction time: 6 - 8 h;;95%
In neat (no solvent) heating 97% V and Cl2 at 200 - 250°C; reaction time: 6 - 8 h;;95%
In neat (no solvent) react. of V powder with gaseous Cl2 at ambient temp., faster on heating;;

descloizite

7632-51-1

vanadiumtetrachloride

Conditions
ConditionsYield
With magnesium chloride In neat (no solvent) reaction by roasting of descloizite with MgCl2*H2O;;43%

vanadinite

7632-51-1

vanadiumtetrachloride

Conditions
ConditionsYield
With magnesium chloride In neat (no solvent) reaction by roasting of vanadinite with MgCl2*H2O;;43%
7440-62-2

vanadium

silver(I) chloride

7632-51-1

vanadiumtetrachloride

Conditions
ConditionsYield
In neat (no solvent) heating under back flow, 800°C;;
In tetrachloromethane heating at 800°C;;
7440-62-2

vanadium

7647-14-5

sodium chloride

7632-51-1

vanadiumtetrachloride

Conditions
ConditionsYield
In neat (no solvent) Electrolysis; crumbling of V-anode;; leakage of VCl4;;
In neat (no solvent) Electrolysis; crumbling of V-anode;; leakage of VCl4;;

vanadia

7782-50-5

chlorine

7704-34-9

sulfur

A

10025-67-9

disulfur dichloride

B

10545-99-0

sulfur dichloride

C

7632-51-1

vanadiumtetrachloride

D

7727-18-6

vanadium(V) oxychloride

Conditions
ConditionsYield
In neat (no solvent) heating;;
7440-62-2

vanadium

7719-09-7

thionyl chloride

7632-51-1

vanadiumtetrachloride

Conditions
ConditionsYield
In neat (no solvent) byproducts: S2, SO2; react. of V-powder with streaming SOCl2 at 600 to 700°C;; gaseous VCl4 besides gaseous S2 and SO2 obtained;;
In neat (no solvent)
75-44-5

phosgene

7440-62-2

vanadium

7719-09-7

thionyl chloride

7632-51-1

vanadiumtetrachloride

Conditions
ConditionsYield
In neat (no solvent) byproducts: S2, CO; react. of V-powder with streaming SOCl2 and COCl2 at 600 to 700°C;; gaseous VCl4 besides gaseous S2 and CO obtained;;
10025-67-9

disulfur dichloride

7440-62-2

vanadium

7632-51-1

vanadiumtetrachloride

Conditions
ConditionsYield
In neat (no solvent) byproducts: S2, SO2; react. of V-powder with streaming S2Cl2 at 600 to 700°C;; gaseous VCl4 besides gaseous S2 and SO2 obtained;;
In neat (no solvent)
7440-62-2

vanadium

mercury(I) chloride

7632-51-1

vanadiumtetrachloride

Conditions
ConditionsYield
In neat (no solvent) heating under back flow, 600°C;;
In tetrachloromethane heating at 600°C;;
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    Vanadium (IV) Chloride

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Chemistry

Product Name: Vanadium tetrachloride (7632-51-1)


Molecular Formula: Cl4V
Molecular Weight: 192.75g/mol
Mol File: 7632-51-1.mol
Einecs: 231-561-1
Appearance: red to brown liquid
Melting Point: -28 °C(lit.)
Boiling point: 154 °C(lit.)
Storage Temperature: water-free area
Flash Point: 148.5°C/755mm
Density: 1.816 g/mL at 25 °C(lit.)
Sensitive: Moisture Sensitive
Product Categories: Catalysis and Inorganic Chemistry; Chemical Synthesis; Salts; Vanadium Salts; VanadiumMetal and Ceramic Science
Synonyms of  Vanadium tetrachloride (7632-51-1): vanadium chloride;vanadium (iv) chloride;vanadium tetrachloride;(beta-4)-vanadiumchloride(vcl4;(t-4)-vanadiumchloride(vcl4;tetrachlorovanadium;vanadium chloride (vcl4), (t-4)-;vanadiumchloride(vcl4)

Toxicity Data With Reference

Corrosive and/or toxic; inhalation, ingestion or contact (skin, eyes) with vapors, dusts or substance may cause severe injury, burns or death. Fire will produce irritating, corrosive and/or toxic gases. Reaction with water may generate much heat that will increase the concentration of fumes in the air. Contact with molten substance may cause severe burns to skin and eyes. Runoff from fire control or dilution water may cause pollution.

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
rat LD50 oral 160mg/kg (160mg/kg)   American Industrial Hygiene Association Journal. Vol. 30, Pg. 470, 1969.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Poison by ingestion. A corrosive irritant to skin, eyes, and mucous membranes. When heated to decomposition it emits toxic fumes of VOx and Cl. See also VANADIUM COMPOUNDS and HYDROCHLORIC ACID.
Except for acetic anhydride (un1715), that is flammable, some of these materials may burn, but none ignite readily. May ignite combustibles (wood, paper, oil, clothing, etc.). Substance will react with water (some violently), releasing corrosive and/or toxic gases and runoff. Flammable/toxic gases may accumulate in confined areas (basement, tanks, hopper/tank cars, etc.). Contact with metals may evolve flammable hydrogen gas. Containers may explode when heated or if contaminated with water. Substance may be transported in a molten form.
Safety Information of Vanadium tetrachloride (7632-51-1):
Hazard Codes: T
Risk Statements: 14-23/24/25-34
14:  Reacts violently with water 
23:  Toxic by inhalation 
24:  Toxic in contact with skin 
25:  Toxic if swallowed 
34:  Causes burns 
Safety Statements: 26-27-36/37/39-45
26:  In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 
36:  Wear suitable protective clothing  
37:  Wear suitable gloves 
39:  Wear eye/face protection
45:  In case of accident or if you feel unwell, seek medical advice immediately (show label where possible)

Standards and Recommendations

ACGIH TLV: TWA 0.05 mg(V2O5)/m3
NIOSH REL: (Vanadium Compounds) CL 0.05 mg(V)/m3/15M
DOT Classification:  6.1; Label: Poison